DAIS - Digital Archive of the Serbian Academy of Sciences and Arts
    • English
    • Српски
    • Српски (Serbia)
  • English 
    • English
    • Serbian (Cyrilic)
    • Serbian (Latin)
  • Login
View Item 
  •   DAIS
  • Институт техничких наука САНУ / Institute of Technical Sciences of SASA
  • ITN SANU - Opšta kolekcija / ITS SASA - General collection
  • View Item
  •   DAIS
  • Институт техничких наука САНУ / Institute of Technical Sciences of SASA
  • ITN SANU - Opšta kolekcija / ITS SASA - General collection
  • View Item
JavaScript is disabled for your browser. Some features of this site may not work without it.

Influence of thermal treatment on structural, morphological and optical characteristics of upconvertors

Thumbnail
2011
692.pdf (70.37Kb)
Authors
Lojpur, Vesna
Mančić, Lidija
Rabanal, Maria Eugenia
Dramićanin, Miroslav
Milošević, Olivera
Conference object (Published version)
Metadata
Show full item record
Abstract
The upconverting phosphors are materials of great interest for optoelectronics operating in the near infrared region. The preparation of highly spherical Y2O3:Yb,Er particles are synthesized via spray pyrolysis from common nitrate solution with fixed dopants ratio of Yb/Er=10. The processing conditions are as follows: precursor concentration 0.1M, atomization frequency 1.3 MHz, temperature regime 200-900-900°C and air flow rate 1,6 dm3/min. The as-prepared particles collected in the electrostatic precipitator are additionally thermally treated at 1100 °C for 12, 24 and 48 hours. Detailed structural analyses are performed by X-ray powder diffraction (XRPD) based on which the structural refinement is done using Topas Academic Software. The results imply that with the increase of calcination time crystallite size increasing along with microstrain diminishing. The particle morphological characteristics are studied by scanning electron microscopy (SEM) and are further correlated with specif...ic surface area (BET), size distribution (LPS) and optical properties followed through photoluminescence measurements (PL).

Keywords:
upconvertors / phosphor / Y2O3:Yb,Er / spray pyrolysis
Source:
Program and the Book of Abstracts / Tenth Young Researchers' Conference Materials Science and Engineering, December 21-23, 2011, Belgrade, Serbia, 2011, 38-38
Publisher:
  • Belgrade : Institute of Technical Sciences of the Serbian Academy of Sciences and Arts
Projects:
  • Materials of Reduced Dimensions for Efficient Light Harvesting and Energy conversion (RS-45020)

ISBN: 9788680321271

[ Google Scholar ]
URI
http://dais.sanu.ac.rs/123456789/695
Collections
  • ITN SANU - Opšta kolekcija / ITS SASA - General collection
Institution
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - CONF
AU  - Lojpur, Vesna
AU  - Mančić, Lidija
AU  - Rabanal, Maria Eugenia
AU  - Dramićanin, Miroslav
AU  - Milošević, Olivera
PY  - 2011
UR  - http://dais.sanu.ac.rs/123456789/695
AB  - The upconverting phosphors are materials of great interest for optoelectronics operating in the near infrared region. The preparation of highly spherical Y2O3:Yb,Er particles are synthesized via spray pyrolysis from common nitrate solution with fixed dopants ratio of Yb/Er=10. The processing conditions are as follows: precursor concentration 0.1M, atomization frequency 1.3 MHz, temperature regime 200-900-900°C and air flow rate 1,6 dm3/min. The as-prepared particles collected in the electrostatic precipitator are additionally thermally treated at 1100 °C for 12, 24 and 48 hours. Detailed structural analyses are performed by X-ray powder diffraction (XRPD) based on which the structural refinement is done using Topas Academic Software. The results imply that with the increase of calcination time crystallite size increasing along with microstrain diminishing. The particle morphological characteristics are studied by scanning electron microscopy (SEM) and are further correlated with specific surface area (BET), size distribution (LPS) and optical properties followed through photoluminescence measurements (PL).
PB  - Belgrade : Institute of Technical Sciences of the Serbian Academy of Sciences and Arts
C3  - Program and the Book of Abstracts / Tenth Young Researchers' Conference Materials Science and Engineering, December 21-23, 2011, Belgrade, Serbia
T1  - Influence of thermal treatment on structural, morphological and optical characteristics of upconvertors
SP  - 38
EP  - 38
ER  - 
@conference{
author = "Lojpur, Vesna and Mančić, Lidija and Rabanal, Maria Eugenia and Dramićanin, Miroslav and Milošević, Olivera",
year = "2011",
url = "http://dais.sanu.ac.rs/123456789/695",
abstract = "The upconverting phosphors are materials of great interest for optoelectronics operating in the near infrared region. The preparation of highly spherical Y2O3:Yb,Er particles are synthesized via spray pyrolysis from common nitrate solution with fixed dopants ratio of Yb/Er=10. The processing conditions are as follows: precursor concentration 0.1M, atomization frequency 1.3 MHz, temperature regime 200-900-900°C and air flow rate 1,6 dm3/min. The as-prepared particles collected in the electrostatic precipitator are additionally thermally treated at 1100 °C for 12, 24 and 48 hours. Detailed structural analyses are performed by X-ray powder diffraction (XRPD) based on which the structural refinement is done using Topas Academic Software. The results imply that with the increase of calcination time crystallite size increasing along with microstrain diminishing. The particle morphological characteristics are studied by scanning electron microscopy (SEM) and are further correlated with specific surface area (BET), size distribution (LPS) and optical properties followed through photoluminescence measurements (PL).",
publisher = "Belgrade : Institute of Technical Sciences of the Serbian Academy of Sciences and Arts",
journal = "Program and the Book of Abstracts / Tenth Young Researchers' Conference Materials Science and Engineering, December 21-23, 2011, Belgrade, Serbia",
title = "Influence of thermal treatment on structural, morphological and optical characteristics of upconvertors",
pages = "38-38"
}
Lojpur V, Mančić L, Rabanal ME, Dramićanin M, Milošević O. Influence of thermal treatment on structural, morphological and optical characteristics of upconvertors. Program and the Book of Abstracts / Tenth Young Researchers' Conference Materials Science and Engineering, December 21-23, 2011, Belgrade, Serbia. 2011;:38-38
Lojpur, V., Mančić, L., Rabanal, M. E., Dramićanin, M.,& Milošević, O. (2011). Influence of thermal treatment on structural, morphological and optical characteristics of upconvertors.
Program and the Book of Abstracts / Tenth Young Researchers' Conference Materials Science and Engineering, December 21-23, 2011, Belgrade, SerbiaBelgrade : Institute of Technical Sciences of the Serbian Academy of Sciences and Arts., null, 38-38. 
Lojpur Vesna, Mančić Lidija, Rabanal Maria Eugenia, Dramićanin Miroslav, Milošević Olivera, "Influence of thermal treatment on structural, morphological and optical characteristics of upconvertors" null (2011):38-38

DSpace software copyright © 2002-2015  DuraSpace
About DAIS - Digital Archive of the Serbian Academy of Sciences and Arts | Send Feedback

re3dataOpenAIRERCUB
 

 

All of DSpaceInstitutionsAuthorsTitlesSubjectsThis institutionAuthorsTitlesSubjects

Statistics

View Usage Statistics

DSpace software copyright © 2002-2015  DuraSpace
About DAIS - Digital Archive of the Serbian Academy of Sciences and Arts | Send Feedback

re3dataOpenAIRERCUB