Mechanical activation as sintering pre-treatment of talc for steatite ceramics
Abstract
The effect of vibratory mill induced mechanical activation on the change of the particle size, crystallinity and the phase transformations of the minerals present in the activated material, was studied with the purpose of decreasing of the sintering temperature of talc (Mg3Si4O10(OH)2) as raw material which is the basic component of the steatite ceramics. The aims of the conducted investigation were, also, increasing of the reactivity of the comminuted raw material and establishing of the optimal activation period. The properties of the activated talc induced by mechanical force were expressed in form of the grain inertia change which was measured by means of automatic grain counter. Mechanically activated grains are the most convenient mineral form for physical concentration since the energy change of the mill-material system is recorded on them. The effect of dry grinding on the structure, particle size and shape of talc was studied by means of XRD, DTA and SEM/EDS methods. Activatio...n of talc produced an increase of the starting surface area value progressively from 4.5 m2/g up to a maximum of 108.5 m2/g achieved at 30 min. A subsequent decrease of rate of surface area change and the rate of size reduction were observed following the prolonged grinding. Talc activated in vibratory mill for optimal 30 min showed properties which positively influence the decrease of sintering temperature and the increase of the sintering rate of steatite ceramics. [Projekat Ministarstva nauke Republike Srbije, br. 172057, br. 45008 i br. 33007]
Keywords:
energy conversion / grain potential / vibratory mill / sintering / steatite ceramicsSource:
Science of Sintering, 2014, 46, 2, 247-258Publisher:
- Belgrade : Interenational Institute for the Science of Sintering
Funding / projects:
- Directed synthesis, structure and properties of multifunctional materials (RS-172057)
- Development and application of multifunctional materials using domestic raw materials in upgraded processing lines (RS-45008)
- Implementation of new technical, technological and environmental solutions in the mining and metallurgical operations RBB and RBM (RS-33007)
DOI: 10.2298/SOS1402247T
ISSN: 0350-820X (Print); 1820-7413 (Online)
WoS: 000342407800011
Scopus: 2-s2.0-84919782388
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - JOUR AU - Terzić, Anja AU - Andrić, Ljubiša AU - Stojanović, J. AU - Obradović, Nina AU - Kostović, M. PY - 2014 UR - https://dais.sanu.ac.rs/123456789/667 AB - The effect of vibratory mill induced mechanical activation on the change of the particle size, crystallinity and the phase transformations of the minerals present in the activated material, was studied with the purpose of decreasing of the sintering temperature of talc (Mg3Si4O10(OH)2) as raw material which is the basic component of the steatite ceramics. The aims of the conducted investigation were, also, increasing of the reactivity of the comminuted raw material and establishing of the optimal activation period. The properties of the activated talc induced by mechanical force were expressed in form of the grain inertia change which was measured by means of automatic grain counter. Mechanically activated grains are the most convenient mineral form for physical concentration since the energy change of the mill-material system is recorded on them. The effect of dry grinding on the structure, particle size and shape of talc was studied by means of XRD, DTA and SEM/EDS methods. Activation of talc produced an increase of the starting surface area value progressively from 4.5 m2/g up to a maximum of 108.5 m2/g achieved at 30 min. A subsequent decrease of rate of surface area change and the rate of size reduction were observed following the prolonged grinding. Talc activated in vibratory mill for optimal 30 min showed properties which positively influence the decrease of sintering temperature and the increase of the sintering rate of steatite ceramics. [Projekat Ministarstva nauke Republike Srbije, br. 172057, br. 45008 i br. 33007] PB - Belgrade : Interenational Institute for the Science of Sintering T2 - Science of Sintering T1 - Mechanical activation as sintering pre-treatment of talc for steatite ceramics SP - 247 EP - 258 VL - 46 IS - 2 DO - 10.2298/SOS1402247T UR - https://hdl.handle.net/21.15107/rcub_dais_667 ER -
@article{ author = "Terzić, Anja and Andrić, Ljubiša and Stojanović, J. and Obradović, Nina and Kostović, M.", year = "2014", abstract = "The effect of vibratory mill induced mechanical activation on the change of the particle size, crystallinity and the phase transformations of the minerals present in the activated material, was studied with the purpose of decreasing of the sintering temperature of talc (Mg3Si4O10(OH)2) as raw material which is the basic component of the steatite ceramics. The aims of the conducted investigation were, also, increasing of the reactivity of the comminuted raw material and establishing of the optimal activation period. The properties of the activated talc induced by mechanical force were expressed in form of the grain inertia change which was measured by means of automatic grain counter. Mechanically activated grains are the most convenient mineral form for physical concentration since the energy change of the mill-material system is recorded on them. The effect of dry grinding on the structure, particle size and shape of talc was studied by means of XRD, DTA and SEM/EDS methods. Activation of talc produced an increase of the starting surface area value progressively from 4.5 m2/g up to a maximum of 108.5 m2/g achieved at 30 min. A subsequent decrease of rate of surface area change and the rate of size reduction were observed following the prolonged grinding. Talc activated in vibratory mill for optimal 30 min showed properties which positively influence the decrease of sintering temperature and the increase of the sintering rate of steatite ceramics. [Projekat Ministarstva nauke Republike Srbije, br. 172057, br. 45008 i br. 33007]", publisher = "Belgrade : Interenational Institute for the Science of Sintering", journal = "Science of Sintering", title = "Mechanical activation as sintering pre-treatment of talc for steatite ceramics", pages = "247-258", volume = "46", number = "2", doi = "10.2298/SOS1402247T", url = "https://hdl.handle.net/21.15107/rcub_dais_667" }
Terzić, A., Andrić, L., Stojanović, J., Obradović, N.,& Kostović, M.. (2014). Mechanical activation as sintering pre-treatment of talc for steatite ceramics. in Science of Sintering Belgrade : Interenational Institute for the Science of Sintering., 46(2), 247-258. https://doi.org/10.2298/SOS1402247T https://hdl.handle.net/21.15107/rcub_dais_667
Terzić A, Andrić L, Stojanović J, Obradović N, Kostović M. Mechanical activation as sintering pre-treatment of talc for steatite ceramics. in Science of Sintering. 2014;46(2):247-258. doi:10.2298/SOS1402247T https://hdl.handle.net/21.15107/rcub_dais_667 .
Terzić, Anja, Andrić, Ljubiša, Stojanović, J., Obradović, Nina, Kostović, M., "Mechanical activation as sintering pre-treatment of talc for steatite ceramics" in Science of Sintering, 46, no. 2 (2014):247-258, https://doi.org/10.2298/SOS1402247T ., https://hdl.handle.net/21.15107/rcub_dais_667 .