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Sol-gel synthesis of Li2FeSiO4/C

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2013
441.pdf (91.51Kb)
Authors
Milović, Miloš
Jugović, Dragana
Mitrić, Miodrag
Jokić, Bojan
Dominko, Robert
Uskoković, Dragan
Conference object (Published version)
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Abstract
Lithium transition-metal orthosilicates with general formula Li2MSiO4 (M = Fe, Mn, Co, etc.) have attracted a lot of interest due to their potentially high theoretical capacities arising from the possibility of the extraction of two Li-ions per formula unit. Li2FeSiO4 takes prominent position among this family of compounds due to its structural stability and natural abundance of iron. In this study, Li2FeSiO4/C composite was synthesized by simple method which involves rapid heating, short high-temperature delay, and subsequent quenching. Starting materials were Li2CO3, Fe(NO3)3·9H2O, Si(OC2H5)4 (TEOS) and water-soluble methylcellulose. Precursor preparation is based on the sol-gel processing and provides homogenous mixing at the molecular level. Structural analysis, morphology examination and electrochemical test of thus obtained powder were performed.
Keywords:
sol-gel synthesis / Li2FeSiO4 / carbon
Source:
Program and the Book of Abstracts / Twelfth Young Researchers' Conference Materials Sciences and Engineering December 11-13, 2013, Belgrade, Serbia, 2013, 31-31
Publisher:
  • Belgrade : Institute of Technical Sciences of SASA
Funding / projects:
  • Molecular designing of nanoparticles with controlled morphological and physicochemical characteristics and functional materials based on them (RS-45004)

ISBN: 9788680321288

[ Google Scholar ]
Handle
https://hdl.handle.net/21.15107/rcub_dais_444
URI
https://dais.sanu.ac.rs/123456789/444
Collections
  • ИТН САНУ - Општа колекција / ITS SASA - General collection
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - CONF
AU  - Milović, Miloš
AU  - Jugović, Dragana
AU  - Mitrić, Miodrag
AU  - Jokić, Bojan
AU  - Dominko, Robert
AU  - Uskoković, Dragan
PY  - 2013
UR  - https://dais.sanu.ac.rs/123456789/444
AB  - Lithium transition-metal orthosilicates with general formula Li2MSiO4 (M = Fe, Mn, Co, etc.) have attracted a lot of interest due to their potentially high theoretical capacities arising from the possibility of the extraction of two Li-ions per formula unit. Li2FeSiO4 takes prominent position among this family of compounds due to its structural stability and natural abundance of iron. In this study, Li2FeSiO4/C composite was synthesized by simple method which involves rapid heating, short high-temperature delay, and subsequent quenching. Starting materials were Li2CO3, Fe(NO3)3·9H2O, Si(OC2H5)4 (TEOS) and water-soluble methylcellulose. Precursor preparation is based on the sol-gel processing and provides homogenous mixing at the molecular level. Structural analysis, morphology examination and electrochemical test of thus obtained powder were performed.
PB  - Belgrade : Institute of Technical Sciences of SASA
C3  - Program and the Book of Abstracts / Twelfth Young Researchers' Conference Materials Sciences and Engineering December 11-13, 2013, Belgrade, Serbia
T1  - Sol-gel synthesis of Li2FeSiO4/C
SP  - 31
EP  - 31
UR  - https://hdl.handle.net/21.15107/rcub_dais_444
ER  - 
@conference{
author = "Milović, Miloš and Jugović, Dragana and Mitrić, Miodrag and Jokić, Bojan and Dominko, Robert and Uskoković, Dragan",
year = "2013",
abstract = "Lithium transition-metal orthosilicates with general formula Li2MSiO4 (M = Fe, Mn, Co, etc.) have attracted a lot of interest due to their potentially high theoretical capacities arising from the possibility of the extraction of two Li-ions per formula unit. Li2FeSiO4 takes prominent position among this family of compounds due to its structural stability and natural abundance of iron. In this study, Li2FeSiO4/C composite was synthesized by simple method which involves rapid heating, short high-temperature delay, and subsequent quenching. Starting materials were Li2CO3, Fe(NO3)3·9H2O, Si(OC2H5)4 (TEOS) and water-soluble methylcellulose. Precursor preparation is based on the sol-gel processing and provides homogenous mixing at the molecular level. Structural analysis, morphology examination and electrochemical test of thus obtained powder were performed.",
publisher = "Belgrade : Institute of Technical Sciences of SASA",
journal = "Program and the Book of Abstracts / Twelfth Young Researchers' Conference Materials Sciences and Engineering December 11-13, 2013, Belgrade, Serbia",
title = "Sol-gel synthesis of Li2FeSiO4/C",
pages = "31-31",
url = "https://hdl.handle.net/21.15107/rcub_dais_444"
}
Milović, M., Jugović, D., Mitrić, M., Jokić, B., Dominko, R.,& Uskoković, D.. (2013). Sol-gel synthesis of Li2FeSiO4/C. in Program and the Book of Abstracts / Twelfth Young Researchers' Conference Materials Sciences and Engineering December 11-13, 2013, Belgrade, Serbia
Belgrade : Institute of Technical Sciences of SASA., 31-31.
https://hdl.handle.net/21.15107/rcub_dais_444
Milović M, Jugović D, Mitrić M, Jokić B, Dominko R, Uskoković D. Sol-gel synthesis of Li2FeSiO4/C. in Program and the Book of Abstracts / Twelfth Young Researchers' Conference Materials Sciences and Engineering December 11-13, 2013, Belgrade, Serbia. 2013;:31-31.
https://hdl.handle.net/21.15107/rcub_dais_444 .
Milović, Miloš, Jugović, Dragana, Mitrić, Miodrag, Jokić, Bojan, Dominko, Robert, Uskoković, Dragan, "Sol-gel synthesis of Li2FeSiO4/C" in Program and the Book of Abstracts / Twelfth Young Researchers' Conference Materials Sciences and Engineering December 11-13, 2013, Belgrade, Serbia (2013):31-31,
https://hdl.handle.net/21.15107/rcub_dais_444 .

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