Tadić, Nenad B.

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Authority KeyName Variants
orcid::0000-0001-9002-9779
  • Tadić, Nenad B. (23)
  • Tadić, Nenad (7)
Projects
Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200175 (Institute of Technical Sciences of SASA, Belgrade) Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing
Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200053 (University of Belgrade, Institute for Multidisciplinary Research) Lithium-ion batteries and fuel cells - research and development
Integration of PAper-based Nucleic acid testing mEthods into Microfluidic devices for improved biosensing Applications Directed synthesis, structure and properties of multifunctional materials
Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200105 (University of Belgrade, Faculty of Mechanical Engineering) Nanostructured Functional and Composite Materials in Catalytic and Sorption Processes
Bilateral collaboration between Serbia and Slovenia (BI-RS-18-19-026) Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200026 (University of Belgrade, Institute of Chemistry, Technology and Metallurgy - IChTM)
Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 451-03-68/2020-14/200116 (University of Belgrade, Faculty of Agriculture) Ministry for Education, Science and Technological Development of the Republic of Serbia
National Science Foundation grant DMR-1523617 National Science Foundation grant HRD-1345219
Serbian Academy of Sciences and Arts, Project F-198

Author's Bibliography

Structural characteristics of MgAl2O4 spinel

Peleš Tadić, Adriana; Živojinović, Jelena; Tadić, Nenad; Lević, Steva; Marković, Smilja; Pavlović, Vladimir B.; Filipović, Suzana; Obradović, Nina

(Belgrade : Serbian Ceramic Society, 2023)

TY  - CONF
AU  - Peleš Tadić, Adriana
AU  - Živojinović, Jelena
AU  - Tadić, Nenad
AU  - Lević, Steva
AU  - Marković, Smilja
AU  - Pavlović, Vladimir B.
AU  - Filipović, Suzana
AU  - Obradović, Nina
PY  - 2023
UR  - https://dais.sanu.ac.rs/123456789/15759
AB  - Magnesium aluminate spinel (MgAl2O4) is a material with good mechanical, chemical, and thermal properties, low dielectric permeability and loss tangent. Based on those properties, MgAl2O4 has found a significant application in refractory ceramics, ceramics windows, integrated electronic devices, etc. Also, it possesses a high chemical and radiation resistance. In this research, MgO was calcined at 1000ºC for an hour, with a step of 10ºC/min to avoid presence of hydroxide or carbonate. MgO and Al2O3 powders were mixed in a one-to-one molar ratio afterwards. The powders were mechanically activated for 15, 30, and 60 minutes. The mass ratio of powder and balls was 1:40. The mechanically activated powders are pressed in the tablets, under the pressure of 0.5 t. The pressed powders were heated up to 1300 ºC with a step of 10 ºC/min and held for 1 h for the reaction. Reacted pellets were crushed and sieved. Obtained spinel powders were sintered at 1450 ºC for 2 h. Both sintered and non-sintered samples were investigated by XRD and SEM. The particle size distribution of the reacted powders was investigated by laser diffraction analysis. Raman spectroscopy was used to determine the lattice vibration in the sintered samples. All results are in accordance with our previous results, and the pure dense spinel phase is obtained.
PB  - Belgrade : Serbian Ceramic Society
C3  - Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application XI New Frontiers in Multifunctional Material Science and Processing, Serbian Academy of Sciences and Art Serbia, Belgrade,18-20.September 2023
T1  - Structural characteristics of MgAl2O4 spinel
SP  - 52
EP  - 52
UR  - https://hdl.handle.net/21.15107/rcub_dais_15759
ER  - 
@conference{
author = "Peleš Tadić, Adriana and Živojinović, Jelena and Tadić, Nenad and Lević, Steva and Marković, Smilja and Pavlović, Vladimir B. and Filipović, Suzana and Obradović, Nina",
year = "2023",
abstract = "Magnesium aluminate spinel (MgAl2O4) is a material with good mechanical, chemical, and thermal properties, low dielectric permeability and loss tangent. Based on those properties, MgAl2O4 has found a significant application in refractory ceramics, ceramics windows, integrated electronic devices, etc. Also, it possesses a high chemical and radiation resistance. In this research, MgO was calcined at 1000ºC for an hour, with a step of 10ºC/min to avoid presence of hydroxide or carbonate. MgO and Al2O3 powders were mixed in a one-to-one molar ratio afterwards. The powders were mechanically activated for 15, 30, and 60 minutes. The mass ratio of powder and balls was 1:40. The mechanically activated powders are pressed in the tablets, under the pressure of 0.5 t. The pressed powders were heated up to 1300 ºC with a step of 10 ºC/min and held for 1 h for the reaction. Reacted pellets were crushed and sieved. Obtained spinel powders were sintered at 1450 ºC for 2 h. Both sintered and non-sintered samples were investigated by XRD and SEM. The particle size distribution of the reacted powders was investigated by laser diffraction analysis. Raman spectroscopy was used to determine the lattice vibration in the sintered samples. All results are in accordance with our previous results, and the pure dense spinel phase is obtained.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application XI New Frontiers in Multifunctional Material Science and Processing, Serbian Academy of Sciences and Art Serbia, Belgrade,18-20.September 2023",
title = "Structural characteristics of MgAl2O4 spinel",
pages = "52-52",
url = "https://hdl.handle.net/21.15107/rcub_dais_15759"
}
Peleš Tadić, A., Živojinović, J., Tadić, N., Lević, S., Marković, S., Pavlović, V. B., Filipović, S.,& Obradović, N.. (2023). Structural characteristics of MgAl2O4 spinel. in Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application XI New Frontiers in Multifunctional Material Science and Processing, Serbian Academy of Sciences and Art Serbia, Belgrade,18-20.September 2023
Belgrade : Serbian Ceramic Society., 52-52.
https://hdl.handle.net/21.15107/rcub_dais_15759
Peleš Tadić A, Živojinović J, Tadić N, Lević S, Marković S, Pavlović VB, Filipović S, Obradović N. Structural characteristics of MgAl2O4 spinel. in Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application XI New Frontiers in Multifunctional Material Science and Processing, Serbian Academy of Sciences and Art Serbia, Belgrade,18-20.September 2023. 2023;:52-52.
https://hdl.handle.net/21.15107/rcub_dais_15759 .
Peleš Tadić, Adriana, Živojinović, Jelena, Tadić, Nenad, Lević, Steva, Marković, Smilja, Pavlović, Vladimir B., Filipović, Suzana, Obradović, Nina, "Structural characteristics of MgAl2O4 spinel" in Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application XI New Frontiers in Multifunctional Material Science and Processing, Serbian Academy of Sciences and Art Serbia, Belgrade,18-20.September 2023 (2023):52-52,
https://hdl.handle.net/21.15107/rcub_dais_15759 .

Influence of Fe Doping on the Crystal Structure and Optical Properties of Mechanically Activated SrTiO3 Powders

Živojinović, Jelena; Peleš Tadić, Adriana; Kosanović, Darko; Tadić, Nenad; Vasiljević, Zorka Ž.; Lević, Steva; Obradović, Nina

(Belgrade : Serbian Ceramic Society, 2023)

TY  - CONF
AU  - Živojinović, Jelena
AU  - Peleš Tadić, Adriana
AU  - Kosanović, Darko
AU  - Tadić, Nenad
AU  - Vasiljević, Zorka Ž.
AU  - Lević, Steva
AU  - Obradović, Nina
PY  - 2023
UR  - https://dais.sanu.ac.rs/123456789/15007
AB  - Iron-doped strontium-titanate (SrTiO3) powders with various iron(III) oxide (Fe2O3) weight percentages (1.5, 3 and 6 wt%) were prepared by a solid-state method in the presence of mechanical activation (10, 30 and 120 min). A systematic investigation by XRD, SEM and Raman spectroscopy has been undertaken to evaluate the role of dopant on the microstructural and morphological study of the perovskite oxide obtained. The optical properties of the different iron-doped and activated Fe-SrTiO3 powders have been also evaluated. The results demonstrated that Fe has been substituted into the lattice and surface layers of particles of SrTiO3 powders and the absorption edge shifted to higher wavelength values with increasing activation time and dopant weight percentage. The lowest value of the band gap (Eg=3.20 eV) was registered for the longest activation (120 min) and the highest weight percentage of dopant (6 wt%). Combining doping with mechanical activation, led to lower values of Eg and that fact could be used in subsequent studies to make Fe-SrTiO3 more suitable photocatalysts.
PB  - Belgrade : Serbian Ceramic Society
C3  - Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application XI New Frontiers in Multifunctional Material Science and Processing, Serbian Academy of Sciences and Art Serbia, Belgrade,18-20.September 2023
T1  - Influence of Fe Doping on the Crystal Structure and Optical Properties of Mechanically Activated SrTiO3 Powders
SP  - 51
EP  - 51
UR  - https://hdl.handle.net/21.15107/rcub_dais_15007
ER  - 
@conference{
author = "Živojinović, Jelena and Peleš Tadić, Adriana and Kosanović, Darko and Tadić, Nenad and Vasiljević, Zorka Ž. and Lević, Steva and Obradović, Nina",
year = "2023",
abstract = "Iron-doped strontium-titanate (SrTiO3) powders with various iron(III) oxide (Fe2O3) weight percentages (1.5, 3 and 6 wt%) were prepared by a solid-state method in the presence of mechanical activation (10, 30 and 120 min). A systematic investigation by XRD, SEM and Raman spectroscopy has been undertaken to evaluate the role of dopant on the microstructural and morphological study of the perovskite oxide obtained. The optical properties of the different iron-doped and activated Fe-SrTiO3 powders have been also evaluated. The results demonstrated that Fe has been substituted into the lattice and surface layers of particles of SrTiO3 powders and the absorption edge shifted to higher wavelength values with increasing activation time and dopant weight percentage. The lowest value of the band gap (Eg=3.20 eV) was registered for the longest activation (120 min) and the highest weight percentage of dopant (6 wt%). Combining doping with mechanical activation, led to lower values of Eg and that fact could be used in subsequent studies to make Fe-SrTiO3 more suitable photocatalysts.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application XI New Frontiers in Multifunctional Material Science and Processing, Serbian Academy of Sciences and Art Serbia, Belgrade,18-20.September 2023",
title = "Influence of Fe Doping on the Crystal Structure and Optical Properties of Mechanically Activated SrTiO3 Powders",
pages = "51-51",
url = "https://hdl.handle.net/21.15107/rcub_dais_15007"
}
Živojinović, J., Peleš Tadić, A., Kosanović, D., Tadić, N., Vasiljević, Z. Ž., Lević, S.,& Obradović, N.. (2023). Influence of Fe Doping on the Crystal Structure and Optical Properties of Mechanically Activated SrTiO3 Powders. in Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application XI New Frontiers in Multifunctional Material Science and Processing, Serbian Academy of Sciences and Art Serbia, Belgrade,18-20.September 2023
Belgrade : Serbian Ceramic Society., 51-51.
https://hdl.handle.net/21.15107/rcub_dais_15007
Živojinović J, Peleš Tadić A, Kosanović D, Tadić N, Vasiljević ZŽ, Lević S, Obradović N. Influence of Fe Doping on the Crystal Structure and Optical Properties of Mechanically Activated SrTiO3 Powders. in Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application XI New Frontiers in Multifunctional Material Science and Processing, Serbian Academy of Sciences and Art Serbia, Belgrade,18-20.September 2023. 2023;:51-51.
https://hdl.handle.net/21.15107/rcub_dais_15007 .
Živojinović, Jelena, Peleš Tadić, Adriana, Kosanović, Darko, Tadić, Nenad, Vasiljević, Zorka Ž., Lević, Steva, Obradović, Nina, "Influence of Fe Doping on the Crystal Structure and Optical Properties of Mechanically Activated SrTiO3 Powders" in Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application XI New Frontiers in Multifunctional Material Science and Processing, Serbian Academy of Sciences and Art Serbia, Belgrade,18-20.September 2023 (2023):51-51,
https://hdl.handle.net/21.15107/rcub_dais_15007 .

Dielectric Properties of Mechanically Activated Strontium Titanate Ceramics

Živojinović, Jelena; Kosanović, Darko; Blagojević, Vladimir A.; Pavlović, Vera P.; Tadić, Nenad; Vlahović, Branislav; Pavlović, Vladimir B.

(2022)

TY  - JOUR
AU  - Živojinović, Jelena
AU  - Kosanović, Darko
AU  - Blagojević, Vladimir A.
AU  - Pavlović, Vera P.
AU  - Tadić, Nenad
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2022
UR  - https://dais.sanu.ac.rs/123456789/13510
AB  - In this study, microstructure evolution and dielectric properties of SrTiO3 ceramic have been investigated, whereby mechanical activation of SrTiO3 powders was used to modify the functional properties of ceramic materials. Microstructural SEM analysis of SrTiO3 ceramics showed that the increase in mechanical activation time results in less porous samples. Raman spectroscopy indicated changes in the broadening and asymmetry of the TO2 mode with a change in the time of mechanical activation. TO2 mode showed a Fano asymmetry due to its interaction with polarization fluctuations in polar micro-regions, which are a consequence of the presence of oxygen vacancies caused by activation. The maximum value of dielectric permittivity was observed in the sample activated for 10 min. Also, the sample activated for 10 min exhibits relatively low values of loss tangent, compared to the other mechanically activated samples, providing the best overall dielectric performance compared to other samples.
T2  - Science of Sintering
T1  - Dielectric Properties of Mechanically Activated Strontium Titanate Ceramics
SP  - 401
EP  - 414
VL  - 54
IS  - 4
DO  - 10.2298/SOS2204401Z
UR  - https://hdl.handle.net/21.15107/rcub_dais_13510
ER  - 
@article{
author = "Živojinović, Jelena and Kosanović, Darko and Blagojević, Vladimir A. and Pavlović, Vera P. and Tadić, Nenad and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2022",
abstract = "In this study, microstructure evolution and dielectric properties of SrTiO3 ceramic have been investigated, whereby mechanical activation of SrTiO3 powders was used to modify the functional properties of ceramic materials. Microstructural SEM analysis of SrTiO3 ceramics showed that the increase in mechanical activation time results in less porous samples. Raman spectroscopy indicated changes in the broadening and asymmetry of the TO2 mode with a change in the time of mechanical activation. TO2 mode showed a Fano asymmetry due to its interaction with polarization fluctuations in polar micro-regions, which are a consequence of the presence of oxygen vacancies caused by activation. The maximum value of dielectric permittivity was observed in the sample activated for 10 min. Also, the sample activated for 10 min exhibits relatively low values of loss tangent, compared to the other mechanically activated samples, providing the best overall dielectric performance compared to other samples.",
journal = "Science of Sintering",
title = "Dielectric Properties of Mechanically Activated Strontium Titanate Ceramics",
pages = "401-414",
volume = "54",
number = "4",
doi = "10.2298/SOS2204401Z",
url = "https://hdl.handle.net/21.15107/rcub_dais_13510"
}
Živojinović, J., Kosanović, D., Blagojević, V. A., Pavlović, V. P., Tadić, N., Vlahović, B.,& Pavlović, V. B.. (2022). Dielectric Properties of Mechanically Activated Strontium Titanate Ceramics. in Science of Sintering, 54(4), 401-414.
https://doi.org/10.2298/SOS2204401Z
https://hdl.handle.net/21.15107/rcub_dais_13510
Živojinović J, Kosanović D, Blagojević VA, Pavlović VP, Tadić N, Vlahović B, Pavlović VB. Dielectric Properties of Mechanically Activated Strontium Titanate Ceramics. in Science of Sintering. 2022;54(4):401-414.
doi:10.2298/SOS2204401Z
https://hdl.handle.net/21.15107/rcub_dais_13510 .
Živojinović, Jelena, Kosanović, Darko, Blagojević, Vladimir A., Pavlović, Vera P., Tadić, Nenad, Vlahović, Branislav, Pavlović, Vladimir B., "Dielectric Properties of Mechanically Activated Strontium Titanate Ceramics" in Science of Sintering, 54, no. 4 (2022):401-414,
https://doi.org/10.2298/SOS2204401Z .,
https://hdl.handle.net/21.15107/rcub_dais_13510 .
3

Study of influence of Mn dopant on dielectric response of SrTiO3 ceramics

Živojinović, Jelena; Kosanović, Darko; Pavlović, Vera P.; Tadić, Nenad; Pavlović, Vladimir B.

