Thermal, morphological, and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process

Lević, Steva; Obradović, Nina; Pavlović, Vladimir B.; Isailović, Bojana; Kostić, Ivana; Mitrić, Miodrag; Bugarski, Branko; Nedović, Viktor

doi:10.1007/s10973-014-4060-4

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2014

Authors

Lević, Steva

Obradović, Nina

Pavlović, Vladimir B.

Isailović, Bojana
Kostić, Ivana
Mitrić, Miodrag

Bugarski, Branko

Nedović, Viktor

Article (Published version)

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Abstract

In this study, polyvinyl alcohol (PVA) nanofibers with ethyl vanillin as an active compound were prepared using electrospinning technique. The final products of electrospinning process were in the form of nanofibers films. PVA/ethyl vanillin nanofibers, having fibers diameters in the range 100–1700 nm, were successfully electrospun from ethanol/water mixture of PVA and ethyl vanillin. The effects of immobilization process on ethyl vanillin thermal properties were investigated by differential scanning calorimetry (DSC). The results of DSC showed significant influence of immobilization process on thermal properties of ethyl vanillin. It was noticed that melting point of immobilized ethyl vanillin was lower (~55 °C) compared to free flavor (~77 °C). Our results showed that films based on PVA/ethyl vanillin nanofibers are mechanically stable.

Keywords:

polyvinyl alcohol / electrospinning / ethyl vanillin / structural analysis

Source:
Journal of Thermal Analysis and Calorimetry, 2014, 118, 2, 661-668

Publisher:

Springer

Funding / projects:

DOI: 10.1007/s10973-014-4060-4

ISSN: 1388-6150 (Print); 1588-2926 (Online)

WoS: 000344098200010

Scopus: 2-s2.0-84910121531

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	15

TY  - JOUR
AU  - Lević, Steva
AU  - Obradović, Nina
AU  - Pavlović, Vladimir B.
AU  - Isailović, Bojana
AU  - Kostić, Ivana
AU  - Mitrić, Miodrag
AU  - Bugarski, Branko
AU  - Nedović, Viktor
PY  - 2014
UR  - https://dais.sanu.ac.rs/123456789/654
AB  - In this study, polyvinyl alcohol (PVA) nanofibers with ethyl vanillin as an active compound were prepared using electrospinning technique. The final products of electrospinning process were in the form of nanofibers films. PVA/ethyl vanillin nanofibers, having fibers diameters in the range 100–1700 nm, were successfully electrospun from ethanol/water mixture of PVA and ethyl vanillin. The effects of immobilization process on ethyl vanillin thermal properties were investigated by differential scanning calorimetry (DSC). The results of DSC showed significant influence of immobilization process on thermal properties of ethyl vanillin. It was noticed that melting point of immobilized ethyl vanillin was lower (~55 °C) compared to free flavor (~77 °C). Our results showed that films based on PVA/ethyl vanillin nanofibers are mechanically stable.
PB  - Springer
T2  - Journal of Thermal Analysis and Calorimetry
T1  - Thermal, morphological, and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process
SP  - 661
EP  - 668
VL  - 118
IS  - 2
DO  - 10.1007/s10973-014-4060-4
UR  - https://hdl.handle.net/21.15107/rcub_dais_654
ER  -

@article{
author = "Lević, Steva and Obradović, Nina and Pavlović, Vladimir B. and Isailović, Bojana and Kostić, Ivana and Mitrić, Miodrag and Bugarski, Branko and Nedović, Viktor",
year = "2014",
abstract = "In this study, polyvinyl alcohol (PVA) nanofibers with ethyl vanillin as an active compound were prepared using electrospinning technique. The final products of electrospinning process were in the form of nanofibers films. PVA/ethyl vanillin nanofibers, having fibers diameters in the range 100–1700 nm, were successfully electrospun from ethanol/water mixture of PVA and ethyl vanillin. The effects of immobilization process on ethyl vanillin thermal properties were investigated by differential scanning calorimetry (DSC). The results of DSC showed significant influence of immobilization process on thermal properties of ethyl vanillin. It was noticed that melting point of immobilized ethyl vanillin was lower (~55 °C) compared to free flavor (~77 °C). Our results showed that films based on PVA/ethyl vanillin nanofibers are mechanically stable.",
publisher = "Springer",
journal = "Journal of Thermal Analysis and Calorimetry",
title = "Thermal, morphological, and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process",
pages = "661-668",
volume = "118",
number = "2",
doi = "10.1007/s10973-014-4060-4",
url = "https://hdl.handle.net/21.15107/rcub_dais_654"
}

Lević, S., Obradović, N., Pavlović, V. B., Isailović, B., Kostić, I., Mitrić, M., Bugarski, B.,& Nedović, V.. (2014). Thermal, morphological, and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process. in Journal of Thermal Analysis and Calorimetry
Springer., 118(2), 661-668.
https://doi.org/10.1007/s10973-014-4060-4
https://hdl.handle.net/21.15107/rcub_dais_654

Lević S, Obradović N, Pavlović VB, Isailović B, Kostić I, Mitrić M, Bugarski B, Nedović V. Thermal, morphological, and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process. in Journal of Thermal Analysis and Calorimetry. 2014;118(2):661-668.
doi:10.1007/s10973-014-4060-4
https://hdl.handle.net/21.15107/rcub_dais_654 .

Lević, Steva, Obradović, Nina, Pavlović, Vladimir B., Isailović, Bojana, Kostić, Ivana, Mitrić, Miodrag, Bugarski, Branko, Nedović, Viktor, "Thermal, morphological, and mechanical properties of ethyl vanillin immobilized in polyvinyl alcohol by electrospinning process" in Journal of Thermal Analysis and Calorimetry, 118, no. 2 (2014):661-668,
https://doi.org/10.1007/s10973-014-4060-4 .,
https://hdl.handle.net/21.15107/rcub_dais_654 .