Electrical Properties of Sintered Magnesium- titanate Ceramics
Abstract
Mixtures of MgO and TiO2 were mechanically activated in a planetary ball mill for different time intervals. Thus obtained powders were sintered in a furnace for 2 h at temperature of 1300 °C in air atmosphere. Raman scattering spectroscopy at room temperature has been used for characterization of sintered samples. Very similar spectra for all samples were observed, which indicate that there has been structure recovery during treatment at higher temperature. SEM analyses were performed in order to investigate effect of activation and sintering process on microstructure. Electrical measurements showed difference in dielectric constant (εr), loss tangent (tgδ) and specific resistance (ρ) as a function of time of mechanical treatment. The aim of this paper was to determine optimal parameters for materials preparation with a goal to obtain dense ceramic with appropriate characteristic.
Keywords:
MgO / TiO2 / mechanical activation / Raman scattering spectroscopy / SEMSource:
The First Serbian Ceramic Society Conference "Advanced Ceramics and Application" May 10-11, 2012: Program and the Book of Abstracts, 2012, 23-23Publisher:
- Belgrade : Serbian Ceramic Society
Funding / projects:
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - CONF AU - Filipović, Suzana AU - Obradović, Nina AU - Šćepanović, M. AU - Pavlović, Vladimir B. AU - Paunović, Vesna PY - 2012 UR - https://dais.sanu.ac.rs/123456789/503 AB - Mixtures of MgO and TiO2 were mechanically activated in a planetary ball mill for different time intervals. Thus obtained powders were sintered in a furnace for 2 h at temperature of 1300 °C in air atmosphere. Raman scattering spectroscopy at room temperature has been used for characterization of sintered samples. Very similar spectra for all samples were observed, which indicate that there has been structure recovery during treatment at higher temperature. SEM analyses were performed in order to investigate effect of activation and sintering process on microstructure. Electrical measurements showed difference in dielectric constant (εr), loss tangent (tgδ) and specific resistance (ρ) as a function of time of mechanical treatment. The aim of this paper was to determine optimal parameters for materials preparation with a goal to obtain dense ceramic with appropriate characteristic. PB - Belgrade : Serbian Ceramic Society C3 - The First Serbian Ceramic Society Conference "Advanced Ceramics and Application" May 10-11, 2012: Program and the Book of Abstracts T1 - Electrical Properties of Sintered Magnesium- titanate Ceramics SP - 23 EP - 23 UR - https://hdl.handle.net/21.15107/rcub_dais_503 ER -
@conference{ author = "Filipović, Suzana and Obradović, Nina and Šćepanović, M. and Pavlović, Vladimir B. and Paunović, Vesna", year = "2012", abstract = "Mixtures of MgO and TiO2 were mechanically activated in a planetary ball mill for different time intervals. Thus obtained powders were sintered in a furnace for 2 h at temperature of 1300 °C in air atmosphere. Raman scattering spectroscopy at room temperature has been used for characterization of sintered samples. Very similar spectra for all samples were observed, which indicate that there has been structure recovery during treatment at higher temperature. SEM analyses were performed in order to investigate effect of activation and sintering process on microstructure. Electrical measurements showed difference in dielectric constant (εr), loss tangent (tgδ) and specific resistance (ρ) as a function of time of mechanical treatment. The aim of this paper was to determine optimal parameters for materials preparation with a goal to obtain dense ceramic with appropriate characteristic.", publisher = "Belgrade : Serbian Ceramic Society", journal = "The First Serbian Ceramic Society Conference "Advanced Ceramics and Application" May 10-11, 2012: Program and the Book of Abstracts", title = "Electrical Properties of Sintered Magnesium- titanate Ceramics", pages = "23-23", url = "https://hdl.handle.net/21.15107/rcub_dais_503" }
Filipović, S., Obradović, N., Šćepanović, M., Pavlović, V. B.,& Paunović, V.. (2012). Electrical Properties of Sintered Magnesium- titanate Ceramics. in The First Serbian Ceramic Society Conference "Advanced Ceramics and Application" May 10-11, 2012: Program and the Book of Abstracts Belgrade : Serbian Ceramic Society., 23-23. https://hdl.handle.net/21.15107/rcub_dais_503
Filipović S, Obradović N, Šćepanović M, Pavlović VB, Paunović V. Electrical Properties of Sintered Magnesium- titanate Ceramics. in The First Serbian Ceramic Society Conference "Advanced Ceramics and Application" May 10-11, 2012: Program and the Book of Abstracts. 2012;:23-23. https://hdl.handle.net/21.15107/rcub_dais_503 .
Filipović, Suzana, Obradović, Nina, Šćepanović, M., Pavlović, Vladimir B., Paunović, Vesna, "Electrical Properties of Sintered Magnesium- titanate Ceramics" in The First Serbian Ceramic Society Conference "Advanced Ceramics and Application" May 10-11, 2012: Program and the Book of Abstracts (2012):23-23, https://hdl.handle.net/21.15107/rcub_dais_503 .