(Belgrade : Materials Research Society of Serbia, 2022)

TY  - CONF
AU  - Živojinović, Jelena
AU  - Kosanović, Darko
AU  - Pavlović, Vera P.
AU  - Tadić, Nenad
AU  - Pavlović, Vladimir B.
PY  - 2022
UR  - https://dais.sanu.ac.rs/123456789/13596
AB  - The influence of Mn incorporation into the Sr and Ti sites of SrTiO3 ceramics on the structure, microstructure and dielectric tunability was studied. Manganese doped SrTiO3 ceramics with various manganese dioxide weight percentages (1.5, 3 and 6 wt %) were prepared by a solid-state method in the presence of mechanical activation (10, 30 and 120 minutes). According to Ritveld's analysis it was found that the size of the crystallite in doped activated SrTiO3 ceramics is smaller than the size of the crystallite in undoped ceramics. This lower degree of crystallinity is a consequence of additional distortion of the crystal structure due to ion substitution. SEM analysis showed that with increasing dopant concentration in the sample, at the same time as a time of mechanical activation, the grain size decreases, which is explained by the increasingly dominant incorporation of Mn4+ ions at sites of Ti4+ ions. On the Raman spectra of doped ceramic samples, the appearance of a peak at 750 cm-1 was observed, its change in intensity with the increase of dopant concentration indicates the incorporation of dopant in the SrTiO3 lattice. It was stated that mechanical activation leads to a more pronounced increase in the intensity of the mentioned peak, i.e. that activation leads to effectively higher incorporation of dopant into the strontium-titanate lattice. Higher values of relative dielectric permittivity of doped SrTiO3 ceramics were observed for 1.5 wt %, in relation to inactivated and activated undoped ceramics. Based on all previous analysis, it is estimated that this can be related not only to higher sample densities but also to the contribution of Mn2+ ion incorporation at Sr2+ ion positions in the lattice. Based on all the above, the optimal electrical properties of SrTiO3 ceramics can be achieved by the appropriate choice of mechanical activation time and dopant concentration.
PB  - Belgrade : Materials Research Society of Serbia
C3  - Program and The Book of abstracts / Twenty-third Annual Conference YUCOMAT 2022 & Twelfth World Round Table Conference on Sintering XII WRTCS 2022, Herceg Novi, Montenegro, August 29 - September 2, 2022
T1  - Study of influence of Mn dopant on dielectric response of SrTiO3 ceramics
SP  - 131
EP  - 131
UR  - https://hdl.handle.net/21.15107/rcub_dais_13596
ER  - 
@conference{
author = "Živojinović, Jelena and Kosanović, Darko and Pavlović, Vera P. and Tadić, Nenad and Pavlović, Vladimir B.",
year = "2022",
abstract = "The influence of Mn incorporation into the Sr and Ti sites of SrTiO3 ceramics on the structure, microstructure and dielectric tunability was studied. Manganese doped SrTiO3 ceramics with various manganese dioxide weight percentages (1.5, 3 and 6 wt %) were prepared by a solid-state method in the presence of mechanical activation (10, 30 and 120 minutes). According to Ritveld's analysis it was found that the size of the crystallite in doped activated SrTiO3 ceramics is smaller than the size of the crystallite in undoped ceramics. This lower degree of crystallinity is a consequence of additional distortion of the crystal structure due to ion substitution. SEM analysis showed that with increasing dopant concentration in the sample, at the same time as a time of mechanical activation, the grain size decreases, which is explained by the increasingly dominant incorporation of Mn4+ ions at sites of Ti4+ ions. On the Raman spectra of doped ceramic samples, the appearance of a peak at 750 cm-1 was observed, its change in intensity with the increase of dopant concentration indicates the incorporation of dopant in the SrTiO3 lattice. It was stated that mechanical activation leads to a more pronounced increase in the intensity of the mentioned peak, i.e. that activation leads to effectively higher incorporation of dopant into the strontium-titanate lattice. Higher values of relative dielectric permittivity of doped SrTiO3 ceramics were observed for 1.5 wt %, in relation to inactivated and activated undoped ceramics. Based on all previous analysis, it is estimated that this can be related not only to higher sample densities but also to the contribution of Mn2+ ion incorporation at Sr2+ ion positions in the lattice. Based on all the above, the optimal electrical properties of SrTiO3 ceramics can be achieved by the appropriate choice of mechanical activation time and dopant concentration.",
publisher = "Belgrade : Materials Research Society of Serbia",
journal = "Program and The Book of abstracts / Twenty-third Annual Conference YUCOMAT 2022 & Twelfth World Round Table Conference on Sintering XII WRTCS 2022, Herceg Novi, Montenegro, August 29 - September 2, 2022",
title = "Study of influence of Mn dopant on dielectric response of SrTiO3 ceramics",
pages = "131-131",
url = "https://hdl.handle.net/21.15107/rcub_dais_13596"
}
Živojinović, J., Kosanović, D., Pavlović, V. P., Tadić, N.,& Pavlović, V. B.. (2022). Study of influence of Mn dopant on dielectric response of SrTiO3 ceramics. in Program and The Book of abstracts / Twenty-third Annual Conference YUCOMAT 2022 & Twelfth World Round Table Conference on Sintering XII WRTCS 2022, Herceg Novi, Montenegro, August 29 - September 2, 2022
Belgrade : Materials Research Society of Serbia., 131-131.
https://hdl.handle.net/21.15107/rcub_dais_13596
Živojinović J, Kosanović D, Pavlović VP, Tadić N, Pavlović VB. Study of influence of Mn dopant on dielectric response of SrTiO3 ceramics. in Program and The Book of abstracts / Twenty-third Annual Conference YUCOMAT 2022 & Twelfth World Round Table Conference on Sintering XII WRTCS 2022, Herceg Novi, Montenegro, August 29 - September 2, 2022. 2022;:131-131.
https://hdl.handle.net/21.15107/rcub_dais_13596 .
Živojinović, Jelena, Kosanović, Darko, Pavlović, Vera P., Tadić, Nenad, Pavlović, Vladimir B., "Study of influence of Mn dopant on dielectric response of SrTiO3 ceramics" in Program and The Book of abstracts / Twenty-third Annual Conference YUCOMAT 2022 & Twelfth World Round Table Conference on Sintering XII WRTCS 2022, Herceg Novi, Montenegro, August 29 - September 2, 2022 (2022):131-131,
https://hdl.handle.net/21.15107/rcub_dais_13596 .

Mixed Ni-Mg Spinel Ferrites Used as Materials for Charge Storage Electrodes

Dojčinović, Milena P.; Vasiljević, Zorka Ž.; Pavlović, Vera P.; Vujančević, Jelena; Tadić, Nenad; Nikolić, Maria Vesna

(Belgrade : University of Belgrade, Faculty of Physical Chemistry, 2022)

TY  - CONF
AU  - Dojčinović, Milena P.
AU  - Vasiljević, Zorka Ž.
AU  - Pavlović, Vera P.
AU  - Vujančević, Jelena
AU  - Tadić, Nenad
AU  - Nikolić, Maria Vesna
PY  - 2022
UR  - https://dais.sanu.ac.rs/123456789/13642
AB  - Problems that countries all over the world have in common are dependence of economy and energy production on fossil fuels. There is a growing need for energy production and storage routes that are safe for the environment, renewable, efficient and cheap. One of the directions in which science is moving forward is discovering materials suitable for use in batteries and supercapacitors to improve their operating potential, electrical capacity or biocompatibility. The objective is also to synthesize materials for batteries or supercapacitors that are cheap, consist of earth abundant elements and have high electrochemical activity.
In this work, mixed nickel-magnesium ferrites NixMg1−xFe2O4, with x being 0, 0.1, 0.3, 0.5, 0.7, 0.9 and 1, were synthesized via sol-gel combustion synthesis with citric acid used as fuel and nitrate ions used as oxidizing agents. Combusted powders were calcined at 700 °C. The structure and morphology of the powders were characterized with X-ray diffraction method (XRD), field emission scanning electron microscopy (FESEM), Raman and FTIR spectroscopy. The band gap was calculated by using UV/Vis diffuse reflectance spectroscopy (DRS). Samples were cast on nickel foam and tested as energy storage materials in a three-electrode setup in 3 M KOH aqueous solution as electrolyte. The methods used were cyclic voltammetry (CV) and constant current chronopotentiometry to obtain galvanostatic charge-discharge (GCD) curves. Results show that all of the synthesized materials show battery-type charge storage in alkaline electrolyte due to the formation of metal cation oxyhydroxides. With increasing nickel content, electrochemical activity drops. The highest value of capacity, 34.3 mA h g-1 at the current density of 500 mA g-1 is ascribed to magnesium ferrite, MgFe2O4.
PB  - Belgrade : University of Belgrade, Faculty of Physical Chemistry
C3  - Contemporary batteries and supercapacitors : COIN2022 : program and book of abstracts / International Symposium Belgrade, June 1-2, 2022
T1  - Mixed Ni-Mg Spinel Ferrites Used as Materials for Charge Storage Electrodes
SP  - 47
EP  - 47
UR  - https://hdl.handle.net/21.15107/rcub_dais_13642
ER  - 
@conference{
author = "Dojčinović, Milena P. and Vasiljević, Zorka Ž. and Pavlović, Vera P. and Vujančević, Jelena and Tadić, Nenad and Nikolić, Maria Vesna",
year = "2022",
abstract = "Problems that countries all over the world have in common are dependence of economy and energy production on fossil fuels. There is a growing need for energy production and storage routes that are safe for the environment, renewable, efficient and cheap. One of the directions in which science is moving forward is discovering materials suitable for use in batteries and supercapacitors to improve their operating potential, electrical capacity or biocompatibility. The objective is also to synthesize materials for batteries or supercapacitors that are cheap, consist of earth abundant elements and have high electrochemical activity.
In this work, mixed nickel-magnesium ferrites NixMg1−xFe2O4, with x being 0, 0.1, 0.3, 0.5, 0.7, 0.9 and 1, were synthesized via sol-gel combustion synthesis with citric acid used as fuel and nitrate ions used as oxidizing agents. Combusted powders were calcined at 700 °C. The structure and morphology of the powders were characterized with X-ray diffraction method (XRD), field emission scanning electron microscopy (FESEM), Raman and FTIR spectroscopy. The band gap was calculated by using UV/Vis diffuse reflectance spectroscopy (DRS). Samples were cast on nickel foam and tested as energy storage materials in a three-electrode setup in 3 M KOH aqueous solution as electrolyte. The methods used were cyclic voltammetry (CV) and constant current chronopotentiometry to obtain galvanostatic charge-discharge (GCD) curves. Results show that all of the synthesized materials show battery-type charge storage in alkaline electrolyte due to the formation of metal cation oxyhydroxides. With increasing nickel content, electrochemical activity drops. The highest value of capacity, 34.3 mA h g-1 at the current density of 500 mA g-1 is ascribed to magnesium ferrite, MgFe2O4.",
publisher = "Belgrade : University of Belgrade, Faculty of Physical Chemistry",
journal = "Contemporary batteries and supercapacitors : COIN2022 : program and book of abstracts / International Symposium Belgrade, June 1-2, 2022",
title = "Mixed Ni-Mg Spinel Ferrites Used as Materials for Charge Storage Electrodes",
pages = "47-47",
url = "https://hdl.handle.net/21.15107/rcub_dais_13642"
}
Dojčinović, M. P., Vasiljević, Z. Ž., Pavlović, V. P., Vujančević, J., Tadić, N.,& Nikolić, M. V.. (2022). Mixed Ni-Mg Spinel Ferrites Used as Materials for Charge Storage Electrodes. in Contemporary batteries and supercapacitors : COIN2022 : program and book of abstracts / International Symposium Belgrade, June 1-2, 2022
Belgrade : University of Belgrade, Faculty of Physical Chemistry., 47-47.
https://hdl.handle.net/21.15107/rcub_dais_13642
Dojčinović MP, Vasiljević ZŽ, Pavlović VP, Vujančević J, Tadić N, Nikolić MV. Mixed Ni-Mg Spinel Ferrites Used as Materials for Charge Storage Electrodes. in Contemporary batteries and supercapacitors : COIN2022 : program and book of abstracts / International Symposium Belgrade, June 1-2, 2022. 2022;:47-47.
https://hdl.handle.net/21.15107/rcub_dais_13642 .
Dojčinović, Milena P., Vasiljević, Zorka Ž., Pavlović, Vera P., Vujančević, Jelena, Tadić, Nenad, Nikolić, Maria Vesna, "Mixed Ni-Mg Spinel Ferrites Used as Materials for Charge Storage Electrodes" in Contemporary batteries and supercapacitors : COIN2022 : program and book of abstracts / International Symposium Belgrade, June 1-2, 2022 (2022):47-47,
https://hdl.handle.net/21.15107/rcub_dais_13642 .

Effect of high energy ball milling on sintering of MgO-TiO2 system

Filipović, Suzana; Obradović, Nina; Fahrenholtz, William G.; Smith, Steven; Mirković, M.; Peleš Tadić, Adriana; Tadić, Nenad; Đorđević, Antonije

(Belgrade : Serbian Ceramic Society, 2022)

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Fahrenholtz, William G.
AU  - Smith, Steven
AU  - Mirković, M.
AU  - Peleš Tadić, Adriana
AU  - Tadić, Nenad
AU  - Đorđević, Antonije
PY  - 2022
UR  - https://dais.sanu.ac.rs/123456789/13622
AB  - Perovskite ceramic material based on MgTiO3 is used in various types of electronic devices owing to its dielectric properties, high dielectric constant, and low losses. These features can be tailored by setting preparation conditions. Densification of magnesium titanate by Spark Plasma Sintering (SPS) was the aim of this work. First, the mechanical activation in the highenergy ball mill was applied on the powder of MgO-TiO2 mixed in mole ratio 1:1. Prepared powder mixtures, activated for different times, were SPS sintered, at 1200 oC with a heating rate of 100oC/min. After reaching the desired temperature, a uniaxial pressure of 50 MPa was applied, and dwelled at this condition for 5 min, followed by cooling to room temperature at 5oC/min. The starting powders, activated mixtures, and sintered ceramics bodies were investigated by X-ray diffraction, scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS). The presence of the MgTi2O5 phase was noticed for the nonmilled ceramics. In the samples obtained from milled powders, MgTi2O5 was detected in EDS spectra in a lower amount, below the threshold of the XRD method. Dielectric measurements were performed at a wide range of frequencies and temperatures. The highest value of the hardness was obtained from powder milled for 15 min before SPS.
PB  - Belgrade : Serbian Ceramic Society
C3  - Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application X New Frontiers in Multifunctional Material Science and Processing, Serbia, Belgrade, 26-27. September 2022.
T1  - Effect of high energy ball milling on sintering of MgO-TiO2 system
SP  - 88
EP  - 88
UR  - https://hdl.handle.net/21.15107/rcub_dais_13622
ER  - 
@conference{
author = "Filipović, Suzana and Obradović, Nina and Fahrenholtz, William G. and Smith, Steven and Mirković, M. and Peleš Tadić, Adriana and Tadić, Nenad and Đorđević, Antonije",
year = "2022",
abstract = "Perovskite ceramic material based on MgTiO3 is used in various types of electronic devices owing to its dielectric properties, high dielectric constant, and low losses. These features can be tailored by setting preparation conditions. Densification of magnesium titanate by Spark Plasma Sintering (SPS) was the aim of this work. First, the mechanical activation in the highenergy ball mill was applied on the powder of MgO-TiO2 mixed in mole ratio 1:1. Prepared powder mixtures, activated for different times, were SPS sintered, at 1200 oC with a heating rate of 100oC/min. After reaching the desired temperature, a uniaxial pressure of 50 MPa was applied, and dwelled at this condition for 5 min, followed by cooling to room temperature at 5oC/min. The starting powders, activated mixtures, and sintered ceramics bodies were investigated by X-ray diffraction, scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS). The presence of the MgTi2O5 phase was noticed for the nonmilled ceramics. In the samples obtained from milled powders, MgTi2O5 was detected in EDS spectra in a lower amount, below the threshold of the XRD method. Dielectric measurements were performed at a wide range of frequencies and temperatures. The highest value of the hardness was obtained from powder milled for 15 min before SPS.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application X New Frontiers in Multifunctional Material Science and Processing, Serbia, Belgrade, 26-27. September 2022.",
title = "Effect of high energy ball milling on sintering of MgO-TiO2 system",
pages = "88-88",
url = "https://hdl.handle.net/21.15107/rcub_dais_13622"
}
Filipović, S., Obradović, N., Fahrenholtz, W. G., Smith, S., Mirković, M., Peleš Tadić, A., Tadić, N.,& Đorđević, A.. (2022). Effect of high energy ball milling on sintering of MgO-TiO2 system. in Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application X New Frontiers in Multifunctional Material Science and Processing, Serbia, Belgrade, 26-27. September 2022.
Belgrade : Serbian Ceramic Society., 88-88.
https://hdl.handle.net/21.15107/rcub_dais_13622
Filipović S, Obradović N, Fahrenholtz WG, Smith S, Mirković M, Peleš Tadić A, Tadić N, Đorđević A. Effect of high energy ball milling on sintering of MgO-TiO2 system. in Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application X New Frontiers in Multifunctional Material Science and Processing, Serbia, Belgrade, 26-27. September 2022.. 2022;:88-88.
https://hdl.handle.net/21.15107/rcub_dais_13622 .
Filipović, Suzana, Obradović, Nina, Fahrenholtz, William G., Smith, Steven, Mirković, M., Peleš Tadić, Adriana, Tadić, Nenad, Đorđević, Antonije, "Effect of high energy ball milling on sintering of MgO-TiO2 system" in Program and the Book of abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application X New Frontiers in Multifunctional Material Science and Processing, Serbia, Belgrade, 26-27. September 2022. (2022):88-88,
https://hdl.handle.net/21.15107/rcub_dais_13622 .

Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application

Rizzotto, Francesco; Vasiljević, Zorka Ž.; Stanojević, Gordana; Dojčinović, Milena P.; Janković-Častvan, Ivona; Vujančević, Jelena; Tadić, Nenad B.; Branković, Goran; Magniez, Aurélie; Vidić, Jasmina; Nikolić, Maria Vesna

(Elsevier Ltd, 2022)

TY  - JOUR
AU  - Rizzotto, Francesco
AU  - Vasiljević, Zorka Ž.
AU  - Stanojević, Gordana
AU  - Dojčinović, Milena P.
AU  - Janković-Častvan, Ivona
AU  - Vujančević, Jelena
AU  - Tadić, Nenad B.
AU  - Branković, Goran
AU  - Magniez, Aurélie
AU  - Vidić, Jasmina
AU  - Nikolić, Maria Vesna
PY  - 2022
UR  - https://dais.sanu.ac.rs/123456789/13437
AB  - An emerging technology of active packaging enables prolongation of food shelf life by limiting the oxygen transfer and the reactivity of free radicals, which both destruct food freshness. In this work, Fe2TiO5 nanoparticles were synthesized using a modified sol–gel method and evaluated as an enforcement of alginate food packaging film. Pure phase Fe2TiO5 nanoparticles had an average particle size of 44 nm and rhombohedral morphology. Fe2TiO5 nanoparticles induce no cell damage of human Caco-2 epithelial cells and show no inhibitory effect towards growth of a panel of bacterial strains, suggesting good biocompatibility. Films obtained by incorporation of Fe2TiO5 nanoparticles into alginate using the solvent casting method show no migration of iron or titanium ions from films to food simulants again suggesting their safety as a packaging material. Fe2TiO5 nanoparticles also showed strong antioxidant efficiency as determined using the DPPḢ assay, and confirmed further in a preservation test on fresh fruit.
PB  - Elsevier Ltd
T2  - Food Chemistry
T1  - Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application
SP  - 133198
VL  - 390
DO  - 10.1016/j.foodchem.2022.133198
UR  - https://hdl.handle.net/21.15107/rcub_dais_13437
ER  - 
@article{
author = "Rizzotto, Francesco and Vasiljević, Zorka Ž. and Stanojević, Gordana and Dojčinović, Milena P. and Janković-Častvan, Ivona and Vujančević, Jelena and Tadić, Nenad B. and Branković, Goran and Magniez, Aurélie and Vidić, Jasmina and Nikolić, Maria Vesna",
year = "2022",
abstract = "An emerging technology of active packaging enables prolongation of food shelf life by limiting the oxygen transfer and the reactivity of free radicals, which both destruct food freshness. In this work, Fe2TiO5 nanoparticles were synthesized using a modified sol–gel method and evaluated as an enforcement of alginate food packaging film. Pure phase Fe2TiO5 nanoparticles had an average particle size of 44 nm and rhombohedral morphology. Fe2TiO5 nanoparticles induce no cell damage of human Caco-2 epithelial cells and show no inhibitory effect towards growth of a panel of bacterial strains, suggesting good biocompatibility. Films obtained by incorporation of Fe2TiO5 nanoparticles into alginate using the solvent casting method show no migration of iron or titanium ions from films to food simulants again suggesting their safety as a packaging material. Fe2TiO5 nanoparticles also showed strong antioxidant efficiency as determined using the DPPḢ assay, and confirmed further in a preservation test on fresh fruit.",
publisher = "Elsevier Ltd",
journal = "Food Chemistry",
title = "Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application",
pages = "133198",
volume = "390",
doi = "10.1016/j.foodchem.2022.133198",
url = "https://hdl.handle.net/21.15107/rcub_dais_13437"
}
Rizzotto, F., Vasiljević, Z. Ž., Stanojević, G., Dojčinović, M. P., Janković-Častvan, I., Vujančević, J., Tadić, N. B., Branković, G., Magniez, A., Vidić, J.,& Nikolić, M. V.. (2022). Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application. in Food Chemistry
Elsevier Ltd., 390, 133198.
https://doi.org/10.1016/j.foodchem.2022.133198
https://hdl.handle.net/21.15107/rcub_dais_13437
Rizzotto F, Vasiljević ZŽ, Stanojević G, Dojčinović MP, Janković-Častvan I, Vujančević J, Tadić NB, Branković G, Magniez A, Vidić J, Nikolić MV. Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application. in Food Chemistry. 2022;390:133198.
doi:10.1016/j.foodchem.2022.133198
https://hdl.handle.net/21.15107/rcub_dais_13437 .
Rizzotto, Francesco, Vasiljević, Zorka Ž., Stanojević, Gordana, Dojčinović, Milena P., Janković-Častvan, Ivona, Vujančević, Jelena, Tadić, Nenad B., Branković, Goran, Magniez, Aurélie, Vidić, Jasmina, Nikolić, Maria Vesna, "Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application" in Food Chemistry, 390 (2022):133198,
https://doi.org/10.1016/j.foodchem.2022.133198 .,
https://hdl.handle.net/21.15107/rcub_dais_13437 .
10
9

Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application

Rizzotto, Francesco; Vasiljević, Zorka Ž.; Stanojević, Gordana; Dojčinović, Milena P.; Janković-Častvan, Ivona; Vujančević, Jelena; Tadić, Nenad B.; Branković, Goran; Magniez, Aurélie; Vidić, Jasmina; Nikolić, Maria Vesna

(Elsevier Ltd, 2022)

TY  - JOUR
AU  - Rizzotto, Francesco
AU  - Vasiljević, Zorka Ž.
AU  - Stanojević, Gordana
AU  - Dojčinović, Milena P.
AU  - Janković-Častvan, Ivona
AU  - Vujančević, Jelena
AU  - Tadić, Nenad B.
AU  - Branković, Goran
AU  - Magniez, Aurélie
AU  - Vidić, Jasmina
AU  - Nikolić, Maria Vesna
PY  - 2022
UR  - https://dais.sanu.ac.rs/123456789/13014
AB  - An emerging technology of active packaging enables prolongation of food shelf life by limiting the oxygen transfer and the reactivity of free radicals, which both destruct food freshness. In this work, Fe2TiO5 nanoparticles were synthesized using a modified sol–gel method and evaluated as an enforcement of alginate food packaging film. Pure phase Fe2TiO5 nanoparticles had an average particle size of 44 nm and rhombohedral morphology. Fe2TiO5 nanoparticles induce no cell damage of human Caco-2 epithelial cells and show no inhibitory effect towards growth of a panel of bacterial strains, suggesting good biocompatibility. Films obtained by incorporation of Fe2TiO5 nanoparticles into alginate using the solvent casting method show no migration of iron or titanium ions from films to food simulants again suggesting their safety as a packaging material. Fe2TiO5 nanoparticles also showed strong antioxidant efficiency as determined using the DPPḢ assay, and confirmed further in a preservation test on fresh fruit.
PB  - Elsevier Ltd
T2  - Food Chemistry
T1  - Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application
SP  - 133198
VL  - 390
DO  - 10.1016/j.foodchem.2022.133198
UR  - https://hdl.handle.net/21.15107/rcub_dais_13014
ER  - 
@article{
author = "Rizzotto, Francesco and Vasiljević, Zorka Ž. and Stanojević, Gordana and Dojčinović, Milena P. and Janković-Častvan, Ivona and Vujančević, Jelena and Tadić, Nenad B. and Branković, Goran and Magniez, Aurélie and Vidić, Jasmina and Nikolić, Maria Vesna",
year = "2022",
abstract = "An emerging technology of active packaging enables prolongation of food shelf life by limiting the oxygen transfer and the reactivity of free radicals, which both destruct food freshness. In this work, Fe2TiO5 nanoparticles were synthesized using a modified sol–gel method and evaluated as an enforcement of alginate food packaging film. Pure phase Fe2TiO5 nanoparticles had an average particle size of 44 nm and rhombohedral morphology. Fe2TiO5 nanoparticles induce no cell damage of human Caco-2 epithelial cells and show no inhibitory effect towards growth of a panel of bacterial strains, suggesting good biocompatibility. Films obtained by incorporation of Fe2TiO5 nanoparticles into alginate using the solvent casting method show no migration of iron or titanium ions from films to food simulants again suggesting their safety as a packaging material. Fe2TiO5 nanoparticles also showed strong antioxidant efficiency as determined using the DPPḢ assay, and confirmed further in a preservation test on fresh fruit.",
publisher = "Elsevier Ltd",
journal = "Food Chemistry",
title = "Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application",
pages = "133198",
volume = "390",
doi = "10.1016/j.foodchem.2022.133198",
url = "https://hdl.handle.net/21.15107/rcub_dais_13014"
}
Rizzotto, F., Vasiljević, Z. Ž., Stanojević, G., Dojčinović, M. P., Janković-Častvan, I., Vujančević, J., Tadić, N. B., Branković, G., Magniez, A., Vidić, J.,& Nikolić, M. V.. (2022). Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application. in Food Chemistry
Elsevier Ltd., 390, 133198.
https://doi.org/10.1016/j.foodchem.2022.133198
https://hdl.handle.net/21.15107/rcub_dais_13014
Rizzotto F, Vasiljević ZŽ, Stanojević G, Dojčinović MP, Janković-Častvan I, Vujančević J, Tadić NB, Branković G, Magniez A, Vidić J, Nikolić MV. Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application. in Food Chemistry. 2022;390:133198.
doi:10.1016/j.foodchem.2022.133198
https://hdl.handle.net/21.15107/rcub_dais_13014 .
Rizzotto, Francesco, Vasiljević, Zorka Ž., Stanojević, Gordana, Dojčinović, Milena P., Janković-Častvan, Ivona, Vujančević, Jelena, Tadić, Nenad B., Branković, Goran, Magniez, Aurélie, Vidić, Jasmina, Nikolić, Maria Vesna, "Antioxidant and cell-friendly Fe2TiO5 nanoparticles for food packaging application" in Food Chemistry, 390 (2022):133198,
https://doi.org/10.1016/j.foodchem.2022.133198 .,
https://hdl.handle.net/21.15107/rcub_dais_13014 .
10
9

Influence of calcination temperature on the structure, morphology and optical properties of electrospun pseudobrookite nanofibers

Vasiljević, Zorka Ž.; Dojčinović, Milena P.; Vujančević, Jelena; Spreitzer, Matjaž; Kovač, Janez; Janković-Čaštvan, Ivona; Bartolić, Dragana; Marković, Smilja; Tadić, Nenad; Nikolić, Maria Vesna

(Novi Sad : Faculty of Technology, 2021)

TY  - CONF
AU  - Vasiljević, Zorka Ž.
AU  - Dojčinović, Milena P.
AU  - Vujančević, Jelena
AU  - Spreitzer, Matjaž
AU  - Kovač, Janez
AU  - Janković-Čaštvan, Ivona
AU  - Bartolić, Dragana
AU  - Marković, Smilja
AU  - Tadić, Nenad
AU  - Nikolić, Maria Vesna
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/15358
AB  - Novel crystalline iron-titanate fibers were synthesized for the first time to the best of our knowledge, through a simple, low cost electrospinning method followed by calcination treatment at different temperatures (500–750 °C for 3 h and at 500 °C for 6 h and at 550 °C for 4 h). The fibers were prepared from a precursor solution containing polyvinylpyrrolidone (PVP), iron(III) nonahydrate, titanium isopropoxide, N,N-Dimethylformamide and ethanol. As spun fibers were smooth, straight, beadless and uniform forming a nonwoven fibrous mat, with an average diameter of ca. 205 nm. Upon calcination in air the PVP matrice was removed and XRD and FTIR analysis showed that the duration of the calcination process, besides the temperature, had a direct influence on phase formation. Pure phase of pseudobrookite was obtained at 600 °C, 500 °C for 6 h and at 550 °C for 4 h. In addition, the morphology of obtained nanofibers was directly affected by the calcination temperature. The surface of fibers obtained after calcination was no longer smooth and the fiber diameter decreased due to complete degradation of PVP. At 700 oC and 750 °C, fibers were thicker which can be attributed to growth of Fe2TiO5 nanoparticles and simultaneous coalescence of small particles. All samples exhibited a type IV nitrogen adsorption isotherm with a type- H3 indicating slit-shaped mesoporous structure. The BET surface areas of 500 °C for 6 h, 550 °C for 4 h and 600 °C for 3 h were estimated to be 62, 38.7 and 33.2 m2/g, respectively.
PB  - Novi Sad : Faculty of Technology
C3  - Programme and book of abstracts / 14th ECerS Conference for Young Scientists in Ceramics (CYSC-2021), October 20-23, 2021, Novi Sad, 2021
T1  - Influence of calcination temperature on the structure, morphology and optical properties of electrospun pseudobrookite nanofibers
SP  - 124
EP  - 124
UR  - https://hdl.handle.net/21.15107/rcub_dais_15358
ER  - 
@conference{
author = "Vasiljević, Zorka Ž. and Dojčinović, Milena P. and Vujančević, Jelena and Spreitzer, Matjaž and Kovač, Janez and Janković-Čaštvan, Ivona and Bartolić, Dragana and Marković, Smilja and Tadić, Nenad and Nikolić, Maria Vesna",
year = "2021",
abstract = "Novel crystalline iron-titanate fibers were synthesized for the first time to the best of our knowledge, through a simple, low cost electrospinning method followed by calcination treatment at different temperatures (500–750 °C for 3 h and at 500 °C for 6 h and at 550 °C for 4 h). The fibers were prepared from a precursor solution containing polyvinylpyrrolidone (PVP), iron(III) nonahydrate, titanium isopropoxide, N,N-Dimethylformamide and ethanol. As spun fibers were smooth, straight, beadless and uniform forming a nonwoven fibrous mat, with an average diameter of ca. 205 nm. Upon calcination in air the PVP matrice was removed and XRD and FTIR analysis showed that the duration of the calcination process, besides the temperature, had a direct influence on phase formation. Pure phase of pseudobrookite was obtained at 600 °C, 500 °C for 6 h and at 550 °C for 4 h. In addition, the morphology of obtained nanofibers was directly affected by the calcination temperature. The surface of fibers obtained after calcination was no longer smooth and the fiber diameter decreased due to complete degradation of PVP. At 700 oC and 750 °C, fibers were thicker which can be attributed to growth of Fe2TiO5 nanoparticles and simultaneous coalescence of small particles. All samples exhibited a type IV nitrogen adsorption isotherm with a type- H3 indicating slit-shaped mesoporous structure. The BET surface areas of 500 °C for 6 h, 550 °C for 4 h and 600 °C for 3 h were estimated to be 62, 38.7 and 33.2 m2/g, respectively.",
publisher = "Novi Sad : Faculty of Technology",
journal = "Programme and book of abstracts / 14th ECerS Conference for Young Scientists in Ceramics (CYSC-2021), October 20-23, 2021, Novi Sad, 2021",
title = "Influence of calcination temperature on the structure, morphology and optical properties of electrospun pseudobrookite nanofibers",
pages = "124-124",
url = "https://hdl.handle.net/21.15107/rcub_dais_15358"
}
Vasiljević, Z. Ž., Dojčinović, M. P., Vujančević, J., Spreitzer, M., Kovač, J., Janković-Čaštvan, I., Bartolić, D., Marković, S., Tadić, N.,& Nikolić, M. V.. (2021). Influence of calcination temperature on the structure, morphology and optical properties of electrospun pseudobrookite nanofibers. in Programme and book of abstracts / 14th ECerS Conference for Young Scientists in Ceramics (CYSC-2021), October 20-23, 2021, Novi Sad, 2021
Novi Sad : Faculty of Technology., 124-124.
https://hdl.handle.net/21.15107/rcub_dais_15358
Vasiljević ZŽ, Dojčinović MP, Vujančević J, Spreitzer M, Kovač J, Janković-Čaštvan I, Bartolić D, Marković S, Tadić N, Nikolić MV. Influence of calcination temperature on the structure, morphology and optical properties of electrospun pseudobrookite nanofibers. in Programme and book of abstracts / 14th ECerS Conference for Young Scientists in Ceramics (CYSC-2021), October 20-23, 2021, Novi Sad, 2021. 2021;:124-124.
https://hdl.handle.net/21.15107/rcub_dais_15358 .
Vasiljević, Zorka Ž., Dojčinović, Milena P., Vujančević, Jelena, Spreitzer, Matjaž, Kovač, Janez, Janković-Čaštvan, Ivona, Bartolić, Dragana, Marković, Smilja, Tadić, Nenad, Nikolić, Maria Vesna, "Influence of calcination temperature on the structure, morphology and optical properties of electrospun pseudobrookite nanofibers" in Programme and book of abstracts / 14th ECerS Conference for Young Scientists in Ceramics (CYSC-2021), October 20-23, 2021, Novi Sad, 2021 (2021):124-124,
https://hdl.handle.net/21.15107/rcub_dais_15358 .

