Mechanochemical synthesis of ZnO nanostructured powder using a different organic surfactants and its influence on the particles size and morphology
Конференцијски прилог (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
Pure zinc oxide (ZnO) nanostructured powder was prepared by mechanochemical method followed by heat-treatment in a planetary ball-mill using agate jars and alumina balls. The frequency of the rotation of jars around the common axis was 180 per minute, activation times were from 30 min to 4 h. Mechanochemical processing involves the mechanical activation of reactant mixture in a liquid phase (wet milling). We studied influence of organic surfactants on reduction of ZnO particles size, their shape and size distribution. As a process controlling agent (PCA), we used different organic compounds such as oxalic acid, oleic acid and isopropanol. After milling procedure, intermediate compounds were calcinated in air to form ZnO powder. Powders characterization was preformed using X-ray diffraction method (XRD) and scanning electron microscopy (SEM).
Кључне речи:
mechanochemical synthesis / nanostructured powders / ZnO / zinc oxideИзвор:
Programme and The Book of Abstracts / Eleventh Annual Conference YUCOMAT 2009, Herceg Novi, August 31 – September 4, 2009, 2009, 164-164Издавач:
- Belgrade : Institute of Technical Sciences of SASA
Финансирање / пројекти:
- Синтеза функционалних материјала са контролисаном структуром на молекуларном и нано нивоу (RS-MESTD-MPN2006-2010-142006)
Напомена:
Повезане информације:
- Повезани садржај
https://hdl.handle.net/21.15107/rcub_dais_263
Институција/група
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - CONF AU - Stanković, Ana AU - Veselinović, Ljiljana AU - Uskoković, Dragan PY - 2009 UR - https://dais.sanu.ac.rs/123456789/14848 AB - Pure zinc oxide (ZnO) nanostructured powder was prepared by mechanochemical method followed by heat-treatment in a planetary ball-mill using agate jars and alumina balls. The frequency of the rotation of jars around the common axis was 180 per minute, activation times were from 30 min to 4 h. Mechanochemical processing involves the mechanical activation of reactant mixture in a liquid phase (wet milling). We studied influence of organic surfactants on reduction of ZnO particles size, their shape and size distribution. As a process controlling agent (PCA), we used different organic compounds such as oxalic acid, oleic acid and isopropanol. After milling procedure, intermediate compounds were calcinated in air to form ZnO powder. Powders characterization was preformed using X-ray diffraction method (XRD) and scanning electron microscopy (SEM). PB - Belgrade : Institute of Technical Sciences of SASA C3 - Programme and The Book of Abstracts / Eleventh Annual Conference YUCOMAT 2009, Herceg Novi, August 31 – September 4, 2009 T1 - Mechanochemical synthesis of ZnO nanostructured powder using a different organic surfactants and its influence on the particles size and morphology SP - 164 EP - 164 UR - https://hdl.handle.net/21.15107/rcub_dais_14848 ER -
@conference{ author = "Stanković, Ana and Veselinović, Ljiljana and Uskoković, Dragan", year = "2009", abstract = "Pure zinc oxide (ZnO) nanostructured powder was prepared by mechanochemical method followed by heat-treatment in a planetary ball-mill using agate jars and alumina balls. The frequency of the rotation of jars around the common axis was 180 per minute, activation times were from 30 min to 4 h. Mechanochemical processing involves the mechanical activation of reactant mixture in a liquid phase (wet milling). We studied influence of organic surfactants on reduction of ZnO particles size, their shape and size distribution. As a process controlling agent (PCA), we used different organic compounds such as oxalic acid, oleic acid and isopropanol. After milling procedure, intermediate compounds were calcinated in air to form ZnO powder. Powders characterization was preformed using X-ray diffraction method (XRD) and scanning electron microscopy (SEM).", publisher = "Belgrade : Institute of Technical Sciences of SASA", journal = "Programme and The Book of Abstracts / Eleventh Annual Conference YUCOMAT 2009, Herceg Novi, August 31 – September 4, 2009", title = "Mechanochemical synthesis of ZnO nanostructured powder using a different organic surfactants and its influence on the particles size and morphology", pages = "164-164", url = "https://hdl.handle.net/21.15107/rcub_dais_14848" }
Stanković, A., Veselinović, L.,& Uskoković, D.. (2009). Mechanochemical synthesis of ZnO nanostructured powder using a different organic surfactants and its influence on the particles size and morphology. in Programme and The Book of Abstracts / Eleventh Annual Conference YUCOMAT 2009, Herceg Novi, August 31 – September 4, 2009 Belgrade : Institute of Technical Sciences of SASA., 164-164. https://hdl.handle.net/21.15107/rcub_dais_14848
Stanković A, Veselinović L, Uskoković D. Mechanochemical synthesis of ZnO nanostructured powder using a different organic surfactants and its influence on the particles size and morphology. in Programme and The Book of Abstracts / Eleventh Annual Conference YUCOMAT 2009, Herceg Novi, August 31 – September 4, 2009. 2009;:164-164. https://hdl.handle.net/21.15107/rcub_dais_14848 .
Stanković, Ana, Veselinović, Ljiljana, Uskoković, Dragan, "Mechanochemical synthesis of ZnO nanostructured powder using a different organic surfactants and its influence on the particles size and morphology" in Programme and The Book of Abstracts / Eleventh Annual Conference YUCOMAT 2009, Herceg Novi, August 31 – September 4, 2009 (2009):164-164, https://hdl.handle.net/21.15107/rcub_dais_14848 .