Characterisation of Mn0.63Zn0.37Fe2O4 powders after intensive milling and subsequent thermal treatment

2016
Authors
Labus, Nebojša
Vasiljević, Zorka Ž.

Aleksić, Obrad S.
Vuković, Miloljub
Marković, Smilja

Pavlović, Vladimir B.

Mentus, Slavko

Nikolić, Maria Vesna

Conference object (Published version)
Metadata
Show full item recordAbstract
Commercial Mn-Zn powder (Mn0.63Zn0.37Fe2O4, 93 wt. % and Fe2O3 7 wt. %) was milled 0.5, 1, 2 and 4 hours in a planetary ball mill. Powders were characterized with XRD, SEM and particle seizer. Subsequent heating was monitored on TGA/DTA in air atmosphere. After compaction of the milled powders, sintering was also performed in a dilatometric device. Sintered specimens were characterized microstructurally with SEM on a fresh breakage. Ferrite powders changed with milling as well as with second run heating are characterised to approach the possible best ratio of the milling and heating that should be used to obtain desired micrstructure.
Keywords:
Mn0.63Zn0.37Fe2O4 powders / milling / mechanochemistry / sinteringSource:
Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts : V Serbian Ceramic Society Conference, Sep 21-23 September 2016, Belgrade, 2016, 48-48Publisher:
- Belgrade : Serbian Ceramic Society
Funding / projects:
- Lithium-ion batteries and fuel cells - research and development (RS-45014)
- Directed synthesis, structure and properties of multifunctional materials (RS-172057)
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - CONF AU - Labus, Nebojša AU - Vasiljević, Zorka Ž. AU - Aleksić, Obrad S. AU - Vuković, Miloljub AU - Marković, Smilja AU - Pavlović, Vladimir B. AU - Mentus, Slavko AU - Nikolić, Maria Vesna PY - 2016 UR - https://dais.sanu.ac.rs/123456789/869 AB - Commercial Mn-Zn powder (Mn0.63Zn0.37Fe2O4, 93 wt. % and Fe2O3 7 wt. %) was milled 0.5, 1, 2 and 4 hours in a planetary ball mill. Powders were characterized with XRD, SEM and particle seizer. Subsequent heating was monitored on TGA/DTA in air atmosphere. After compaction of the milled powders, sintering was also performed in a dilatometric device. Sintered specimens were characterized microstructurally with SEM on a fresh breakage. Ferrite powders changed with milling as well as with second run heating are characterised to approach the possible best ratio of the milling and heating that should be used to obtain desired micrstructure. PB - Belgrade : Serbian Ceramic Society C3 - Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts : V Serbian Ceramic Society Conference, Sep 21-23 September 2016, Belgrade T1 - Characterisation of Mn0.63Zn0.37Fe2O4 powders after intensive milling and subsequent thermal treatment SP - 48 EP - 48 UR - https://hdl.handle.net/21.15107/rcub_dais_869 ER -
@conference{ author = "Labus, Nebojša and Vasiljević, Zorka Ž. and Aleksić, Obrad S. and Vuković, Miloljub and Marković, Smilja and Pavlović, Vladimir B. and Mentus, Slavko and Nikolić, Maria Vesna", year = "2016", abstract = "Commercial Mn-Zn powder (Mn0.63Zn0.37Fe2O4, 93 wt. % and Fe2O3 7 wt. %) was milled 0.5, 1, 2 and 4 hours in a planetary ball mill. Powders were characterized with XRD, SEM and particle seizer. Subsequent heating was monitored on TGA/DTA in air atmosphere. After compaction of the milled powders, sintering was also performed in a dilatometric device. Sintered specimens were characterized microstructurally with SEM on a fresh breakage. Ferrite powders changed with milling as well as with second run heating are characterised to approach the possible best ratio of the milling and heating that should be used to obtain desired micrstructure.", publisher = "Belgrade : Serbian Ceramic Society", journal = "Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts : V Serbian Ceramic Society Conference, Sep 21-23 September 2016, Belgrade", title = "Characterisation of Mn0.63Zn0.37Fe2O4 powders after intensive milling and subsequent thermal treatment", pages = "48-48", url = "https://hdl.handle.net/21.15107/rcub_dais_869" }
Labus, N., Vasiljević, Z. Ž., Aleksić, O. S., Vuković, M., Marković, S., Pavlović, V. B., Mentus, S.,& Nikolić, M. V.. (2016). Characterisation of Mn0.63Zn0.37Fe2O4 powders after intensive milling and subsequent thermal treatment. in Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts : V Serbian Ceramic Society Conference, Sep 21-23 September 2016, Belgrade Belgrade : Serbian Ceramic Society., 48-48. https://hdl.handle.net/21.15107/rcub_dais_869
Labus N, Vasiljević ZŽ, Aleksić OS, Vuković M, Marković S, Pavlović VB, Mentus S, Nikolić MV. Characterisation of Mn0.63Zn0.37Fe2O4 powders after intensive milling and subsequent thermal treatment. in Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts : V Serbian Ceramic Society Conference, Sep 21-23 September 2016, Belgrade. 2016;:48-48. https://hdl.handle.net/21.15107/rcub_dais_869 .
Labus, Nebojša, Vasiljević, Zorka Ž., Aleksić, Obrad S., Vuković, Miloljub, Marković, Smilja, Pavlović, Vladimir B., Mentus, Slavko, Nikolić, Maria Vesna, "Characterisation of Mn0.63Zn0.37Fe2O4 powders after intensive milling and subsequent thermal treatment" in Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts : V Serbian Ceramic Society Conference, Sep 21-23 September 2016, Belgrade (2016):48-48, https://hdl.handle.net/21.15107/rcub_dais_869 .