The influence of mechanical activation on microstructure and dielectric properties of SrTiO3 ceramics

Živojinović, Jelena; Blagojević, Vladimir A.; Pavlović, Vera P.; Kosanović, Darko; Tadić, Nenad B.; Pavlović, Vladimir B.

(Belgrade : Innovation Center of Faculty of Mechanical Engineering, 2021)

TY  - CONF
AU  - Živojinović, Jelena
AU  - Blagojević, Vladimir A.
AU  - Pavlović, Vera P.
AU  - Kosanović, Darko
AU  - Tadić, Nenad B.
AU  - Pavlović, Vladimir B.
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/12349
AB  - In recent years, a lot of interest has been shown in obtaining materials with predetermined properties. The aim is to establish a functional dependence between the synthesis parameters, structural characteristics, and properties of the material. Ceramic materials based on strontium titanate (SrTiO3) are of special interest due to their unique physical-chemical properties. Having in mind the importance of examining the influence of synthesis parameters on the process of obtaining and properties of functional electroceramic materials, and the importance of SrTiO3 as a perovskite material, the motive was to analyze and consider the influence of mechanical activation. It has been established that the time of mechanical activation (0, 10, 30, 60, 90, and 120 minutes) of SrTiO3 powders indirectly affects on electrical properties of SrTiO3 ceramics. It was noticed that in SrTiO3 ceramics the values of relative dielectric permittivity in the radio frequency range (0,3 MHz-3 GHz) are stable, which is important for the fabrication of electronic components. Microstructural SEM analysis showed that the increase in mechanical activation time results in less porous samples. It was found that the value of the relative dielectric permittivity of ceramic samples at room temperature changes following the combined effect of changes in sample density, grain size, as well as changes in the grain boundary region. The maximum value of dielectric permittivity was observed in the sample activated for 10 minutes. Also, the sample activated for 10 min exhibits relatively low values of loss tangent, compared to the other mechanically activated samples, providing the best overall dielectric performance compared to other samples.
PB  - Belgrade : Innovation Center of Faculty of Mechanical Engineering
C3  - Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia
T1  - The influence of mechanical activation on microstructure and dielectric properties of SrTiO3 ceramics
SP  - 80
EP  - 80
UR  - https://hdl.handle.net/21.15107/rcub_dais_12349
ER  - 
@conference{
author = "Živojinović, Jelena and Blagojević, Vladimir A. and Pavlović, Vera P. and Kosanović, Darko and Tadić, Nenad B. and Pavlović, Vladimir B.",
year = "2021",
abstract = "In recent years, a lot of interest has been shown in obtaining materials with predetermined properties. The aim is to establish a functional dependence between the synthesis parameters, structural characteristics, and properties of the material. Ceramic materials based on strontium titanate (SrTiO3) are of special interest due to their unique physical-chemical properties. Having in mind the importance of examining the influence of synthesis parameters on the process of obtaining and properties of functional electroceramic materials, and the importance of SrTiO3 as a perovskite material, the motive was to analyze and consider the influence of mechanical activation. It has been established that the time of mechanical activation (0, 10, 30, 60, 90, and 120 minutes) of SrTiO3 powders indirectly affects on electrical properties of SrTiO3 ceramics. It was noticed that in SrTiO3 ceramics the values of relative dielectric permittivity in the radio frequency range (0,3 MHz-3 GHz) are stable, which is important for the fabrication of electronic components. Microstructural SEM analysis showed that the increase in mechanical activation time results in less porous samples. It was found that the value of the relative dielectric permittivity of ceramic samples at room temperature changes following the combined effect of changes in sample density, grain size, as well as changes in the grain boundary region. The maximum value of dielectric permittivity was observed in the sample activated for 10 minutes. Also, the sample activated for 10 min exhibits relatively low values of loss tangent, compared to the other mechanically activated samples, providing the best overall dielectric performance compared to other samples.",
publisher = "Belgrade : Innovation Center of Faculty of Mechanical Engineering",
journal = "Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia",
title = "The influence of mechanical activation on microstructure and dielectric properties of SrTiO3 ceramics",
pages = "80-80",
url = "https://hdl.handle.net/21.15107/rcub_dais_12349"
}
Živojinović, J., Blagojević, V. A., Pavlović, V. P., Kosanović, D., Tadić, N. B.,& Pavlović, V. B.. (2021). The influence of mechanical activation on microstructure and dielectric properties of SrTiO3 ceramics. in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia
Belgrade : Innovation Center of Faculty of Mechanical Engineering., 80-80.
https://hdl.handle.net/21.15107/rcub_dais_12349
Živojinović J, Blagojević VA, Pavlović VP, Kosanović D, Tadić NB, Pavlović VB. The influence of mechanical activation on microstructure and dielectric properties of SrTiO3 ceramics. in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia. 2021;:80-80.
https://hdl.handle.net/21.15107/rcub_dais_12349 .
Živojinović, Jelena, Blagojević, Vladimir A., Pavlović, Vera P., Kosanović, Darko, Tadić, Nenad B., Pavlović, Vladimir B., "The influence of mechanical activation on microstructure and dielectric properties of SrTiO3 ceramics" in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia (2021):80-80,
https://hdl.handle.net/21.15107/rcub_dais_12349 .

Nanocrystalline Zn2SnO4/SnO2: Crystal structure and humidity influence on complex impedance

Nikolić, Maria Vesna; Labus, Nebojša; Pavlović, Vera P.; Marković, Smilja; Luković, Miloljub D.; Tadić, Nenad B.; Vujančević, Jelena; Vlahović, Branislav; Pavlović, Vladimir B.

(Springer, 2021)

TY  - JOUR
AU  - Nikolić, Maria Vesna
AU  - Labus, Nebojša
AU  - Pavlović, Vera P.
AU  - Marković, Smilja
AU  - Luković, Miloljub D.
AU  - Tadić, Nenad B.
AU  - Vujančević, Jelena
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/11954
AB  - Nanocrystalline Zn2SnO4/SnO2 powder was obtained by a solid state reaction of ZnO and SnO2 nanopowders mixed in the molar ratio 1:1. The phase composition of the obtained powder was studied by XRD and Raman spectroscopy, morphology and texture were characterized by FESEM, TEM, BET and Hg porosimetry, while XPS and FTIR spectroscopy were used to determine the surface chemistry. The influence of humidity on complex impedance was monitored on bulk samples in the relative humidity (RH) range 30–90% in a climatic chamber in the frequency range 42 Hz- 1 MHz at working temperatures of 25 and 50 °C. Change in RH had a significant influence on impedance reduction, especially noticeable in the lower frequency range, indicating potential application of this nanocomposite as a humidity sensing material. Increase in RH led to an increase in AC conductivity that changed with frequency according to the Jonscher power law. The frequency exponent decreased with increase in RH and sample temperature indicating that the correlated hopping barrier model is the dominant conduction mechanism. Complex impedance was analyzed using an equivalent circuit consisting of a parallel resistance and constant phase element, showing the dominant influence of grain boundaries at both working temperatures (25 and 50 °C). The resistance decreased, while the capacitance and relaxation frequency increased with increase in RH. At high humidity an added Wartburg element enabled modeling of the charge diffusion process
PB  - Springer
T2  - Journal of Electroceramics
T1  - Nanocrystalline Zn2SnO4/SnO2: Crystal structure and humidity influence on complex impedance
SP  - 135
EP  - 147
VL  - 45
DO  - 10.1007/s10832-021-00232-z
UR  - https://hdl.handle.net/21.15107/rcub_dais_11954
ER  - 
@article{
author = "Nikolić, Maria Vesna and Labus, Nebojša and Pavlović, Vera P. and Marković, Smilja and Luković, Miloljub D. and Tadić, Nenad B. and Vujančević, Jelena and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2021",
abstract = "Nanocrystalline Zn2SnO4/SnO2 powder was obtained by a solid state reaction of ZnO and SnO2 nanopowders mixed in the molar ratio 1:1. The phase composition of the obtained powder was studied by XRD and Raman spectroscopy, morphology and texture were characterized by FESEM, TEM, BET and Hg porosimetry, while XPS and FTIR spectroscopy were used to determine the surface chemistry. The influence of humidity on complex impedance was monitored on bulk samples in the relative humidity (RH) range 30–90% in a climatic chamber in the frequency range 42 Hz- 1 MHz at working temperatures of 25 and 50 °C. Change in RH had a significant influence on impedance reduction, especially noticeable in the lower frequency range, indicating potential application of this nanocomposite as a humidity sensing material. Increase in RH led to an increase in AC conductivity that changed with frequency according to the Jonscher power law. The frequency exponent decreased with increase in RH and sample temperature indicating that the correlated hopping barrier model is the dominant conduction mechanism. Complex impedance was analyzed using an equivalent circuit consisting of a parallel resistance and constant phase element, showing the dominant influence of grain boundaries at both working temperatures (25 and 50 °C). The resistance decreased, while the capacitance and relaxation frequency increased with increase in RH. At high humidity an added Wartburg element enabled modeling of the charge diffusion process",
publisher = "Springer",
journal = "Journal of Electroceramics",
title = "Nanocrystalline Zn2SnO4/SnO2: Crystal structure and humidity influence on complex impedance",
pages = "135-147",
volume = "45",
doi = "10.1007/s10832-021-00232-z",
url = "https://hdl.handle.net/21.15107/rcub_dais_11954"
}
Nikolić, M. V., Labus, N., Pavlović, V. P., Marković, S., Luković, M. D., Tadić, N. B., Vujančević, J., Vlahović, B.,& Pavlović, V. B.. (2021). Nanocrystalline Zn2SnO4/SnO2: Crystal structure and humidity influence on complex impedance. in Journal of Electroceramics
Springer., 45, 135-147.
https://doi.org/10.1007/s10832-021-00232-z
https://hdl.handle.net/21.15107/rcub_dais_11954
Nikolić MV, Labus N, Pavlović VP, Marković S, Luković MD, Tadić NB, Vujančević J, Vlahović B, Pavlović VB. Nanocrystalline Zn2SnO4/SnO2: Crystal structure and humidity influence on complex impedance. in Journal of Electroceramics. 2021;45:135-147.
doi:10.1007/s10832-021-00232-z
https://hdl.handle.net/21.15107/rcub_dais_11954 .
Nikolić, Maria Vesna, Labus, Nebojša, Pavlović, Vera P., Marković, Smilja, Luković, Miloljub D., Tadić, Nenad B., Vujančević, Jelena, Vlahović, Branislav, Pavlović, Vladimir B., "Nanocrystalline Zn2SnO4/SnO2: Crystal structure and humidity influence on complex impedance" in Journal of Electroceramics, 45 (2021):135-147,
https://doi.org/10.1007/s10832-021-00232-z .,
https://hdl.handle.net/21.15107/rcub_dais_11954 .
4
4

Electrospun Nickel Manganite (NiMn2O4) Nanocrystalline Fibers for Humidity and Temperature Sensing

Dojčinović, Milena P.; Vasiljević, Zorka Ž.; Krstić, Jugoslav B.; Vujančević, Jelena D.; Marković, Smilja; Tadić, Nenad B.; Nikolic, Maria Vesna

(Basel : MDPI AG, 2021)

TY  - JOUR
AU  - Dojčinović, Milena P.
AU  - Vasiljević, Zorka Ž.
AU  - Krstić, Jugoslav B.
AU  - Vujančević, Jelena D.
AU  - Marković, Smilja
AU  - Tadić, Nenad B.
AU  - Nikolic, Maria Vesna
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/11797
AB  - Nickel manganite nanocrystalline fibers were obtained by electrospinning and subsequent calcination at 400 °C. As-spun fibers were characterized by TG/DTA, Scanning Electron Microscopy and FT-IR spectroscopy analysis. X-ray diffraction and FT-IR spectroscopy analysis confirmed the formation of nickel manganite with a cubic spinel structure, while N2 physisorption at 77 K enabled determination of the BET specific surface area as 25.3 m2/g and (BJH) mesopore volume as 21.5 m2/g. The material constant (B) of the nanocrystalline nickel manganite fibers applied by drop-casting on test interdigitated electrodes on alumina substrate, dried at room temperature, was determined as 4379 K in the 20–50 °C temperature range and a temperature sensitivity of −4.95%/K at room temperature (25 °C). The change of impedance with relative humidity was monitored at 25 and 50 °C for a relative humidity (RH) change of 40 to 90% in the 42 Hzπ1 MHz frequency range. At 100 Hz and 25 °C, the sensitivity of 327.36 ± 80.12 kΩ/%RH was determined, showing that nickel manganite obtained by electrospinning has potential as a multifunctional material for combined humidity and temperature sensing.
PB  - Basel : MDPI AG
T2  - Sensors
T1  - Electrospun Nickel Manganite (NiMn2O4) Nanocrystalline Fibers for Humidity and Temperature Sensing
SP  - 4357
VL  - 21
IS  - 13
DO  - 10.3390/s21134357
UR  - https://hdl.handle.net/21.15107/rcub_dais_11797
ER  - 
@article{
author = "Dojčinović, Milena P. and Vasiljević, Zorka Ž. and Krstić, Jugoslav B. and Vujančević, Jelena D. and Marković, Smilja and Tadić, Nenad B. and Nikolic, Maria Vesna",
year = "2021",
abstract = "Nickel manganite nanocrystalline fibers were obtained by electrospinning and subsequent calcination at 400 °C. As-spun fibers were characterized by TG/DTA, Scanning Electron Microscopy and FT-IR spectroscopy analysis. X-ray diffraction and FT-IR spectroscopy analysis confirmed the formation of nickel manganite with a cubic spinel structure, while N2 physisorption at 77 K enabled determination of the BET specific surface area as 25.3 m2/g and (BJH) mesopore volume as 21.5 m2/g. The material constant (B) of the nanocrystalline nickel manganite fibers applied by drop-casting on test interdigitated electrodes on alumina substrate, dried at room temperature, was determined as 4379 K in the 20–50 °C temperature range and a temperature sensitivity of −4.95%/K at room temperature (25 °C). The change of impedance with relative humidity was monitored at 25 and 50 °C for a relative humidity (RH) change of 40 to 90% in the 42 Hzπ1 MHz frequency range. At 100 Hz and 25 °C, the sensitivity of 327.36 ± 80.12 kΩ/%RH was determined, showing that nickel manganite obtained by electrospinning has potential as a multifunctional material for combined humidity and temperature sensing.",
publisher = "Basel : MDPI AG",
journal = "Sensors",
title = "Electrospun Nickel Manganite (NiMn2O4) Nanocrystalline Fibers for Humidity and Temperature Sensing",
pages = "4357",
volume = "21",
number = "13",
doi = "10.3390/s21134357",
url = "https://hdl.handle.net/21.15107/rcub_dais_11797"
}
Dojčinović, M. P., Vasiljević, Z. Ž., Krstić, J. B., Vujančević, J. D., Marković, S., Tadić, N. B.,& Nikolic, M. V.. (2021). Electrospun Nickel Manganite (NiMn2O4) Nanocrystalline Fibers for Humidity and Temperature Sensing. in Sensors
Basel : MDPI AG., 21(13), 4357.
https://doi.org/10.3390/s21134357
https://hdl.handle.net/21.15107/rcub_dais_11797
Dojčinović MP, Vasiljević ZŽ, Krstić JB, Vujančević JD, Marković S, Tadić NB, Nikolic MV. Electrospun Nickel Manganite (NiMn2O4) Nanocrystalline Fibers for Humidity and Temperature Sensing. in Sensors. 2021;21(13):4357.
doi:10.3390/s21134357
https://hdl.handle.net/21.15107/rcub_dais_11797 .
Dojčinović, Milena P., Vasiljević, Zorka Ž., Krstić, Jugoslav B., Vujančević, Jelena D., Marković, Smilja, Tadić, Nenad B., Nikolic, Maria Vesna, "Electrospun Nickel Manganite (NiMn2O4) Nanocrystalline Fibers for Humidity and Temperature Sensing" in Sensors, 21, no. 13 (2021):4357,
https://doi.org/10.3390/s21134357 .,
https://hdl.handle.net/21.15107/rcub_dais_11797 .
9
1
8

