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Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method

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2020
bitstream_38527.pdf (1.324Mb)
Authors
Vasiljević, Zorka Ž.
Dojčinović, Milena
Vujančević, Jelena
Janković Častvan, Ivona
Ognjanović, M.
Tadić, Nenad B.
Stojadinović, Stevan
Branković, Goran
Nikolić, Maria Vesna
Article (Published version)
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Abstract
The aim of this work was to synthesize semiconducting oxide nanoparticles using a simple method with low production cost to be applied in natural sunlight for photocatalytic degradation of pollutants in waste water. Iron titanate (Fe2TiO5) nanoparticles with an orthorhombic structure were successfully synthesized using a modified sol–gel method and calcination at 750°C. The as-prepared Fe2TiO5 nanoparticles exhibited a moderate specific surface area. The mesoporous Fe2TiO5 nanoparticles possessed strong absorption in the visible-light region and the band gap was estimated to be around 2.16 eV. The photocatalytic activity was evaluated by the degradation of methylene blue under natural sunlight. The effect of parameters such as the amount of catalyst, initial concentration of the dye and pH of the dye solution on the removal efficiency of methylene blue was investigated. Fe2TiO5 showed high degradation efficiency in a strong alkaline medium that can be the result of the facilitated form...ation of OH radicals due to an increased concentration of hydroxyl ions.

Keywords:
photocatalytic degradation / methylene blue dye / sol–gel method / dye waste water / iron titanate
Source:
Royal Society Open Science, 2020, 7, 9
Publisher:
  • Royal Society
Funding / projects:
  • Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 200175 (Institute of Technical Sciences of SASA, Belgrade) (RS-200175)
  • Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 200053 (University of Belgrade, Institute for Multidisciplinary Research) (RS-200053)
  • Bilateral collaboration between Serbia and Slovenia (BI-RS-18-19-026)
Note:
  • Supplementary material: Material characterization results and methylene blue aqueous solution degradation data https://doi.org/10.5061/dryad.69p8cz8z5
  • Supplementary material: https://doi.org/10.6084/m9.figshare.c.5105934

DOI: 10.1098/rsos.200708

ISSN: 2054-5703

WoS: 000568902100001

[ Google Scholar ]
20
Handle
https://hdl.handle.net/21.15107/rcub_dais_9107
URI
https://dais.sanu.ac.rs/123456789/9107
Collections
  • ИТН САНУ - Општа колекција / ITS SASA - General collection
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - JOUR
AU  - Vasiljević, Zorka Ž.
AU  - Dojčinović, Milena
AU  - Vujančević, Jelena
AU  - Janković Častvan, Ivona
AU  - Ognjanović, M.
AU  - Tadić, Nenad B.
AU  - Stojadinović, Stevan
AU  - Branković, Goran
AU  - Nikolić, Maria Vesna
PY  - 2020
UR  - https://dais.sanu.ac.rs/123456789/9107
AB  - The aim of this work was to synthesize semiconducting oxide nanoparticles using a simple method with low production cost to be applied in natural sunlight for photocatalytic degradation of pollutants in waste water. Iron titanate (Fe2TiO5) nanoparticles with an orthorhombic structure were successfully synthesized using a modified sol–gel method and calcination at 750°C. The as-prepared Fe2TiO5 nanoparticles exhibited a moderate specific surface area. The mesoporous Fe2TiO5 nanoparticles possessed strong absorption in the visible-light region and the band gap was estimated to be around 2.16 eV. The photocatalytic activity was evaluated by the degradation of methylene blue under natural sunlight. The effect of parameters such as the amount of catalyst, initial concentration of the dye and pH of the dye solution on the removal efficiency of methylene blue was investigated. Fe2TiO5 showed high degradation efficiency in a strong alkaline medium that can be the result of the facilitated formation of OH radicals due to an increased concentration of hydroxyl ions.
PB  - Royal Society
T2  - Royal Society Open Science
T1  - Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method
VL  - 7
IS  - 9
DO  - 10.1098/rsos.200708
UR  - https://hdl.handle.net/21.15107/rcub_dais_9107
ER  - 
@article{
author = "Vasiljević, Zorka Ž. and Dojčinović, Milena and Vujančević, Jelena and Janković Častvan, Ivona and Ognjanović, M. and Tadić, Nenad B. and Stojadinović, Stevan and Branković, Goran and Nikolić, Maria Vesna",
year = "2020",
abstract = "The aim of this work was to synthesize semiconducting oxide nanoparticles using a simple method with low production cost to be applied in natural sunlight for photocatalytic degradation of pollutants in waste water. Iron titanate (Fe2TiO5) nanoparticles with an orthorhombic structure were successfully synthesized using a modified sol–gel method and calcination at 750°C. The as-prepared Fe2TiO5 nanoparticles exhibited a moderate specific surface area. The mesoporous Fe2TiO5 nanoparticles possessed strong absorption in the visible-light region and the band gap was estimated to be around 2.16 eV. The photocatalytic activity was evaluated by the degradation of methylene blue under natural sunlight. The effect of parameters such as the amount of catalyst, initial concentration of the dye and pH of the dye solution on the removal efficiency of methylene blue was investigated. Fe2TiO5 showed high degradation efficiency in a strong alkaline medium that can be the result of the facilitated formation of OH radicals due to an increased concentration of hydroxyl ions.",
publisher = "Royal Society",
journal = "Royal Society Open Science",
title = "Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method",
volume = "7",
number = "9",
doi = "10.1098/rsos.200708",
url = "https://hdl.handle.net/21.15107/rcub_dais_9107"
}
Vasiljević, Z. Ž., Dojčinović, M., Vujančević, J., Janković Častvan, I., Ognjanović, M., Tadić, N. B., Stojadinović, S., Branković, G.,& Nikolić, M. V.. (2020). Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method. in Royal Society Open Science
Royal Society., 7(9).
https://doi.org/10.1098/rsos.200708
https://hdl.handle.net/21.15107/rcub_dais_9107
Vasiljević ZŽ, Dojčinović M, Vujančević J, Janković Častvan I, Ognjanović M, Tadić NB, Stojadinović S, Branković G, Nikolić MV. Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method. in Royal Society Open Science. 2020;7(9).
doi:10.1098/rsos.200708
https://hdl.handle.net/21.15107/rcub_dais_9107 .
Vasiljević, Zorka Ž., Dojčinović, Milena, Vujančević, Jelena, Janković Častvan, Ivona, Ognjanović, M., Tadić, Nenad B., Stojadinović, Stevan, Branković, Goran, Nikolić, Maria Vesna, "Photocatalytic degradation of methylene blue under natural sunlight using iron titanate nanoparticles prepared by a modified sol–gel method" in Royal Society Open Science, 7, no. 9 (2020),
https://doi.org/10.1098/rsos.200708 .,
https://hdl.handle.net/21.15107/rcub_dais_9107 .

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