Thermal, morphological and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process

2013
Authors
Lević, Steva
Obradović, Nina

Pavlović, Vladimir B.

Isailović, Bojana
Kostić, Ivana
Bugarski, Branko

Nedović, Viktor

Conference object (Published version)
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In this study, polyvinyl alcohol (PVA) nanofibers with ethyl vanillin as active compound were prepared using electrospinning technique. The final products of electrospinning process were in the form of films consist of nanofibers. PVNethyl vanillin nanofibers, having fibers diameters in the range 100-1700 nm, were successfully electrospun from ethanol/water mixture of PVA and ethyl vanillin. The effects of immobilization process on ethyl vanillin thermal properties were investigated by differential scanning calorimetry (DSC). The results of DSC showed significant influence of immobilization process on thermal properties of ethyl vanillin. It was noticed that melting point of immobilized ethyl vanillin was lower (~55°C) compared to free flavor (~77°C). Our results showed that films based on PVNethyl vanillin nanofibers are mechanically stable.
Keywords:
electrospinning / ethyl vanillin / polyvinyl alcohol / differential scanning calorimetrySource:
2nd Central and Eastern European Conference on Thermal Analysis and Calorimetry 27-30 August 2013, Vilnius, Lithuania: Book of Abstracts, 2013, 294-294Publisher:
- Vilnus : Central and Eastern European Committee for Thermal Analysis and Calorimetry
Funding / projects:
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - CONF AU - Lević, Steva AU - Obradović, Nina AU - Pavlović, Vladimir B. AU - Isailović, Bojana AU - Kostić, Ivana AU - Bugarski, Branko AU - Nedović, Viktor PY - 2013 UR - https://dais.sanu.ac.rs/123456789/759 AB - In this study, polyvinyl alcohol (PVA) nanofibers with ethyl vanillin as active compound were prepared using electrospinning technique. The final products of electrospinning process were in the form of films consist of nanofibers. PVNethyl vanillin nanofibers, having fibers diameters in the range 100-1700 nm, were successfully electrospun from ethanol/water mixture of PVA and ethyl vanillin. The effects of immobilization process on ethyl vanillin thermal properties were investigated by differential scanning calorimetry (DSC). The results of DSC showed significant influence of immobilization process on thermal properties of ethyl vanillin. It was noticed that melting point of immobilized ethyl vanillin was lower (~55°C) compared to free flavor (~77°C). Our results showed that films based on PVNethyl vanillin nanofibers are mechanically stable. PB - Vilnus : Central and Eastern European Committee for Thermal Analysis and Calorimetry C3 - 2nd Central and Eastern European Conference on Thermal Analysis and Calorimetry 27-30 August 2013, Vilnius, Lithuania: Book of Abstracts T1 - Thermal, morphological and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process SP - 294 EP - 294 UR - https://hdl.handle.net/21.15107/rcub_dais_759 ER -
@conference{ author = "Lević, Steva and Obradović, Nina and Pavlović, Vladimir B. and Isailović, Bojana and Kostić, Ivana and Bugarski, Branko and Nedović, Viktor", year = "2013", abstract = "In this study, polyvinyl alcohol (PVA) nanofibers with ethyl vanillin as active compound were prepared using electrospinning technique. The final products of electrospinning process were in the form of films consist of nanofibers. PVNethyl vanillin nanofibers, having fibers diameters in the range 100-1700 nm, were successfully electrospun from ethanol/water mixture of PVA and ethyl vanillin. The effects of immobilization process on ethyl vanillin thermal properties were investigated by differential scanning calorimetry (DSC). The results of DSC showed significant influence of immobilization process on thermal properties of ethyl vanillin. It was noticed that melting point of immobilized ethyl vanillin was lower (~55°C) compared to free flavor (~77°C). Our results showed that films based on PVNethyl vanillin nanofibers are mechanically stable.", publisher = "Vilnus : Central and Eastern European Committee for Thermal Analysis and Calorimetry", journal = "2nd Central and Eastern European Conference on Thermal Analysis and Calorimetry 27-30 August 2013, Vilnius, Lithuania: Book of Abstracts", title = "Thermal, morphological and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process", pages = "294-294", url = "https://hdl.handle.net/21.15107/rcub_dais_759" }
Lević, S., Obradović, N., Pavlović, V. B., Isailović, B., Kostić, I., Bugarski, B.,& Nedović, V.. (2013). Thermal, morphological and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process. in 2nd Central and Eastern European Conference on Thermal Analysis and Calorimetry 27-30 August 2013, Vilnius, Lithuania: Book of Abstracts Vilnus : Central and Eastern European Committee for Thermal Analysis and Calorimetry., 294-294. https://hdl.handle.net/21.15107/rcub_dais_759
Lević S, Obradović N, Pavlović VB, Isailović B, Kostić I, Bugarski B, Nedović V. Thermal, morphological and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process. in 2nd Central and Eastern European Conference on Thermal Analysis and Calorimetry 27-30 August 2013, Vilnius, Lithuania: Book of Abstracts. 2013;:294-294. https://hdl.handle.net/21.15107/rcub_dais_759 .
Lević, Steva, Obradović, Nina, Pavlović, Vladimir B., Isailović, Bojana, Kostić, Ivana, Bugarski, Branko, Nedović, Viktor, "Thermal, morphological and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process" in 2nd Central and Eastern European Conference on Thermal Analysis and Calorimetry 27-30 August 2013, Vilnius, Lithuania: Book of Abstracts (2013):294-294, https://hdl.handle.net/21.15107/rcub_dais_759 .