Exploring the impact of calcination parameters on the crystal structure, morphology, and optical properties of electrospun Fe 2 TiO 5 nanofibers

Vasiljević, Zorka Ž.; Dojčinović, Milena P.; Vujančević, Jelena D.; Spreitzer, Matjaž; Kovač, Janez; Bartolić, Dragana; Marković, Smilja; Janković-Čaštvan, Ivona; Tadić, Nenad B.; Nikolić, Maria Vesna

(Royal Society of Chemistry (RSC), 2021)

TY  - JOUR
AU  - Vasiljević, Zorka Ž.
AU  - Dojčinović, Milena P.
AU  - Vujančević, Jelena D.
AU  - Spreitzer, Matjaž
AU  - Kovač, Janez
AU  - Bartolić, Dragana
AU  - Marković, Smilja
AU  - Janković-Čaštvan, Ivona
AU  - Tadić, Nenad B.
AU  - Nikolić, Maria Vesna
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/12338
AB  - Nanostructured Fe2TiO5 (pseudobrookite), a mixed metal oxide material holds significant promise for utilization in energy and environmental applications. However, its full application is still hindered due to the difficulty to synthesize monophasic Fe2TiO5 with high crystallinity and a large specific surface area. Herein, Fe2TiO5 nanofibers were synthesized via a versatile and low-cost electrospinning method, followed by a calcination process at different temperatures. We found a significant effect of the calcination process and its duration on the crystalline phase in the form of either pseudobrookite or pseudobrookite–hematite–rutile and the morphology of calcined nanofibers. The crystallite size increased whereas the specific surface area decreased with an increase in calcination temperature. At higher temperatures, the growth of Fe2TiO5 nanoparticles and simultaneous coalescence of small particles was noted. The highest specific surface area was obtained for the sample calcined at 500 °C for 6 h (SBET = 64.4 m2 g−1). This work opens new opportunities in the synthesis of Fe2TiO5 nanostructures using the electrospinning method and a subsequent optimized calcination process for energy-related applications.
PB  - Royal Society of Chemistry (RSC)
T2  - RSC Advances
T1  - Exploring the impact of calcination parameters on the crystal structure, morphology, and optical properties of electrospun Fe                    2                    TiO                    5                    nanofibers
SP  - 32358
EP  - 32368
VL  - 11
IS  - 51
DO  - 10.1039/D1RA05748K
UR  - https://hdl.handle.net/21.15107/rcub_dais_12338
ER  - 
@article{
author = "Vasiljević, Zorka Ž. and Dojčinović, Milena P. and Vujančević, Jelena D. and Spreitzer, Matjaž and Kovač, Janez and Bartolić, Dragana and Marković, Smilja and Janković-Čaštvan, Ivona and Tadić, Nenad B. and Nikolić, Maria Vesna",
year = "2021",
abstract = "Nanostructured Fe2TiO5 (pseudobrookite), a mixed metal oxide material holds significant promise for utilization in energy and environmental applications. However, its full application is still hindered due to the difficulty to synthesize monophasic Fe2TiO5 with high crystallinity and a large specific surface area. Herein, Fe2TiO5 nanofibers were synthesized via a versatile and low-cost electrospinning method, followed by a calcination process at different temperatures. We found a significant effect of the calcination process and its duration on the crystalline phase in the form of either pseudobrookite or pseudobrookite–hematite–rutile and the morphology of calcined nanofibers. The crystallite size increased whereas the specific surface area decreased with an increase in calcination temperature. At higher temperatures, the growth of Fe2TiO5 nanoparticles and simultaneous coalescence of small particles was noted. The highest specific surface area was obtained for the sample calcined at 500 °C for 6 h (SBET = 64.4 m2 g−1). This work opens new opportunities in the synthesis of Fe2TiO5 nanostructures using the electrospinning method and a subsequent optimized calcination process for energy-related applications.",
publisher = "Royal Society of Chemistry (RSC)",
journal = "RSC Advances",
title = "Exploring the impact of calcination parameters on the crystal structure, morphology, and optical properties of electrospun Fe                    2                    TiO                    5                    nanofibers",
pages = "32358-32368",
volume = "11",
number = "51",
doi = "10.1039/D1RA05748K",
url = "https://hdl.handle.net/21.15107/rcub_dais_12338"
}
Vasiljević, Z. Ž., Dojčinović, M. P., Vujančević, J. D., Spreitzer, M., Kovač, J., Bartolić, D., Marković, S., Janković-Čaštvan, I., Tadić, N. B.,& Nikolić, M. V.. (2021). Exploring the impact of calcination parameters on the crystal structure, morphology, and optical properties of electrospun Fe                    2                    TiO                    5                    nanofibers. in RSC Advances
Royal Society of Chemistry (RSC)., 11(51), 32358-32368.
https://doi.org/10.1039/D1RA05748K
https://hdl.handle.net/21.15107/rcub_dais_12338
Vasiljević ZŽ, Dojčinović MP, Vujančević JD, Spreitzer M, Kovač J, Bartolić D, Marković S, Janković-Čaštvan I, Tadić NB, Nikolić MV. Exploring the impact of calcination parameters on the crystal structure, morphology, and optical properties of electrospun Fe                    2                    TiO                    5                    nanofibers. in RSC Advances. 2021;11(51):32358-32368.
doi:10.1039/D1RA05748K
https://hdl.handle.net/21.15107/rcub_dais_12338 .
Vasiljević, Zorka Ž., Dojčinović, Milena P., Vujančević, Jelena D., Spreitzer, Matjaž, Kovač, Janez, Bartolić, Dragana, Marković, Smilja, Janković-Čaštvan, Ivona, Tadić, Nenad B., Nikolić, Maria Vesna, "Exploring the impact of calcination parameters on the crystal structure, morphology, and optical properties of electrospun Fe                    2                    TiO                    5                    nanofibers" in RSC Advances, 11, no. 51 (2021):32358-32368,
https://doi.org/10.1039/D1RA05748K .,
https://hdl.handle.net/21.15107/rcub_dais_12338 .
11
11

Synthesis, structure and electrochemical performance of NiMn2O4

Dojčinović, Milena; Vasiljević, Zorka Ž.; Tadić, Nenad B.; Krstić, Jugoslav B.; Marković, Smilja; Spreitzer, Matjaž; Kovač, Janez; Nikolić, Maria Vesna

(Novi Sad : Faculty of Technology, 2021)

TY  - CONF
AU  - Dojčinović, Milena
AU  - Vasiljević, Zorka Ž.
AU  - Tadić, Nenad B.
AU  - Krstić, Jugoslav B.
AU  - Marković, Smilja
AU  - Spreitzer, Matjaž
AU  - Kovač, Janez
AU  - Nikolić, Maria Vesna
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/12397
AB  - NiMn2O4, with a cubic spinel structure and numerous and various applications in modern technology, were synthesized with two synthetic routes: sol-gel combustion method with glycine as fuel and electrospinning method with polyvinylpyrrolidone (PVP). Both amorphous powders from sol-gel synthesis and as-spun fibers from electrospinning synthesis were calcined, electrospun fibers at 400 °C and the sol-gel synthesized powders at 800 °C. Electrospun fibers were previously characterized with DTA-TGA to investigate the influence of thermal process on a polymer fiber.
The obtained powders were characterized accordingly. Structural analysis was done via X-ray diffraction (XRD) and results show spinel structure with no impurity. The texture and morphology was investigated via N2 physisorption and transmission electron microscopy (TEM), respectively. Chemical states of elements were investigated by X-ray photoelectron spectroscopy (XPS). The electrochemical performance of the synthesized materials as supercapacitors was tested via cyclic voltammetry (CV), electric impedance spectroscopy (EIS), and chronopotentiometry (CP) to aquire galvanostatic charge-discharge (GCD) curves. Experiments were done in 6 M KOH solution with nickel foam as a working electrode. The results show good electrochemical capacity circa 200 F/g, with the potential for further structural improvement of the materials.
PB  - Novi Sad : Faculty of Technology
C3  - Programme and book of abstracts / 14th ECerS Conference for Young Scientists in Ceramics (CYSC-2021), October 20-23, 2021, Novi Sad
T1  - Synthesis, structure and electrochemical performance of NiMn2O4
SP  - 81
EP  - 81
UR  - https://hdl.handle.net/21.15107/rcub_dais_12397
ER  - 
@conference{
author = "Dojčinović, Milena and Vasiljević, Zorka Ž. and Tadić, Nenad B. and Krstić, Jugoslav B. and Marković, Smilja and Spreitzer, Matjaž and Kovač, Janez and Nikolić, Maria Vesna",
year = "2021",
abstract = "NiMn2O4, with a cubic spinel structure and numerous and various applications in modern technology, were synthesized with two synthetic routes: sol-gel combustion method with glycine as fuel and electrospinning method with polyvinylpyrrolidone (PVP). Both amorphous powders from sol-gel synthesis and as-spun fibers from electrospinning synthesis were calcined, electrospun fibers at 400 °C and the sol-gel synthesized powders at 800 °C. Electrospun fibers were previously characterized with DTA-TGA to investigate the influence of thermal process on a polymer fiber.
The obtained powders were characterized accordingly. Structural analysis was done via X-ray diffraction (XRD) and results show spinel structure with no impurity. The texture and morphology was investigated via N2 physisorption and transmission electron microscopy (TEM), respectively. Chemical states of elements were investigated by X-ray photoelectron spectroscopy (XPS). The electrochemical performance of the synthesized materials as supercapacitors was tested via cyclic voltammetry (CV), electric impedance spectroscopy (EIS), and chronopotentiometry (CP) to aquire galvanostatic charge-discharge (GCD) curves. Experiments were done in 6 M KOH solution with nickel foam as a working electrode. The results show good electrochemical capacity circa 200 F/g, with the potential for further structural improvement of the materials.",
publisher = "Novi Sad : Faculty of Technology",
journal = "Programme and book of abstracts / 14th ECerS Conference for Young Scientists in Ceramics (CYSC-2021), October 20-23, 2021, Novi Sad",
title = "Synthesis, structure and electrochemical performance of NiMn2O4",
pages = "81-81",
url = "https://hdl.handle.net/21.15107/rcub_dais_12397"
}
Dojčinović, M., Vasiljević, Z. Ž., Tadić, N. B., Krstić, J. B., Marković, S., Spreitzer, M., Kovač, J.,& Nikolić, M. V.. (2021). Synthesis, structure and electrochemical performance of NiMn2O4. in Programme and book of abstracts / 14th ECerS Conference for Young Scientists in Ceramics (CYSC-2021), October 20-23, 2021, Novi Sad
Novi Sad : Faculty of Technology., 81-81.
https://hdl.handle.net/21.15107/rcub_dais_12397
Dojčinović M, Vasiljević ZŽ, Tadić NB, Krstić JB, Marković S, Spreitzer M, Kovač J, Nikolić MV. Synthesis, structure and electrochemical performance of NiMn2O4. in Programme and book of abstracts / 14th ECerS Conference for Young Scientists in Ceramics (CYSC-2021), October 20-23, 2021, Novi Sad. 2021;:81-81.
https://hdl.handle.net/21.15107/rcub_dais_12397 .
Dojčinović, Milena, Vasiljević, Zorka Ž., Tadić, Nenad B., Krstić, Jugoslav B., Marković, Smilja, Spreitzer, Matjaž, Kovač, Janez, Nikolić, Maria Vesna, "Synthesis, structure and electrochemical performance of NiMn2O4" in Programme and book of abstracts / 14th ECerS Conference for Young Scientists in Ceramics (CYSC-2021), October 20-23, 2021, Novi Sad (2021):81-81,
https://hdl.handle.net/21.15107/rcub_dais_12397 .

Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing

Nikolić, Maria Vesna; Krstić, Jugoslav; Labus, Nebojša; Luković, Miloljub; Dojčinović, Milena; Radovanović, Milan; Tadić, Nenad B.

(Elsevier, 2020)

TY  - JOUR
AU  - Nikolić, Maria Vesna
AU  - Krstić, Jugoslav
AU  - Labus, Nebojša
AU  - Luković, Miloljub
AU  - Dojčinović, Milena
AU  - Radovanović, Milan
AU  - Tadić, Nenad B.
PY  - 2020
UR  - https://dais.sanu.ac.rs/123456789/8950
AB  - Iron manganite (FeMnO3) powder with a cubic (bixbyite,−Ia3) crystal structure was obtained by a solid statereaction. Thick film paste (powder+organic vehicles) was screen printed on alumina substrate with test interdigitatedPdAg electrodes. Significant porosity (60.6%) composed of macropores (larger than 100 nm) wasdetermined by Hg porosimetry, changing only slightly from the first extrusion run indicating a stable poresystem. Hg porosimetry evaluation of thick film samples enabled estimation of true textural parameters of thethick film compared to powder. Impedance response of the thick film sensor was monitored in a humiditychamber in the relative humidity (RH) range 30–90%, at room temperature (25 °C) and frequency range from42 Hz to 1 MHz. At 100 Hz the impedance reduced from 10.41 MΩ for RH 30% to 0.68 MΩ for RH 90%. Analysisof complex impedance using an equivalent circuit showed the dominant influence of grain boundaries. Thesensor response and recovery was fast (several seconds) and a relatively low hysteresis value of 2.8% wasobtained.
PB  - Elsevier
T2  - Materials Science and Engineering B: Solid-State Materials for Advanced Technology
T1  - Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing
SP  - 114547
VL  - 257
DO  - 10.1016/j.mseb.2020.114547
UR  - https://hdl.handle.net/21.15107/rcub_dais_8950
ER  - 
@article{
author = "Nikolić, Maria Vesna and Krstić, Jugoslav and Labus, Nebojša and Luković, Miloljub and Dojčinović, Milena and Radovanović, Milan and Tadić, Nenad B.",
year = "2020",
abstract = "Iron manganite (FeMnO3) powder with a cubic (bixbyite,−Ia3) crystal structure was obtained by a solid statereaction. Thick film paste (powder+organic vehicles) was screen printed on alumina substrate with test interdigitatedPdAg electrodes. Significant porosity (60.6%) composed of macropores (larger than 100 nm) wasdetermined by Hg porosimetry, changing only slightly from the first extrusion run indicating a stable poresystem. Hg porosimetry evaluation of thick film samples enabled estimation of true textural parameters of thethick film compared to powder. Impedance response of the thick film sensor was monitored in a humiditychamber in the relative humidity (RH) range 30–90%, at room temperature (25 °C) and frequency range from42 Hz to 1 MHz. At 100 Hz the impedance reduced from 10.41 MΩ for RH 30% to 0.68 MΩ for RH 90%. Analysisof complex impedance using an equivalent circuit showed the dominant influence of grain boundaries. Thesensor response and recovery was fast (several seconds) and a relatively low hysteresis value of 2.8% wasobtained.",
publisher = "Elsevier",
journal = "Materials Science and Engineering B: Solid-State Materials for Advanced Technology",
title = "Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing",
pages = "114547",
volume = "257",
doi = "10.1016/j.mseb.2020.114547",
url = "https://hdl.handle.net/21.15107/rcub_dais_8950"
}
Nikolić, M. V., Krstić, J., Labus, N., Luković, M., Dojčinović, M., Radovanović, M.,& Tadić, N. B.. (2020). Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing. in Materials Science and Engineering B: Solid-State Materials for Advanced Technology
Elsevier., 257, 114547.
https://doi.org/10.1016/j.mseb.2020.114547
https://hdl.handle.net/21.15107/rcub_dais_8950
Nikolić MV, Krstić J, Labus N, Luković M, Dojčinović M, Radovanović M, Tadić NB. Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing. in Materials Science and Engineering B: Solid-State Materials for Advanced Technology. 2020;257:114547.
doi:10.1016/j.mseb.2020.114547
https://hdl.handle.net/21.15107/rcub_dais_8950 .
Nikolić, Maria Vesna, Krstić, Jugoslav, Labus, Nebojša, Luković, Miloljub, Dojčinović, Milena, Radovanović, Milan, Tadić, Nenad B., "Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing" in Materials Science and Engineering B: Solid-State Materials for Advanced Technology, 257 (2020):114547,
https://doi.org/10.1016/j.mseb.2020.114547 .,
https://hdl.handle.net/21.15107/rcub_dais_8950 .
8
3
7

Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing

Nikolić, Maria Vesna; Krstić, Jugoslav; Labus, Nebojša; Luković, Miloljub; Dojčinović, Milena; Radovanović, Milan; Tadić, Nenad B.

