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Structure and photocatalytic properties of sintered TiO2 nanotube arrays

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2018
Vujancevic_Science-of-Sintering_50_1_39-50.pdf (1.093Mb)
Authors
Vujančević, Jelena
Bjelajac, Anđelika
Ćirković, Jovana
Pavlović, Vera P.
Horváth, Endre
Forró, László
Vlahović, Branislav
Mitrić, Miodrag
Janaćković, Đorđe
Pavlović, Vladimir B.
Article (Published version)
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Abstract
One-dimensional (1D) TiO2 nanotubes perpendicular to the substrate were obtained by electrochemical oxidation of titanium foil in an acid electrolyte. In order to alter the crystallinity and the morphology of films the as-anodized amorphous TiO2 nanotube films were sintered at elevated temperatures. The evolution of the morphology was visualized via scanning electron microscopy (SEM), while the crystalline structure was investigated by X-ray diffraction (XRD) and Raman spectroscopy. The chemical composition was studied by X-ray photoelectron spectroscopy (XPS). The effects of crystallinity and morphology of TiO2 nanotube (NTs) films on photocatalytic degradation of methyl orange (MO) in an aqueous solution under UV light irradiation were also investigated. The TiO2 nanotubes sintered at 650°C for 30 min had the highest degree of crystallinity and exhibited the best photocatalytic activity among the studied TiO2 nanotube films. [Project of the Serbian Ministry of Education, Science and ...Technological Development, Grant no. OI 172057 and Grant no. III 45019]

Keywords:
TiO2 / nanotubes / sintering
Source:
Science of Sintering, 2018, 50, 1, 39-50
Publisher:
  • Belgrade : ETRAN
Funding / projects:
  • Directed synthesis, structure and properties of multifunctional materials (RS-172057)
  • Synthesis, processing and applications of nanostructured multifunctional materials with defined properties (RS-45019)

DOI: 10.2298/SOS1801039V

ISSN: 0350-820X

WoS: 000429909100004

Scopus: 2-s2.0-85053939304
[ Google Scholar ]
11
9
Handle
https://hdl.handle.net/21.15107/rcub_dais_4528
URI
https://dais.sanu.ac.rs/123456789/4528
Collections
  • ИТН САНУ - Општа колекција / ITS SASA - General collection
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - JOUR
AU  - Vujančević, Jelena
AU  - Bjelajac, Anđelika
AU  - Ćirković, Jovana
AU  - Pavlović, Vera P.
AU  - Horváth, Endre
AU  - Forró, László
AU  - Vlahović, Branislav
AU  - Mitrić, Miodrag
AU  - Janaćković, Đorđe
AU  - Pavlović, Vladimir B.
PY  - 2018
UR  - https://dais.sanu.ac.rs/123456789/4528
AB  - One-dimensional (1D) TiO2 nanotubes perpendicular to the substrate were obtained by electrochemical oxidation of titanium foil in an acid electrolyte. In order to alter the crystallinity and the morphology of films the as-anodized amorphous TiO2 nanotube films were sintered at elevated temperatures. The evolution of the morphology was visualized via scanning electron microscopy (SEM), while the crystalline structure was investigated by X-ray diffraction (XRD) and Raman spectroscopy. The chemical composition was studied by X-ray photoelectron spectroscopy (XPS). The effects of crystallinity and morphology of TiO2 nanotube (NTs) films on photocatalytic degradation of methyl orange (MO) in an aqueous solution under UV light irradiation were also investigated. The TiO2 nanotubes sintered at 650°C for 30 min had the highest degree of crystallinity and exhibited the best photocatalytic activity among the studied TiO2 nanotube films. [Project of the Serbian Ministry of Education, Science and Technological Development, Grant no. OI 172057 and Grant no. III 45019]
PB  - Belgrade : ETRAN
T2  - Science of Sintering
T2  - Science of Sintering
T1  - Structure and photocatalytic properties of sintered TiO2 nanotube arrays
SP  - 39
EP  - 50
VL  - 50
IS  - 1
DO  - 10.2298/SOS1801039V
UR  - https://hdl.handle.net/21.15107/rcub_dais_4528
ER  - 
@article{
author = "Vujančević, Jelena and Bjelajac, Anđelika and Ćirković, Jovana and Pavlović, Vera P. and Horváth, Endre and Forró, László and Vlahović, Branislav and Mitrić, Miodrag and Janaćković, Đorđe and Pavlović, Vladimir B.",
year = "2018",
abstract = "One-dimensional (1D) TiO2 nanotubes perpendicular to the substrate were obtained by electrochemical oxidation of titanium foil in an acid electrolyte. In order to alter the crystallinity and the morphology of films the as-anodized amorphous TiO2 nanotube films were sintered at elevated temperatures. The evolution of the morphology was visualized via scanning electron microscopy (SEM), while the crystalline structure was investigated by X-ray diffraction (XRD) and Raman spectroscopy. The chemical composition was studied by X-ray photoelectron spectroscopy (XPS). The effects of crystallinity and morphology of TiO2 nanotube (NTs) films on photocatalytic degradation of methyl orange (MO) in an aqueous solution under UV light irradiation were also investigated. The TiO2 nanotubes sintered at 650°C for 30 min had the highest degree of crystallinity and exhibited the best photocatalytic activity among the studied TiO2 nanotube films. [Project of the Serbian Ministry of Education, Science and Technological Development, Grant no. OI 172057 and Grant no. III 45019]",
publisher = "Belgrade : ETRAN",
journal = "Science of Sintering, Science of Sintering",
title = "Structure and photocatalytic properties of sintered TiO2 nanotube arrays",
pages = "39-50",
volume = "50",
number = "1",
doi = "10.2298/SOS1801039V",
url = "https://hdl.handle.net/21.15107/rcub_dais_4528"
}
Vujančević, J., Bjelajac, A., Ćirković, J., Pavlović, V. P., Horváth, E., Forró, L., Vlahović, B., Mitrić, M., Janaćković, Đ.,& Pavlović, V. B.. (2018). Structure and photocatalytic properties of sintered TiO2 nanotube arrays. in Science of Sintering
Belgrade : ETRAN., 50(1), 39-50.
https://doi.org/10.2298/SOS1801039V
https://hdl.handle.net/21.15107/rcub_dais_4528
Vujančević J, Bjelajac A, Ćirković J, Pavlović VP, Horváth E, Forró L, Vlahović B, Mitrić M, Janaćković Đ, Pavlović VB. Structure and photocatalytic properties of sintered TiO2 nanotube arrays. in Science of Sintering. 2018;50(1):39-50.
doi:10.2298/SOS1801039V
https://hdl.handle.net/21.15107/rcub_dais_4528 .
Vujančević, Jelena, Bjelajac, Anđelika, Ćirković, Jovana, Pavlović, Vera P., Horváth, Endre, Forró, László, Vlahović, Branislav, Mitrić, Miodrag, Janaćković, Đorđe, Pavlović, Vladimir B., "Structure and photocatalytic properties of sintered TiO2 nanotube arrays" in Science of Sintering, 50, no. 1 (2018):39-50,
https://doi.org/10.2298/SOS1801039V .,
https://hdl.handle.net/21.15107/rcub_dais_4528 .

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