Mixtures of MgO-TiO2 powders were mechanically activated in a planetary ball mill for time interval from 0 to 120 minutes. On thus obtained powders, structural investigations have been performed. N2 adsorption method was used to determine the BET specific surface area and pore size distribution. Unusual results are obtained: specific surface area continuously decreases up to 40 minutes of activation and after that increases, reaching its minimum value of 4.4 m2/g. The influence of mechanical activation on lattice vibrational spectra was examined by Raman spectroscopy at room temperatures. The differential thermal analysis has been performed in order to investigate thermal behavior of the mixtures, indicating at several endothermal peaks in range of RT to 1100oC. SEM gave information about changes in microstructures, showing the clear decrease in particle size.
Keywords:
MgO-TiO2 / mechanical activation / ball milling
Source:
The Thirteenth Annual Conference YUCOMAT 2011: Programme and the Book of Abstracts, 2011, 101-101
TY - CONF
AU - Filipović, Suzana
AU - Obradović, Nina
AU - Krstić, Jugoslav
AU - Kosanović, Darko
AU - Šćepanović, M.
AU - Pavlović, Vladimir B.
AU - Maričić, Aleksa
AU - Ristić, Momčilo M.
PY - 2011
UR - https://dais.sanu.ac.rs/123456789/629
AB - Mixtures of MgO-TiO2 powders were mechanically activated in a planetary ball mill for time interval from 0 to 120 minutes. On thus obtained powders, structural investigations have been performed. N2 adsorption method was used to determine the BET specific surface area and pore size distribution. Unusual results are obtained: specific surface area continuously decreases up to 40 minutes of activation and after that increases, reaching its minimum value of 4.4 m2/g. The influence of mechanical activation on lattice vibrational spectra was examined by Raman spectroscopy at room temperatures. The differential thermal analysis has been performed in order to investigate thermal behavior of the mixtures, indicating at several endothermal peaks in range of RT to 1100oC. SEM gave information about changes in microstructures, showing the clear decrease in particle size.
PB - Belgrade : Materials Research Society of Serbia
C3 - The Thirteenth Annual Conference YUCOMAT 2011: Programme and the Book of Abstracts
T1 - Structural characterization of mechanically activated MgO-TiO2 system
SP - 101
EP - 101
UR - https://hdl.handle.net/21.15107/rcub_dais_629
ER -
@conference{
author = "Filipović, Suzana and Obradović, Nina and Krstić, Jugoslav and Kosanović, Darko and Šćepanović, M. and Pavlović, Vladimir B. and Maričić, Aleksa and Ristić, Momčilo M.",
year = "2011",
abstract = "Mixtures of MgO-TiO2 powders were mechanically activated in a planetary ball mill for time interval from 0 to 120 minutes. On thus obtained powders, structural investigations have been performed. N2 adsorption method was used to determine the BET specific surface area and pore size distribution. Unusual results are obtained: specific surface area continuously decreases up to 40 minutes of activation and after that increases, reaching its minimum value of 4.4 m2/g. The influence of mechanical activation on lattice vibrational spectra was examined by Raman spectroscopy at room temperatures. The differential thermal analysis has been performed in order to investigate thermal behavior of the mixtures, indicating at several endothermal peaks in range of RT to 1100oC. SEM gave information about changes in microstructures, showing the clear decrease in particle size.",
publisher = "Belgrade : Materials Research Society of Serbia",
journal = "The Thirteenth Annual Conference YUCOMAT 2011: Programme and the Book of Abstracts",
title = "Structural characterization of mechanically activated MgO-TiO2 system",
pages = "101-101",
url = "https://hdl.handle.net/21.15107/rcub_dais_629"
}
Filipović, S., Obradović, N., Krstić, J., Kosanović, D., Šćepanović, M., Pavlović, V. B., Maričić, A.,& Ristić, M. M.. (2011). Structural characterization of mechanically activated MgO-TiO2 system. in The Thirteenth Annual Conference YUCOMAT 2011: Programme and the Book of Abstracts
Belgrade : Materials Research Society of Serbia., 101-101.
https://hdl.handle.net/21.15107/rcub_dais_629
Filipović S, Obradović N, Krstić J, Kosanović D, Šćepanović M, Pavlović VB, Maričić A, Ristić MM. Structural characterization of mechanically activated MgO-TiO2 system. in The Thirteenth Annual Conference YUCOMAT 2011: Programme and the Book of Abstracts. 2011;:101-101.
https://hdl.handle.net/21.15107/rcub_dais_629 .
Filipović, Suzana, Obradović, Nina, Krstić, Jugoslav, Kosanović, Darko, Šćepanović, M., Pavlović, Vladimir B., Maričić, Aleksa, Ristić, Momčilo M., "Structural characterization of mechanically activated MgO-TiO2 system" in The Thirteenth Annual Conference YUCOMAT 2011: Programme and the Book of Abstracts (2011):101-101,
https://hdl.handle.net/21.15107/rcub_dais_629 .