(Elsevier, 2020)

TY  - JOUR
AU  - Nikolić, Maria Vesna
AU  - Krstić, Jugoslav
AU  - Labus, Nebojša
AU  - Luković, Miloljub
AU  - Dojčinović, Milena
AU  - Radovanović, Milan
AU  - Tadić, Nenad B.
PY  - 2020
UR  - https://dais.sanu.ac.rs/123456789/10036
AB  - Iron manganite (FeMnO3) powder with a cubic (bixbyite,−Ia3) crystal structure was obtained by a solid statereaction. Thick film paste (powder+organic vehicles) was screen printed on alumina substrate with test interdigitatedPdAg electrodes. Significant porosity (60.6%) composed of macropores (larger than 100 nm) wasdetermined by Hg porosimetry, changing only slightly from the first extrusion run indicating a stable poresystem. Hg porosimetry evaluation of thick film samples enabled estimation of true textural parameters of thethick film compared to powder. Impedance response of the thick film sensor was monitored in a humiditychamber in the relative humidity (RH) range 30–90%, at room temperature (25 °C) and frequency range from42 Hz to 1 MHz. At 100 Hz the impedance reduced from 10.41 MΩ for RH 30% to 0.68 MΩ for RH 90%. Analysisof complex impedance using an equivalent circuit showed the dominant influence of grain boundaries. Thesensor response and recovery was fast (several seconds) and a relatively low hysteresis value of 2.8% wasobtained.
PB  - Elsevier
T2  - Materials Science and Engineering B: Solid-State Materials for Advanced Technology
T1  - Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing
SP  - 114547
VL  - 257
DO  - 10.1016/j.mseb.2020.114547
UR  - https://hdl.handle.net/21.15107/rcub_dais_10036
ER  - 
@article{
author = "Nikolić, Maria Vesna and Krstić, Jugoslav and Labus, Nebojša and Luković, Miloljub and Dojčinović, Milena and Radovanović, Milan and Tadić, Nenad B.",
year = "2020",
abstract = "Iron manganite (FeMnO3) powder with a cubic (bixbyite,−Ia3) crystal structure was obtained by a solid statereaction. Thick film paste (powder+organic vehicles) was screen printed on alumina substrate with test interdigitatedPdAg electrodes. Significant porosity (60.6%) composed of macropores (larger than 100 nm) wasdetermined by Hg porosimetry, changing only slightly from the first extrusion run indicating a stable poresystem. Hg porosimetry evaluation of thick film samples enabled estimation of true textural parameters of thethick film compared to powder. Impedance response of the thick film sensor was monitored in a humiditychamber in the relative humidity (RH) range 30–90%, at room temperature (25 °C) and frequency range from42 Hz to 1 MHz. At 100 Hz the impedance reduced from 10.41 MΩ for RH 30% to 0.68 MΩ for RH 90%. Analysisof complex impedance using an equivalent circuit showed the dominant influence of grain boundaries. Thesensor response and recovery was fast (several seconds) and a relatively low hysteresis value of 2.8% wasobtained.",
publisher = "Elsevier",
journal = "Materials Science and Engineering B: Solid-State Materials for Advanced Technology",
title = "Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing",
pages = "114547",
volume = "257",
doi = "10.1016/j.mseb.2020.114547",
url = "https://hdl.handle.net/21.15107/rcub_dais_10036"
}
Nikolić, M. V., Krstić, J., Labus, N., Luković, M., Dojčinović, M., Radovanović, M.,& Tadić, N. B.. (2020). Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing. in Materials Science and Engineering B: Solid-State Materials for Advanced Technology
Elsevier., 257, 114547.
https://doi.org/10.1016/j.mseb.2020.114547
https://hdl.handle.net/21.15107/rcub_dais_10036
Nikolić MV, Krstić J, Labus N, Luković M, Dojčinović M, Radovanović M, Tadić NB. Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing. in Materials Science and Engineering B: Solid-State Materials for Advanced Technology. 2020;257:114547.
doi:10.1016/j.mseb.2020.114547
https://hdl.handle.net/21.15107/rcub_dais_10036 .
Nikolić, Maria Vesna, Krstić, Jugoslav, Labus, Nebojša, Luković, Miloljub, Dojčinović, Milena, Radovanović, Milan, Tadić, Nenad B., "Structural, morphological and textural properties of iron manganite (FeMnO3) thick films applied for humidity sensing" in Materials Science and Engineering B: Solid-State Materials for Advanced Technology, 257 (2020):114547,
https://doi.org/10.1016/j.mseb.2020.114547 .,
https://hdl.handle.net/21.15107/rcub_dais_10036 .
8
3
7

Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method

Vasiljević, Zorka Ž.; Dojčinović, Milena; Vujančević, Jelena; Janković Častvan, Ivona; Ognjanović, M.; Tadić, Nenad B.; Stojadinović, Stevan; Branković, Goran; Nikolić, Maria Vesna

(Royal Society, 2020)

TY  - JOUR
AU  - Vasiljević, Zorka Ž.
AU  - Dojčinović, Milena
AU  - Vujančević, Jelena
AU  - Janković Častvan, Ivona
AU  - Ognjanović, M.
AU  - Tadić, Nenad B.
AU  - Stojadinović, Stevan
AU  - Branković, Goran
AU  - Nikolić, Maria Vesna
PY  - 2020
UR  - https://dais.sanu.ac.rs/123456789/9107
AB  - The aim of this work was to synthesize semiconducting oxide nanoparticles using a simple method with low production cost to be applied in natural sunlight for photocatalytic degradation of pollutants in waste water. Iron titanate (Fe2TiO5) nanoparticles with an orthorhombic structure were successfully synthesized using a modified sol–gel method and calcination at 750°C. The as-prepared Fe2TiO5 nanoparticles exhibited a moderate specific surface area. The mesoporous Fe2TiO5 nanoparticles possessed strong absorption in the visible-light region and the band gap was estimated to be around 2.16 eV. The photocatalytic activity was evaluated by the degradation of methylene blue under natural sunlight. The effect of parameters such as the amount of catalyst, initial concentration of the dye and pH of the dye solution on the removal efficiency of methylene blue was investigated. Fe2TiO5 showed high degradation efficiency in a strong alkaline medium that can be the result of the facilitated formation of OH radicals due to an increased concentration of hydroxyl ions.
PB  - Royal Society
T2  - Royal Society Open Science
T1  - Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method
VL  - 7
IS  - 9
DO  - 10.1098/rsos.200708
UR  - https://hdl.handle.net/21.15107/rcub_dais_9107
ER  - 
@article{
author = "Vasiljević, Zorka Ž. and Dojčinović, Milena and Vujančević, Jelena and Janković Častvan, Ivona and Ognjanović, M. and Tadić, Nenad B. and Stojadinović, Stevan and Branković, Goran and Nikolić, Maria Vesna",
year = "2020",
abstract = "The aim of this work was to synthesize semiconducting oxide nanoparticles using a simple method with low production cost to be applied in natural sunlight for photocatalytic degradation of pollutants in waste water. Iron titanate (Fe2TiO5) nanoparticles with an orthorhombic structure were successfully synthesized using a modified sol–gel method and calcination at 750°C. The as-prepared Fe2TiO5 nanoparticles exhibited a moderate specific surface area. The mesoporous Fe2TiO5 nanoparticles possessed strong absorption in the visible-light region and the band gap was estimated to be around 2.16 eV. The photocatalytic activity was evaluated by the degradation of methylene blue under natural sunlight. The effect of parameters such as the amount of catalyst, initial concentration of the dye and pH of the dye solution on the removal efficiency of methylene blue was investigated. Fe2TiO5 showed high degradation efficiency in a strong alkaline medium that can be the result of the facilitated formation of OH radicals due to an increased concentration of hydroxyl ions.",
publisher = "Royal Society",
journal = "Royal Society Open Science",
title = "Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method",
volume = "7",
number = "9",
doi = "10.1098/rsos.200708",
url = "https://hdl.handle.net/21.15107/rcub_dais_9107"
}
Vasiljević, Z. Ž., Dojčinović, M., Vujančević, J., Janković Častvan, I., Ognjanović, M., Tadić, N. B., Stojadinović, S., Branković, G.,& Nikolić, M. V.. (2020). Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method. in Royal Society Open Science
Royal Society., 7(9).
https://doi.org/10.1098/rsos.200708
https://hdl.handle.net/21.15107/rcub_dais_9107
Vasiljević ZŽ, Dojčinović M, Vujančević J, Janković Častvan I, Ognjanović M, Tadić NB, Stojadinović S, Branković G, Nikolić MV. Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method. in Royal Society Open Science. 2020;7(9).
doi:10.1098/rsos.200708
https://hdl.handle.net/21.15107/rcub_dais_9107 .
Vasiljević, Zorka Ž., Dojčinović, Milena, Vujančević, Jelena, Janković Častvan, Ivona, Ognjanović, M., Tadić, Nenad B., Stojadinović, Stevan, Branković, Goran, Nikolić, Maria Vesna, "Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method" in Royal Society Open Science, 7, no. 9 (2020),
https://doi.org/10.1098/rsos.200708 .,
https://hdl.handle.net/21.15107/rcub_dais_9107 .
1
163
20

Synthesis and antibacterial activity of iron manganite (FeMnO3) particles against the environmental bacterium Bacillus subtilis

Vasiljević, Zorka Ž.; Dojčinović, Milena; Krstić, Jugoslav B.; Ribić, Vesna; Tadić, Nenad B.; Ognjanović, Miloš; Auger, Sandrine; Vidić, Jasmina; Nikolić, Maria Vesna

(Royal Society of Chemistry, 2020)

TY  - JOUR
AU  - Vasiljević, Zorka Ž.
AU  - Dojčinović, Milena
AU  - Krstić, Jugoslav B.
AU  - Ribić, Vesna
AU  - Tadić, Nenad B.
AU  - Ognjanović, Miloš
AU  - Auger, Sandrine
AU  - Vidić, Jasmina
AU  - Nikolić, Maria Vesna
PY  - 2020
UR  - https://dais.sanu.ac.rs/123456789/7780
AB  - Nanocrystalline iron manganite powder was synthesized using the sol–gel combustion process, with glycine as fuel. It was further calcined at 900 °C for 8 h, resulting in the formation of a loose cubic FeMnO3 powder with a small specific surface area, net-like structure and plate-like particles as confirmed by XRD, N2 physisorption, FESEM and TEM analyses. The metal ion release was studied by ICP-OES and showed that less than 10 ppb of Fe or Mn ions were released by leaching in water, but 0.36 ppm Fe and 3.69 ppm Mn was found in LB (Luria–Bertani) bacterial medium. The generation of reactive oxygen species (ROS) was monitored in distilled water and bacterial medium and showed that FeMnO3 particles do not generate O2˙− ions with or without UV irradiation, but synthesize H2O2 and show an antioxidative effect. Besides the higher stability of FeMnO3 particles in aqueous solution they showed an inhibitory effect on Bacillus subtilis growth in LB medium even at low concentrations (0.01 mg ml−1), but not in BHI medium even at 1 mg ml−1. This study points out that the mechanism of antibacterial action of engineered metal oxides needs continued investigation and specific experimental controls.
PB  - Royal Society of Chemistry
T2  - RSC Advances
T1  - Synthesis and antibacterial activity of iron manganite (FeMnO3) particles against the environmental bacterium Bacillus subtilis
SP  - 13879
EP  - 13888
VL  - 10
IS  - 23
DO  - 10.1039/D0RA01809K
UR  - https://hdl.handle.net/21.15107/rcub_dais_7780
ER  - 
@article{
author = "Vasiljević, Zorka Ž. and Dojčinović, Milena and Krstić, Jugoslav B. and Ribić, Vesna and Tadić, Nenad B. and Ognjanović, Miloš and Auger, Sandrine and Vidić, Jasmina and Nikolić, Maria Vesna",
year = "2020",
abstract = "Nanocrystalline iron manganite powder was synthesized using the sol–gel combustion process, with glycine as fuel. It was further calcined at 900 °C for 8 h, resulting in the formation of a loose cubic FeMnO3 powder with a small specific surface area, net-like structure and plate-like particles as confirmed by XRD, N2 physisorption, FESEM and TEM analyses. The metal ion release was studied by ICP-OES and showed that less than 10 ppb of Fe or Mn ions were released by leaching in water, but 0.36 ppm Fe and 3.69 ppm Mn was found in LB (Luria–Bertani) bacterial medium. The generation of reactive oxygen species (ROS) was monitored in distilled water and bacterial medium and showed that FeMnO3 particles do not generate O2˙− ions with or without UV irradiation, but synthesize H2O2 and show an antioxidative effect. Besides the higher stability of FeMnO3 particles in aqueous solution they showed an inhibitory effect on Bacillus subtilis growth in LB medium even at low concentrations (0.01 mg ml−1), but not in BHI medium even at 1 mg ml−1. This study points out that the mechanism of antibacterial action of engineered metal oxides needs continued investigation and specific experimental controls.",
publisher = "Royal Society of Chemistry",
journal = "RSC Advances",
title = "Synthesis and antibacterial activity of iron manganite (FeMnO3) particles against the environmental bacterium Bacillus subtilis",
pages = "13879-13888",
volume = "10",
number = "23",
doi = "10.1039/D0RA01809K",
url = "https://hdl.handle.net/21.15107/rcub_dais_7780"
}
Vasiljević, Z. Ž., Dojčinović, M., Krstić, J. B., Ribić, V., Tadić, N. B., Ognjanović, M., Auger, S., Vidić, J.,& Nikolić, M. V.. (2020). Synthesis and antibacterial activity of iron manganite (FeMnO3) particles against the environmental bacterium Bacillus subtilis. in RSC Advances
Royal Society of Chemistry., 10(23), 13879-13888.
https://doi.org/10.1039/D0RA01809K
https://hdl.handle.net/21.15107/rcub_dais_7780
Vasiljević ZŽ, Dojčinović M, Krstić JB, Ribić V, Tadić NB, Ognjanović M, Auger S, Vidić J, Nikolić MV. Synthesis and antibacterial activity of iron manganite (FeMnO3) particles against the environmental bacterium Bacillus subtilis. in RSC Advances. 2020;10(23):13879-13888.
doi:10.1039/D0RA01809K
https://hdl.handle.net/21.15107/rcub_dais_7780 .
Vasiljević, Zorka Ž., Dojčinović, Milena, Krstić, Jugoslav B., Ribić, Vesna, Tadić, Nenad B., Ognjanović, Miloš, Auger, Sandrine, Vidić, Jasmina, Nikolić, Maria Vesna, "Synthesis and antibacterial activity of iron manganite (FeMnO3) particles against the environmental bacterium Bacillus subtilis" in RSC Advances, 10, no. 23 (2020):13879-13888,
https://doi.org/10.1039/D0RA01809K .,
https://hdl.handle.net/21.15107/rcub_dais_7780 .
18
11
18

Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen‐printed thick films for application in humidity sensing

Nikolić, Maria Vesna; Vasiljević, Zorka Ž.; Luković, Miloljub D.; Pavlović, Vera P.; Krstić, Jugoslav B.; Vujančević, Jelena; Tadić, Nenad B.; Vlahović, Branislav; Pavlović, Vladimir B.

