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One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles
dc.creator | Jeremić, Dejan | |
dc.creator | Anđelković, Ljubica | |
dc.creator | Milenković, Milica R. | |
dc.creator | Šuljagić, Marija | |
dc.creator | Šumar Ristović, Maja | |
dc.creator | Ostojić, Sanja | |
dc.creator | Nikolić, Aleksandar S. | |
dc.creator | Vulić, Predrag | |
dc.creator | Brčeski, Ilija | |
dc.creator | Pavlović, Vladimir B. | |
dc.date.accessioned | 2021-11-16T11:45:01Z | |
dc.date.available | 2021-11-16T11:45:01Z | |
dc.date.issued | 2020 | |
dc.identifier.issn | 0350-820X | |
dc.identifier.uri | https://dais.sanu.ac.rs/123456789/12085 | |
dc.description.abstract | This work is the first report of a very simple and fast one-pot synthesis of nickel oxide (NiO) and hematite (α-Fe2O3) nanoparticles by thermal decomposition of transition metal aqua complexes with camphor sulfonate anions. Obtained nanopowders were characterized by X-ray powder diffraction, Fourier transform IR analysis, scanning electron microscopy, and Energy-dispersive X-ray spectroscopy. X-ray powder diffraction confirmed the formation of high purity NiO and α-Fe2O3 crystal phases. In the case of α-Fe2O3, about five times larger average crystallite size was obtained. Fourier transform IR spectra of synthesized materials showed characteristic peaks for NiO and α-Fe2O3 nanostructures. To visualize the morphology and the chemical composition of the final products Scanning electron microscopy and Energy-dispersive X-ray spectroscopy were performed. The thermogravimetric analysis was done for a better understanding of the general thermal behavior of precursor compounds. This easy-to-perform and fast preparation method opens a broad range of obtained materials’ usage, particularly due to its economic viability | |
dc.relation | info:eu-repo/grantAgreement/MESTD/inst-2020/200026/RS// | |
dc.relation | info:eu-repo/grantAgreement/MESTD/inst-2020/200168/RS// | |
dc.relation | info:eu-repo/grantAgreement/MESTD/inst-2020/200168/RS// | |
dc.relation | info:eu-repo/grantAgreement/MESTD/inst-2020/200116/RS// | |
dc.rights | openAccess | |
dc.rights.uri | https://creativecommons.org/licenses/by/4.0/ | |
dc.source | Science of Sintering | |
dc.subject | nanomaterials | |
dc.subject | nickel oxide | |
dc.subject | hematite | |
dc.subject | camphor sulfonates | |
dc.subject | one-pot synthesis | |
dc.title | One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles | |
dc.type | article | en |
dc.rights.license | BY | |
dc.citation.spage | 481 | |
dc.citation.epage | 490 | |
dc.citation.volume | 52 | |
dc.citation.issue | 4 | |
dc.identifier.wos | 000600505000009 | |
dc.identifier.doi | 10.2298/SOS2004481J | |
dc.identifier.scopus | 2-s2.0-85098651318 | |
dc.type.version | publishedVersion | |
dc.identifier.fulltext | https://dais.sanu.ac.rs/bitstream/id/48141/One-pot_combustion_pub_2020.pdf | |
dc.identifier.rcub | https://hdl.handle.net/21.15107/rcub_dais_12085 |