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Theoretical and experimental analysis of droplet-to-particle formation during aerosol processing of colloidal TiO2 nanoparticles

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2013
816.pdf (204.6Kb)
Authors
Dugandžić, Ivan
Jovanović, Dragana J.
Mančić, Lidija
Šaponjić, Zoran
Nedeljković, Jovan
Milošević, Olivera
Conference object (Published version)
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Abstract
Theoretical and experimental investigation of the particle formation during processing of colloidal nanoparticles in aerosol laminar flow reactor is presented. Simple analytical model taking into consideration all important process parameters, such as physico-chemical properties of the colloidal solution, initial droplet size, residence time and temperature, is developed in order to predict the final particle morphology. The formation of spherical, hierarchically organized, ~450 nm sized TiO2 particles has been followed at 150°C starting from colloidal TiO2 nanoparticle (~4.5 nm) solution as precursor. It has been shown that the final particle morphology is formed in the evaporation/drying stage through the self assembly processes of colloidal nanoparticles collision and aggregation. The dimensionless numbers Re, Nu, Pr and Bi, were used in modeling to briefly describe the transport properties in dispersed system and heat and mass transport phenomena. The predicted particle size and mo...rphology is confirmed by using scanning electron microscopy (SEM/FESEM) and laser diffraction particle size analyzer (LPS). Additionally, closer morphological investigation is performed with transmission electron microscopy (TEM) and nanotomography. Correspondingly, theoretical analysis under this study presents a simple procedure to predict the final morphology and mean particle size during aerosol processing.

Keywords:
TiO2 / colloidal nanoparticles / aerosol
Source:
EUROMAT 2013: European Congress and Exhibition on Advanced Materials and Processes, Sevilla 8-13, October, 2013: CD Book of Abstracts, 2013
Publisher:
  • Sevilla : FEMS
Projects:
  • Materials of Reduced Dimensions for Efficient Light Harvesting and Energy conversion (RS-45020)
[ Google Scholar ]
URI
http://dais.sanu.ac.rs/123456789/819
Collections
  • ITN SANU - Opšta kolekcija / ITS SASA - General collection
Institution
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - CONF
AU  - Dugandžić, Ivan
AU  - Jovanović, Dragana J.
AU  - Mančić, Lidija
AU  - Šaponjić, Zoran
AU  - Nedeljković, Jovan
AU  - Milošević, Olivera
PY  - 2013
UR  - http://dais.sanu.ac.rs/123456789/819
AB  - Theoretical and experimental investigation of the particle formation during processing of colloidal nanoparticles in aerosol laminar flow reactor is presented. Simple analytical model taking into consideration all important process parameters, such as physico-chemical properties of the colloidal solution, initial droplet size, residence time and temperature, is developed in order to predict the final particle morphology. The formation of spherical, hierarchically organized, ~450 nm sized TiO2 particles has been followed at 150°C starting from colloidal TiO2 nanoparticle (~4.5 nm) solution as precursor. It has been shown that the final particle morphology is formed in the evaporation/drying stage through the self assembly processes of colloidal nanoparticles collision and aggregation. The dimensionless numbers Re, Nu, Pr and Bi, were used in modeling to briefly describe the transport properties in dispersed system and heat and mass transport phenomena. The predicted particle size and morphology is confirmed by using scanning electron microscopy (SEM/FESEM) and laser diffraction particle size analyzer (LPS). Additionally, closer morphological investigation is performed with transmission electron microscopy (TEM) and nanotomography. Correspondingly, theoretical analysis under this study presents a simple procedure to predict the final morphology and mean particle size during aerosol processing.
PB  - Sevilla : FEMS
C3  - EUROMAT 2013: European Congress and Exhibition on Advanced Materials and Processes, Sevilla 8-13, October, 2013: CD Book of Abstracts
T1  - Theoretical and experimental analysis of droplet-to-particle formation during aerosol processing of colloidal TiO2 nanoparticles
ER  - 
@conference{
author = "Dugandžić, Ivan and Jovanović, Dragana J. and Mančić, Lidija and Šaponjić, Zoran and Nedeljković, Jovan and Milošević, Olivera",
year = "2013",
url = "http://dais.sanu.ac.rs/123456789/819",
abstract = "Theoretical and experimental investigation of the particle formation during processing of colloidal nanoparticles in aerosol laminar flow reactor is presented. Simple analytical model taking into consideration all important process parameters, such as physico-chemical properties of the colloidal solution, initial droplet size, residence time and temperature, is developed in order to predict the final particle morphology. The formation of spherical, hierarchically organized, ~450 nm sized TiO2 particles has been followed at 150°C starting from colloidal TiO2 nanoparticle (~4.5 nm) solution as precursor. It has been shown that the final particle morphology is formed in the evaporation/drying stage through the self assembly processes of colloidal nanoparticles collision and aggregation. The dimensionless numbers Re, Nu, Pr and Bi, were used in modeling to briefly describe the transport properties in dispersed system and heat and mass transport phenomena. The predicted particle size and morphology is confirmed by using scanning electron microscopy (SEM/FESEM) and laser diffraction particle size analyzer (LPS). Additionally, closer morphological investigation is performed with transmission electron microscopy (TEM) and nanotomography. Correspondingly, theoretical analysis under this study presents a simple procedure to predict the final morphology and mean particle size during aerosol processing.",
publisher = "Sevilla : FEMS",
journal = "EUROMAT 2013: European Congress and Exhibition on Advanced Materials and Processes, Sevilla 8-13, October, 2013: CD Book of Abstracts",
title = "Theoretical and experimental analysis of droplet-to-particle formation during aerosol processing of colloidal TiO2 nanoparticles"
}
Dugandžić I, Jovanović DJ, Mančić L, Šaponjić Z, Nedeljković J, Milošević O. Theoretical and experimental analysis of droplet-to-particle formation during aerosol processing of colloidal TiO2 nanoparticles. EUROMAT 2013: European Congress and Exhibition on Advanced Materials and Processes, Sevilla 8-13, October, 2013: CD Book of Abstracts. 2013;
Dugandžić, I., Jovanović, D. J., Mančić, L., Šaponjić, Z., Nedeljković, J.,& Milošević, O. (2013). Theoretical and experimental analysis of droplet-to-particle formation during aerosol processing of colloidal TiO2 nanoparticles.
EUROMAT 2013: European Congress and Exhibition on Advanced Materials and Processes, Sevilla 8-13, October, 2013: CD Book of AbstractsSevilla : FEMS., null. 
Dugandžić Ivan, Jovanović Dragana J., Mančić Lidija, Šaponjić Zoran, Nedeljković Jovan, Milošević Olivera, "Theoretical and experimental analysis of droplet-to-particle formation during aerosol processing of colloidal TiO2 nanoparticles" null (2013)

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