(John Wiley & Sons, Inc., 2019)

TY  - JOUR
AU  - Nikolić, Maria Vesna
AU  - Vasiljević, Zorka Ž.
AU  - Luković, Miloljub D.
AU  - Pavlović, Vera P.
AU  - Krstić, Jugoslav B.
AU  - Vujančević, Jelena
AU  - Tadić, Nenad B.
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://ceramics.onlinelibrary.wiley.com/doi/abs/10.1111/ijac.13190
UR  - https://dais.sanu.ac.rs/123456789/5766
AB  - Zinc ferrite nanocrystalline powder was obtained by solid state synthesis of starting zinc oxide and hematite nanopowders. Field emission scanning electron microscopy (FESEM and transmission electron microscopy (TEM), X‐ray diffraction (XRD), X‐ray photoelectron spectroscopy (XPS) and Raman spectroscopy confirmed the formation of nanocrystalline zinc‐ferrite powder with a mixed spinel structure with small amounts of remaining zinc oxide and hematite as impurities. Thick film paste was formed and screen printed on test interdigitated PdAg electrodes on alumina substrate. Formation of a porous nanocrystalline structure was confirmed by scanning electron microscopy (SEM) and Hg porosimetry. Humidity sensing properties of zinc ferrite thick films were investigated by monitoring the change in impedance in the relative humidity interval 30‐90% in the frequency range 42 Hz – 1 MHz at room temperature (25 °C) and 50 °C. At 42 Hz at both analyzed temperatures the impedance reduced ~ 46 times in the humidity range 30‐90%. The dominant influence of grain boundaries was confirmed by analysis of complex impedance with an equivalent circuit.
PB  - John Wiley & Sons, Inc.
T2  - International Journal of Applied Ceramic Technology
T1  - Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen‐printed thick films for application in humidity sensing
SP  - 981
EP  - 993
VL  - 16
IS  - 3
DO  - 10.1111/ijac.13190
UR  - https://hdl.handle.net/21.15107/rcub_dais_5766
ER  - 
@article{
author = "Nikolić, Maria Vesna and Vasiljević, Zorka Ž. and Luković, Miloljub D. and Pavlović, Vera P. and Krstić, Jugoslav B. and Vujančević, Jelena and Tadić, Nenad B. and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2019",
abstract = "Zinc ferrite nanocrystalline powder was obtained by solid state synthesis of starting zinc oxide and hematite nanopowders. Field emission scanning electron microscopy (FESEM and transmission electron microscopy (TEM), X‐ray diffraction (XRD), X‐ray photoelectron spectroscopy (XPS) and Raman spectroscopy confirmed the formation of nanocrystalline zinc‐ferrite powder with a mixed spinel structure with small amounts of remaining zinc oxide and hematite as impurities. Thick film paste was formed and screen printed on test interdigitated PdAg electrodes on alumina substrate. Formation of a porous nanocrystalline structure was confirmed by scanning electron microscopy (SEM) and Hg porosimetry. Humidity sensing properties of zinc ferrite thick films were investigated by monitoring the change in impedance in the relative humidity interval 30‐90% in the frequency range 42 Hz – 1 MHz at room temperature (25 °C) and 50 °C. At 42 Hz at both analyzed temperatures the impedance reduced ~ 46 times in the humidity range 30‐90%. The dominant influence of grain boundaries was confirmed by analysis of complex impedance with an equivalent circuit.",
publisher = "John Wiley & Sons, Inc.",
journal = "International Journal of Applied Ceramic Technology",
title = "Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen‐printed thick films for application in humidity sensing",
pages = "981-993",
volume = "16",
number = "3",
doi = "10.1111/ijac.13190",
url = "https://hdl.handle.net/21.15107/rcub_dais_5766"
}
Nikolić, M. V., Vasiljević, Z. Ž., Luković, M. D., Pavlović, V. P., Krstić, J. B., Vujančević, J., Tadić, N. B., Vlahović, B.,& Pavlović, V. B.. (2019). Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen‐printed thick films for application in humidity sensing. in International Journal of Applied Ceramic Technology
John Wiley & Sons, Inc.., 16(3), 981-993.
https://doi.org/10.1111/ijac.13190
https://hdl.handle.net/21.15107/rcub_dais_5766
Nikolić MV, Vasiljević ZŽ, Luković MD, Pavlović VP, Krstić JB, Vujančević J, Tadić NB, Vlahović B, Pavlović VB. Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen‐printed thick films for application in humidity sensing. in International Journal of Applied Ceramic Technology. 2019;16(3):981-993.
doi:10.1111/ijac.13190
https://hdl.handle.net/21.15107/rcub_dais_5766 .
Nikolić, Maria Vesna, Vasiljević, Zorka Ž., Luković, Miloljub D., Pavlović, Vera P., Krstić, Jugoslav B., Vujančević, Jelena, Tadić, Nenad B., Vlahović, Branislav, Pavlović, Vladimir B., "Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen‐printed thick films for application in humidity sensing" in International Journal of Applied Ceramic Technology, 16, no. 3 (2019):981-993,
https://doi.org/10.1111/ijac.13190 .,
https://hdl.handle.net/21.15107/rcub_dais_5766 .
36
15
37

Nanocrystalline iron-manganite (FeMnO3) applied for humidity sensing

Vasiljević, Zorka Ž.; Dojčinović, Milena; Vujančević, Jelena; Tadić, Nenad B.; Nikolić, Maria Vesna

(Belgrade : Institute for Multidisciplinary Research, 2019)

TY  - CONF
AU  - Vasiljević, Zorka Ž.
AU  - Dojčinović, Milena
AU  - Vujančević, Jelena
AU  - Tadić, Nenad B.
AU  - Nikolić, Maria Vesna
PY  - 2019
UR  - https://dais.sanu.ac.rs/123456789/7005
AB  - Nanocrystalline iron manganite was synthesized using a sol-gel self-combustion method with glycine as fuel, followed by calcination at 900 °C for 8 hours. Structural characterization was performed using X-ray diffraction (XRD) and field emission scanning electron microscopy (FESEM). It confirmed the formation of nanocrystalline iron-manganite with a perovskite structure. Humidity sensing properties of bulk and thick film samples of the obtained nanocrystalline iron manganite powder were analyzed. Organic vehicles were added to the powder to form a thick film paste that was screen printed on alumina substrate with test PdAg interdigitated electrodes. Impedance response of bulk and thick film samples was analyzed in a humidity chamber in the relative humidity range 30-90% in the frequency range 42 Hz to 1 MHz in view of applying iron-manganite for humidity sensing applications.
PB  - Belgrade : Institute for Multidisciplinary Research
C3  - Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia
T1  - Nanocrystalline iron-manganite (FeMnO3) applied for humidity sensing
SP  - 94
EP  - 94
UR  - https://hdl.handle.net/21.15107/rcub_dais_7005
ER  - 
@conference{
author = "Vasiljević, Zorka Ž. and Dojčinović, Milena and Vujančević, Jelena and Tadić, Nenad B. and Nikolić, Maria Vesna",
year = "2019",
abstract = "Nanocrystalline iron manganite was synthesized using a sol-gel self-combustion method with glycine as fuel, followed by calcination at 900 °C for 8 hours. Structural characterization was performed using X-ray diffraction (XRD) and field emission scanning electron microscopy (FESEM). It confirmed the formation of nanocrystalline iron-manganite with a perovskite structure. Humidity sensing properties of bulk and thick film samples of the obtained nanocrystalline iron manganite powder were analyzed. Organic vehicles were added to the powder to form a thick film paste that was screen printed on alumina substrate with test PdAg interdigitated electrodes. Impedance response of bulk and thick film samples was analyzed in a humidity chamber in the relative humidity range 30-90% in the frequency range 42 Hz to 1 MHz in view of applying iron-manganite for humidity sensing applications.",
publisher = "Belgrade : Institute for Multidisciplinary Research",
journal = "Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia",
title = "Nanocrystalline iron-manganite (FeMnO3) applied for humidity sensing",
pages = "94-94",
url = "https://hdl.handle.net/21.15107/rcub_dais_7005"
}
Vasiljević, Z. Ž., Dojčinović, M., Vujančević, J., Tadić, N. B.,& Nikolić, M. V.. (2019). Nanocrystalline iron-manganite (FeMnO3) applied for humidity sensing. in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia
Belgrade : Institute for Multidisciplinary Research., 94-94.
https://hdl.handle.net/21.15107/rcub_dais_7005
Vasiljević ZŽ, Dojčinović M, Vujančević J, Tadić NB, Nikolić MV. Nanocrystalline iron-manganite (FeMnO3) applied for humidity sensing. in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia. 2019;:94-94.
https://hdl.handle.net/21.15107/rcub_dais_7005 .
Vasiljević, Zorka Ž., Dojčinović, Milena, Vujančević, Jelena, Tadić, Nenad B., Nikolić, Maria Vesna, "Nanocrystalline iron-manganite (FeMnO3) applied for humidity sensing" in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia (2019):94-94,
https://hdl.handle.net/21.15107/rcub_dais_7005 .

Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites

Vasiljević, Zorka Ž.; Dojčinović, Milena; Pavlović, Vera P.; Vujančević, Jelena; Marković, Smilja; Tadić, Nenad B.; Nikolić, Maria Vesna

(Belgrade : Institute for Multidisciplinary Research, 2019)

TY  - CONF
AU  - Vasiljević, Zorka Ž.
AU  - Dojčinović, Milena
AU  - Pavlović, Vera P.
AU  - Vujančević, Jelena
AU  - Marković, Smilja
AU  - Tadić, Nenad B.
AU  - Nikolić, Maria Vesna
PY  - 2019
UR  - https://dais.sanu.ac.rs/123456789/7003
AB  - In this work, spinel magnesium cobalt ferrites (CoxMg1-xFe2O4, x = 0.0, 0.1, 0.3, 0.5, 0.7, 0.9) were synthesized by a sol-gel combustion method. Magnesium nitrate, cobalt nitrate and iron nitrate were used as oxidizers and citric acid was used as a reducing agent. The effects of cobalt ions on structural and morphological properties were investigated and characterized by X-ray diffraction (XRD), Raman spectroscopy, Field emission scanning electron microscope (FESEM) and Fourier transform infrared (FT-IR) spectroscopy. A cubic spinel structure formed with a varied distribution of cobalt and magnesium ions on tetrahedral and octahedral sites that depended on their content. All ferrite powders consisted of multigrain agglomerates. Optical properties were investigated by UV- vis spectrophotometry. The photocatalytic activity of as prepared samples was evaluated by measuring the rate of photodegradation reaction of methylene blue (MB) under visible light irradiation. After 240 min, compared to other samples, the sample labeled as Co0.1Mg0.9Fe2O4 showed the best rate of photodecomposition of MB resulting in reduction of 90% of its initial concentration.
PB  - Belgrade : Institute for Multidisciplinary Research
C3  - Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia
T1  - Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites
SP  - 73
EP  - 73
UR  - https://hdl.handle.net/21.15107/rcub_dais_7003
ER  - 
@conference{
author = "Vasiljević, Zorka Ž. and Dojčinović, Milena and Pavlović, Vera P. and Vujančević, Jelena and Marković, Smilja and Tadić, Nenad B. and Nikolić, Maria Vesna",
year = "2019",
abstract = "In this work, spinel magnesium cobalt ferrites (CoxMg1-xFe2O4, x = 0.0, 0.1, 0.3, 0.5, 0.7, 0.9) were synthesized by a sol-gel combustion method. Magnesium nitrate, cobalt nitrate and iron nitrate were used as oxidizers and citric acid was used as a reducing agent. The effects of cobalt ions on structural and morphological properties were investigated and characterized by X-ray diffraction (XRD), Raman spectroscopy, Field emission scanning electron microscope (FESEM) and Fourier transform infrared (FT-IR) spectroscopy. A cubic spinel structure formed with a varied distribution of cobalt and magnesium ions on tetrahedral and octahedral sites that depended on their content. All ferrite powders consisted of multigrain agglomerates. Optical properties were investigated by UV- vis spectrophotometry. The photocatalytic activity of as prepared samples was evaluated by measuring the rate of photodegradation reaction of methylene blue (MB) under visible light irradiation. After 240 min, compared to other samples, the sample labeled as Co0.1Mg0.9Fe2O4 showed the best rate of photodecomposition of MB resulting in reduction of 90% of its initial concentration.",
publisher = "Belgrade : Institute for Multidisciplinary Research",
journal = "Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia",
title = "Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites",
pages = "73-73",
url = "https://hdl.handle.net/21.15107/rcub_dais_7003"
}
Vasiljević, Z. Ž., Dojčinović, M., Pavlović, V. P., Vujančević, J., Marković, S., Tadić, N. B.,& Nikolić, M. V.. (2019). Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites. in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia
Belgrade : Institute for Multidisciplinary Research., 73-73.
https://hdl.handle.net/21.15107/rcub_dais_7003
Vasiljević ZŽ, Dojčinović M, Pavlović VP, Vujančević J, Marković S, Tadić NB, Nikolić MV. Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites. in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia. 2019;:73-73.
https://hdl.handle.net/21.15107/rcub_dais_7003 .
Vasiljević, Zorka Ž., Dojčinović, Milena, Pavlović, Vera P., Vujančević, Jelena, Marković, Smilja, Tadić, Nenad B., Nikolić, Maria Vesna, "Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites" in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia (2019):73-73,
https://hdl.handle.net/21.15107/rcub_dais_7003 .

