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Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films

Authorized Users Only
2018
Authors
Nikolić, Maria Vesna
Vasiljević, Zorka Ž.
Luković, Miloljub D.
Pavlović, Vera P.
Vujančević, Jelena
Radovanović, Milan
Krstić, Jugoslav
Vlahović, Branislav
Pavlović, Vladimir B.
Article (Published version)
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Abstract
Pseudobrookite based nanopowder was obtained by solid state synthesis of starting hematite and anatase nanopowders in the weight ratio 55:45. Structural and morphological properties were analyzed using X-ray diffraction (XRD), BET, X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, UV/Vis diffuse reflectance spectroscopy, Field emission scanning electron microscopy (FESEM) and Transmission electron microscopy (TEM) confirming the formation of nanocrystalline pseudobrookite. The obtained powder was mixed with a binder (ethyl cellulose), dispersant (α-terpinol) and adhesion agents (acetic acid and distilled water) to obtain a thick film paste. It was screen printed on alumina substrate with interdigitated PdAg electrodes and fired at 600 °C for 30 min. Formation of a porous nanocrystalline thick film structure was shown using Scanning electron microscopy (SEM), while Hall measurements enabled determination of carrier mobility. Change of impedance response in the frequency range ...42 Hz–1 MHz with humidity was analyzed at room temperature (25 °C) and 50 °C in the relative humidity range 30–90% and 40–90%, respectively. At 42 Hz, and room temperature the impedance reduced ∼28 times, while at 50 °C it reduced ∼147 times in the relative humidity range 40–90%. The sensor showed rapid response (16 s) and relatively low hysteresis (8.39% at 25 °C and 2.64% at 50 °C) showing that this is a promising material for application in humidity sensing.

Keywords:
FeTiO / humidity sensors / pseudobrookite / thick films
Source:
Sensors and Actuators B: Chemical, 2018, 277, 654-664
Publisher:
  • Elsevier
Projects:
  • Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing (RS-45007)
  • Lithium-ion batteries and fuel cells - research and development (RS-45014)

DOI: 10.1016/j.snb.2018.09.063

ISSN: 0925-4005

WoS: 000453066700081

Scopus: 2-s2.0-85053789141
[ Google Scholar ]
16
11
URI
http://www.sciencedirect.com/science/article/pii/S0925400518316836
http://dais.sanu.ac.rs/123456789/4527
Collections
  • ITN SANU - Opšta kolekcija / ITS SASA - General collection
Institution
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - JOUR
AU  - Nikolić, Maria Vesna
AU  - Vasiljević, Zorka Ž.
AU  - Luković, Miloljub D.
AU  - Pavlović, Vera P.
AU  - Vujančević, Jelena
AU  - Radovanović, Milan
AU  - Krstić, Jugoslav
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2018
UR  - http://www.sciencedirect.com/science/article/pii/S0925400518316836
UR  - http://dais.sanu.ac.rs/123456789/4527
AB  - Pseudobrookite based nanopowder was obtained by solid state synthesis of starting hematite and anatase nanopowders in the weight ratio 55:45. Structural and morphological properties were analyzed using X-ray diffraction (XRD), BET, X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, UV/Vis diffuse reflectance spectroscopy, Field emission scanning electron microscopy (FESEM) and Transmission electron microscopy (TEM) confirming the formation of nanocrystalline pseudobrookite. The obtained powder was mixed with a binder (ethyl cellulose), dispersant (α-terpinol) and adhesion agents (acetic acid and distilled water) to obtain a thick film paste. It was screen printed on alumina substrate with interdigitated PdAg electrodes and fired at 600 °C for 30 min. Formation of a porous nanocrystalline thick film structure was shown using Scanning electron microscopy (SEM), while Hall measurements enabled determination of carrier mobility. Change of impedance response in the frequency range 42 Hz–1 MHz with humidity was analyzed at room temperature (25 °C) and 50 °C in the relative humidity range 30–90% and 40–90%, respectively. At 42 Hz, and room temperature the impedance reduced ∼28 times, while at 50 °C it reduced ∼147 times in the relative humidity range 40–90%. The sensor showed rapid response (16 s) and relatively low hysteresis (8.39% at 25 °C and 2.64% at 50 °C) showing that this is a promising material for application in humidity sensing.
PB  - Elsevier
T2  - Sensors and Actuators B: Chemical
T1  - Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films
SP  - 654
EP  - 664
VL  - 277
DO  - 10.1016/j.snb.2018.09.063
ER  - 
@article{
author = "Nikolić, Maria Vesna and Vasiljević, Zorka Ž. and Luković, Miloljub D. and Pavlović, Vera P. and Vujančević, Jelena and Radovanović, Milan and Krstić, Jugoslav and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2018",
url = "http://www.sciencedirect.com/science/article/pii/S0925400518316836, http://dais.sanu.ac.rs/123456789/4527",
abstract = "Pseudobrookite based nanopowder was obtained by solid state synthesis of starting hematite and anatase nanopowders in the weight ratio 55:45. Structural and morphological properties were analyzed using X-ray diffraction (XRD), BET, X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, UV/Vis diffuse reflectance spectroscopy, Field emission scanning electron microscopy (FESEM) and Transmission electron microscopy (TEM) confirming the formation of nanocrystalline pseudobrookite. The obtained powder was mixed with a binder (ethyl cellulose), dispersant (α-terpinol) and adhesion agents (acetic acid and distilled water) to obtain a thick film paste. It was screen printed on alumina substrate with interdigitated PdAg electrodes and fired at 600 °C for 30 min. Formation of a porous nanocrystalline thick film structure was shown using Scanning electron microscopy (SEM), while Hall measurements enabled determination of carrier mobility. Change of impedance response in the frequency range 42 Hz–1 MHz with humidity was analyzed at room temperature (25 °C) and 50 °C in the relative humidity range 30–90% and 40–90%, respectively. At 42 Hz, and room temperature the impedance reduced ∼28 times, while at 50 °C it reduced ∼147 times in the relative humidity range 40–90%. The sensor showed rapid response (16 s) and relatively low hysteresis (8.39% at 25 °C and 2.64% at 50 °C) showing that this is a promising material for application in humidity sensing.",
publisher = "Elsevier",
journal = "Sensors and Actuators B: Chemical",
title = "Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films",
pages = "654-664",
volume = "277",
doi = "10.1016/j.snb.2018.09.063"
}
Nikolić MV, Vasiljević ZŽ, Luković MD, Pavlović VP, Vujančević J, Radovanović M, Krstić J, Vlahović B, Pavlović VB. Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films. Sensors and Actuators B: Chemical. 2018;277:654-664
Nikolić, M. V., Vasiljević, Z. Ž., Luković, M. D., Pavlović, V. P., Vujančević, J., Radovanović, M., Krstić, J., Vlahović, B.,& Pavlović, V. B. (2018). Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films.
Sensors and Actuators B: ChemicalElsevier., 277, 654-664. 
https://doi.org/10.1016/j.snb.2018.09.063
Nikolić Maria Vesna, Vasiljević Zorka Ž., Luković Miloljub D., Pavlović Vera P., Vujančević Jelena, Radovanović Milan, Krstić Jugoslav, Vlahović Branislav, Pavlović Vladimir B., "Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films" 277 (2018):654-664,
https://doi.org/10.1016/j.snb.2018.09.063 .

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