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Synthesis of the Nanostructured YAP:Ce via Spray Pyrolysis by Polymeric Precursor Solution
dc.creator | Lojpur, Vesna | |
dc.creator | Mančić, Lidija | |
dc.creator | Rabanal, Maria Eugenia | |
dc.creator | Milošević, Olivera | |
dc.date.accessioned | 2017-06-10T15:45:07Z | |
dc.date.issued | 2011 | |
dc.identifier.uri | https://dais.sanu.ac.rs/123456789/682 | |
dc.description.abstract | The yttrium aluminum system (Y2O3-Al2O3) includes three compounds: yttrium aluminum garnet (Y3Al5O12, YAG), yttrium aluminum perovskite (YAlO3, YAP) and yttrium aluminum monoclinic (Y4Al2O9, YAM). YAP doped with Ce is well known optical material used as a fast scintillator for synchrotron X-ray experiments. Synthesizing single YAP phase is difficult even through wet chemical processing because of the possible allocations of other phases. Here, we synthesized fine powders of YAlO3:Ce3+ via spray pyrolysis of polymeric precursor obtained by dissolving the corresponding nitrates in ethylenediaminetetraacetic acid (EDTA) and ethylene glycol (EG) solution. Aerosol droplets are decomposed at 550 °C in argon atmosphere. In order to get a pure YAP:Ce phase as-prepared particles were additionally thermally treated in the range from 900 °C to 1100 °C for 12 hours in the air atmosphere. Energy dispersive analysis (EDS) confirmed high particle purity and desirable Y:Al ratio. Also, scanning electron microscopy (SEM) showed changing morphology with increasing the heating temperature. Inner particle structure is analysed by transmission electron microscopy (TEM) while phase identification is performed by X-ray powder diffraction (XRD). Detailed structural analysis is performed through Rietveld refinement in Topas Academic software. | en |
dc.format | (2011) 97-97 | |
dc.format | application/pdf | |
dc.language | en | |
dc.publisher | Belgrade : Materials Research Society of Serbia | |
dc.relation | info:eu-repo/grantAgreement/MESTD/Integrated and Interdisciplinary Research (IIR or III)/45020/RS// | |
dc.relation | info:eu-repo/grantAgreement/MESTD/Basic Research (BR or ON)/172035/RS// | |
dc.rights | openAccess | |
dc.rights.uri | https://creativecommons.org/licenses/by-nc-nd/4.0/ | |
dc.source | The Thirteenth Annual Conference YUCOMAT 2011: Programme and the Book of Abstracts | en |
dc.subject | Y2O3-Al2O3 | |
dc.subject | yttrium aluminum | |
dc.subject | spray pyrolysis | |
dc.subject | nanostructured materials | |
dc.title | Synthesis of the Nanostructured YAP:Ce via Spray Pyrolysis by Polymeric Precursor Solution | en |
dc.type | conferenceObject | |
dc.rights.license | BY-NC-ND | |
dcterms.abstract | Рабанал, Мариа Еугениа; Лојпур, Весна; Манчић, Лидија; Милошевић, Оливера; | |
dc.citation.spage | 97 | |
dc.citation.epage | 97 | |
dc.type.version | publishedVersion | |
dc.identifier.fulltext | https://dais.sanu.ac.rs/bitstream/id/21649/679.pdf | |
dc.identifier.rcub | https://hdl.handle.net/21.15107/rcub_dais_682 |