Structure and photocatalytic properties of sol-gel synthesized pseudobrookite

Vasiljević, Zorka Ž.; Dojčinović, Milena; Janković Častvan, Ivona; Vujančević, Jelena; Tadić, Nenad B.; Nikolić, Maria Vesna

(Novi Sad : Faculty of Technology, 2019)

TY  - CONF
AU  - Vasiljević, Zorka Ž.
AU  - Dojčinović, Milena
AU  - Janković Častvan, Ivona
AU  - Vujančević, Jelena
AU  - Tadić, Nenad B.
AU  - Nikolić, Maria Vesna
PY  - 2019
UR  - https://dais.sanu.ac.rs/123456789/6988
AB  - Fe2TiO5 nanopartcles were synthesized by modified sol-gel method with aid of
Fe(NO3)3 9H2O and Ti(OC3H7)4 as starting reagents, oxalic acid as chilate agent and cetyltrimethylammonium bromide as surfactant. The aim of this study was to asses the photocatalytic degradaton of the antibiotic Oxytetracycline (OTC) using visible light irradiation. As prepared nanoparticles were characterized by XRD, BET, FESEM and UV-vis DRS. The optimal operating conditions of oxytetracycline photocatalytic degradation were achived by changing the pH of the solution and changing the concentration of photocatalyst.
PB  - Novi Sad : Faculty of Technology
C3  - Programme and book of abstracts / 13th Conference for Young Scientists in Ceramics (CYSC-2017), October 16-19, 2019, Novi Sad
T1  - Structure and photocatalytic properties of sol-gel synthesized pseudobrookite
SP  - 133
EP  - 133
UR  - https://hdl.handle.net/21.15107/rcub_dais_6988
ER  - 
@conference{
author = "Vasiljević, Zorka Ž. and Dojčinović, Milena and Janković Častvan, Ivona and Vujančević, Jelena and Tadić, Nenad B. and Nikolić, Maria Vesna",
year = "2019",
abstract = "Fe2TiO5 nanopartcles were synthesized by modified sol-gel method with aid of
Fe(NO3)3 9H2O and Ti(OC3H7)4 as starting reagents, oxalic acid as chilate agent and cetyltrimethylammonium bromide as surfactant. The aim of this study was to asses the photocatalytic degradaton of the antibiotic Oxytetracycline (OTC) using visible light irradiation. As prepared nanoparticles were characterized by XRD, BET, FESEM and UV-vis DRS. The optimal operating conditions of oxytetracycline photocatalytic degradation were achived by changing the pH of the solution and changing the concentration of photocatalyst.",
publisher = "Novi Sad : Faculty of Technology",
journal = "Programme and book of abstracts / 13th Conference for Young Scientists in Ceramics (CYSC-2017), October 16-19, 2019, Novi Sad",
title = "Structure and photocatalytic properties of sol-gel synthesized pseudobrookite",
pages = "133-133",
url = "https://hdl.handle.net/21.15107/rcub_dais_6988"
}
Vasiljević, Z. Ž., Dojčinović, M., Janković Častvan, I., Vujančević, J., Tadić, N. B.,& Nikolić, M. V.. (2019). Structure and photocatalytic properties of sol-gel synthesized pseudobrookite. in Programme and book of abstracts / 13th Conference for Young Scientists in Ceramics (CYSC-2017), October 16-19, 2019, Novi Sad
Novi Sad : Faculty of Technology., 133-133.
https://hdl.handle.net/21.15107/rcub_dais_6988
Vasiljević ZŽ, Dojčinović M, Janković Častvan I, Vujančević J, Tadić NB, Nikolić MV. Structure and photocatalytic properties of sol-gel synthesized pseudobrookite. in Programme and book of abstracts / 13th Conference for Young Scientists in Ceramics (CYSC-2017), October 16-19, 2019, Novi Sad. 2019;:133-133.
https://hdl.handle.net/21.15107/rcub_dais_6988 .
Vasiljević, Zorka Ž., Dojčinović, Milena, Janković Častvan, Ivona, Vujančević, Jelena, Tadić, Nenad B., Nikolić, Maria Vesna, "Structure and photocatalytic properties of sol-gel synthesized pseudobrookite" in Programme and book of abstracts / 13th Conference for Young Scientists in Ceramics (CYSC-2017), October 16-19, 2019, Novi Sad (2019):133-133,
https://hdl.handle.net/21.15107/rcub_dais_6988 .

Visible light photocatalytic activity of nanocrystalline CoxMg1-xFe2O4 (x = 0-1)

Dojčinović, Milena; Vasiljević, Zorka Ž.; Vujančević, Jelena; Pavlović, Vera P.; Marković, Smilja; Tadić, Nenad B.; Nikolić, Marina V.

(Novi Sad : Faculty of Technology, 2019)

TY  - CONF
AU  - Dojčinović, Milena
AU  - Vasiljević, Zorka Ž.
AU  - Vujančević, Jelena
AU  - Pavlović, Vera P.
AU  - Marković, Smilja
AU  - Tadić, Nenad B.
AU  - Nikolić, Marina V.
PY  - 2019
UR  - https://dais.sanu.ac.rs/123456789/6986
AB  - The sol-gel combustion method was applied for synthesis of spinel magnesium cobalt ferrites CoxMg1-xFe2O4, with varying cobalt and magnesium content, x = 0.0, 0.1, 0.3, 0.5, 0.7, 0.9. Magnesium nitrate, cobalt nitrate and iron nitrate were used as oxidizers and citric acid was used as a reducing agent. Structural and morphological properties of the obtained ferrite powders were investigated and characterized by X-ray diffraction (XRD), Raman spectroscopy, Field emission scanning electron microscope (FESEM) and Fourier transform infrared (FT-IR) spectroscopy. Optical properties were investigated by UV-VIS spectrophotometry. A cubic spinel structure with multigrain agglomerates formed. Visible light photocatalytic activity of the spinel ferrite powder samples was evaluated by measuring the rate of photodegradation reaction of methylene blue (MB). After 240 min Co0.1Mg0.9Fe2O4 showed the best rate of photodecomposition of MB resulting in 90% of its initial concentration in an alkaline environment.
PB  - Novi Sad : Faculty of Technology
C3  - Programme and book of abstracts / 13th Conference for Young Scientists in Ceramics (CYSC-2017), October 16-19, 2019, Novi Sad
T1  - Visible light photocatalytic activity of nanocrystalline CoxMg1-xFe2O4 (x = 0-1)
SP  - 136
EP  - 136
UR  - https://hdl.handle.net/21.15107/rcub_dais_6986
ER  - 
@conference{
author = "Dojčinović, Milena and Vasiljević, Zorka Ž. and Vujančević, Jelena and Pavlović, Vera P. and Marković, Smilja and Tadić, Nenad B. and Nikolić, Marina V.",
year = "2019",
abstract = "The sol-gel combustion method was applied for synthesis of spinel magnesium cobalt ferrites CoxMg1-xFe2O4, with varying cobalt and magnesium content, x = 0.0, 0.1, 0.3, 0.5, 0.7, 0.9. Magnesium nitrate, cobalt nitrate and iron nitrate were used as oxidizers and citric acid was used as a reducing agent. Structural and morphological properties of the obtained ferrite powders were investigated and characterized by X-ray diffraction (XRD), Raman spectroscopy, Field emission scanning electron microscope (FESEM) and Fourier transform infrared (FT-IR) spectroscopy. Optical properties were investigated by UV-VIS spectrophotometry. A cubic spinel structure with multigrain agglomerates formed. Visible light photocatalytic activity of the spinel ferrite powder samples was evaluated by measuring the rate of photodegradation reaction of methylene blue (MB). After 240 min Co0.1Mg0.9Fe2O4 showed the best rate of photodecomposition of MB resulting in 90% of its initial concentration in an alkaline environment.",
publisher = "Novi Sad : Faculty of Technology",
journal = "Programme and book of abstracts / 13th Conference for Young Scientists in Ceramics (CYSC-2017), October 16-19, 2019, Novi Sad",
title = "Visible light photocatalytic activity of nanocrystalline CoxMg1-xFe2O4 (x = 0-1)",
pages = "136-136",
url = "https://hdl.handle.net/21.15107/rcub_dais_6986"
}
Dojčinović, M., Vasiljević, Z. Ž., Vujančević, J., Pavlović, V. P., Marković, S., Tadić, N. B.,& Nikolić, M. V.. (2019). Visible light photocatalytic activity of nanocrystalline CoxMg1-xFe2O4 (x = 0-1). in Programme and book of abstracts / 13th Conference for Young Scientists in Ceramics (CYSC-2017), October 16-19, 2019, Novi Sad
Novi Sad : Faculty of Technology., 136-136.
https://hdl.handle.net/21.15107/rcub_dais_6986
Dojčinović M, Vasiljević ZŽ, Vujančević J, Pavlović VP, Marković S, Tadić NB, Nikolić MV. Visible light photocatalytic activity of nanocrystalline CoxMg1-xFe2O4 (x = 0-1). in Programme and book of abstracts / 13th Conference for Young Scientists in Ceramics (CYSC-2017), October 16-19, 2019, Novi Sad. 2019;:136-136.
https://hdl.handle.net/21.15107/rcub_dais_6986 .
Dojčinović, Milena, Vasiljević, Zorka Ž., Vujančević, Jelena, Pavlović, Vera P., Marković, Smilja, Tadić, Nenad B., Nikolić, Marina V., "Visible light photocatalytic activity of nanocrystalline CoxMg1-xFe2O4 (x = 0-1)" in Programme and book of abstracts / 13th Conference for Young Scientists in Ceramics (CYSC-2017), October 16-19, 2019, Novi Sad (2019):136-136,
https://hdl.handle.net/21.15107/rcub_dais_6986 .

Photocatalytic degradation of methylene blue and oxytetracycline via sol-gel synthesized pseudobrookite

Vasiljević, Zorka Ž.; Dojčinović, Milena; Janković Častvan, Ivona; Vujančević, Jelena; Tadić, Nenad B.; Nikolić, Maria Vesna

(Belgrade : Institute of Technical Sciences of SASA, 2019)

TY  - CONF
AU  - Vasiljević, Zorka Ž.
AU  - Dojčinović, Milena
AU  - Janković Častvan, Ivona
AU  - Vujančević, Jelena
AU  - Tadić, Nenad B.
AU  - Nikolić, Maria Vesna
PY  - 2019
UR  - https://dais.sanu.ac.rs/123456789/6967
AB  - Fe2TiO5 nanoparticles were synthesized by modified sol-gel method using Fe(NO3)3×9H2O and Ti(OC3H7)4 as starting reagents, oxalic acid as chilate agent and cetyltrimethylammonium bromide as surfactant. The aim of this study was to asses the photocatalytic degradaton of water pollutants, methylene blue and the antibiotic Oxytetracycline (OTC) using natural sunlight irradiation. As prepared nanoparticles were characterized by XRD, BET, FESEM and UV-vis DRS. The optimal operating conditions of photocatalytic degradation of water pollutants were achived by changing the pH of the solution and changing the concentration of photocatalyst.
PB  - Belgrade : Institute of Technical Sciences of SASA
C3  - Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
T1  - Photocatalytic degradation of methylene blue and oxytetracycline via sol-gel synthesized pseudobrookite
SP  - 70
EP  - 70
UR  - https://hdl.handle.net/21.15107/rcub_dais_6967
ER  - 
@conference{
author = "Vasiljević, Zorka Ž. and Dojčinović, Milena and Janković Častvan, Ivona and Vujančević, Jelena and Tadić, Nenad B. and Nikolić, Maria Vesna",
year = "2019",
abstract = "Fe2TiO5 nanoparticles were synthesized by modified sol-gel method using Fe(NO3)3×9H2O and Ti(OC3H7)4 as starting reagents, oxalic acid as chilate agent and cetyltrimethylammonium bromide as surfactant. The aim of this study was to asses the photocatalytic degradaton of water pollutants, methylene blue and the antibiotic Oxytetracycline (OTC) using natural sunlight irradiation. As prepared nanoparticles were characterized by XRD, BET, FESEM and UV-vis DRS. The optimal operating conditions of photocatalytic degradation of water pollutants were achived by changing the pH of the solution and changing the concentration of photocatalyst.",
publisher = "Belgrade : Institute of Technical Sciences of SASA",
journal = "Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia",
title = "Photocatalytic degradation of methylene blue and oxytetracycline via sol-gel synthesized pseudobrookite",
pages = "70-70",
url = "https://hdl.handle.net/21.15107/rcub_dais_6967"
}
Vasiljević, Z. Ž., Dojčinović, M., Janković Častvan, I., Vujančević, J., Tadić, N. B.,& Nikolić, M. V.. (2019). Photocatalytic degradation of methylene blue and oxytetracycline via sol-gel synthesized pseudobrookite. in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
Belgrade : Institute of Technical Sciences of SASA., 70-70.
https://hdl.handle.net/21.15107/rcub_dais_6967
Vasiljević ZŽ, Dojčinović M, Janković Častvan I, Vujančević J, Tadić NB, Nikolić MV. Photocatalytic degradation of methylene blue and oxytetracycline via sol-gel synthesized pseudobrookite. in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia. 2019;:70-70.
https://hdl.handle.net/21.15107/rcub_dais_6967 .
Vasiljević, Zorka Ž., Dojčinović, Milena, Janković Častvan, Ivona, Vujančević, Jelena, Tadić, Nenad B., Nikolić, Maria Vesna, "Photocatalytic degradation of methylene blue and oxytetracycline via sol-gel synthesized pseudobrookite" in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia (2019):70-70,
https://hdl.handle.net/21.15107/rcub_dais_6967 .

Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts

Dojčinović, Milena; Vasiljević, Zorka Ž.; Tadić, Nenad B.; Pavlović, Vera P.; Barišić, Dario; Pajić, Damir; Nikolić, Maria Vesna

(Belgrade : Institute of Technical Sciences of SASA, 2019)

TY  - CONF
AU  - Dojčinović, Milena
AU  - Vasiljević, Zorka Ž.
AU  - Tadić, Nenad B.
AU  - Pavlović, Vera P.
AU  - Barišić, Dario
AU  - Pajić, Damir
AU  - Nikolić, Maria Vesna
PY  - 2019
UR  - https://dais.sanu.ac.rs/123456789/6963
AB  - Cobalt/magnesium ferrites with various mole percentage ratio of the metals (obtained structures are CoxMg1-xFe2O4 with x being 0, 0.1, 0.3, 0.5, 0.7, 0.9, 1.0) were synthesized by sol-gel combustion synthesis using glycine as fuel, following the rules of propellant chemistry. The powders were then sintered at 700 °C for 3 hours. Obtained powders were characterized by X-Ray diffraction (XRD), scanning electron microscopy (SEM), Raman
spectroscopy, UV/vis diffuse reflectance spectroscopy (DRS). Investigation of the magnetic properties was also conducted by vibrating sample magnetometry (VSM). The obtained powders were proved to be phase-pure cubic spinels which formed agglomerated micrograins. Series of photocatalytic experiments of methylene blue degradation were done.
The influence of different experimental conditions was investigated including variations of: pH values, concentrations of the pollutant, masses of the photocatalyst, different light sources and therefore different light irradiation. Interesting results, including enhancement of the degradation rate with the introduction of cobalt into MgFe2O4 and decrease of the degradation rate with further increase of cobalt content and formation of hard agglomerates, open new possibilities for further investigation of the utilisation of Co/Mg ferrites as photocatalysts.
PB  - Belgrade : Institute of Technical Sciences of SASA
C3  - Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
T1  - Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts
SP  - 71
EP  - 71
UR  - https://hdl.handle.net/21.15107/rcub_dais_6963
ER  - 
@conference{
author = "Dojčinović, Milena and Vasiljević, Zorka Ž. and Tadić, Nenad B. and Pavlović, Vera P. and Barišić, Dario and Pajić, Damir and Nikolić, Maria Vesna",
year = "2019",
abstract = "Cobalt/magnesium ferrites with various mole percentage ratio of the metals (obtained structures are CoxMg1-xFe2O4 with x being 0, 0.1, 0.3, 0.5, 0.7, 0.9, 1.0) were synthesized by sol-gel combustion synthesis using glycine as fuel, following the rules of propellant chemistry. The powders were then sintered at 700 °C for 3 hours. Obtained powders were characterized by X-Ray diffraction (XRD), scanning electron microscopy (SEM), Raman
spectroscopy, UV/vis diffuse reflectance spectroscopy (DRS). Investigation of the magnetic properties was also conducted by vibrating sample magnetometry (VSM). The obtained powders were proved to be phase-pure cubic spinels which formed agglomerated micrograins. Series of photocatalytic experiments of methylene blue degradation were done.
The influence of different experimental conditions was investigated including variations of: pH values, concentrations of the pollutant, masses of the photocatalyst, different light sources and therefore different light irradiation. Interesting results, including enhancement of the degradation rate with the introduction of cobalt into MgFe2O4 and decrease of the degradation rate with further increase of cobalt content and formation of hard agglomerates, open new possibilities for further investigation of the utilisation of Co/Mg ferrites as photocatalysts.",
publisher = "Belgrade : Institute of Technical Sciences of SASA",
journal = "Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia",
title = "Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts",
pages = "71-71",
url = "https://hdl.handle.net/21.15107/rcub_dais_6963"
}
Dojčinović, M., Vasiljević, Z. Ž., Tadić, N. B., Pavlović, V. P., Barišić, D., Pajić, D.,& Nikolić, M. V.. (2019). Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts. in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
Belgrade : Institute of Technical Sciences of SASA., 71-71.
https://hdl.handle.net/21.15107/rcub_dais_6963
Dojčinović M, Vasiljević ZŽ, Tadić NB, Pavlović VP, Barišić D, Pajić D, Nikolić MV. Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts. in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia. 2019;:71-71.
https://hdl.handle.net/21.15107/rcub_dais_6963 .
Dojčinović, Milena, Vasiljević, Zorka Ž., Tadić, Nenad B., Pavlović, Vera P., Barišić, Dario, Pajić, Damir, Nikolić, Maria Vesna, "Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts" in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia (2019):71-71,
https://hdl.handle.net/21.15107/rcub_dais_6963 .