Structural and magnetic properties of Y1-xYbxF3 solid solution
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In this work, the polycrystalline samples Y1-xYbxF3 (x = 0.01, 0.05, 0.1, 0.25, 0.5, 0.75 and 1) were synthesized and characterized by X-ray powder diffraction and magnetic measurements. In the first stage of synthesis, mixed sesquioxides (Y1-xYbx)2O3 were obtained by ceramic technology. In the second stage, obtained mixed sesquioxides were treated with an excess of ammonium hydrogen fluoride in air at 170 °C for 20 h. In the third and last stage, Y1-xYbxF3 samples were obtained by heating the product from the second stage of synthesis at 500 °C for 3 h in an inert atmosphere. The X-ray diffraction revealed that the crystal structure of the Y1-xYbxF3 solid solution is orthorhombic (YF3 structural type). The structure refinements were done by the Rietveld full-profile method within Pnma space group. Magnetic susceptibility measurements of all samples were done in a temperature range 2-300 K by SQUID magnetometer. The relation between magnetic and structural properties was discussed.
Keywords:
Y1-xYbxF3 / magnetic properties / structural analysis / X-ray powder diffraction / crystal structureSource:
Program and the Book of Abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application VII : New Frontiers in Multifunctional Material Science and Processing, Serbia, Belgrade, 17-19 September 2018, 2018, 99-99Publisher:
- Belgrade : Serbian Ceramic Society
Funding / projects:
- Nanostructured Functional and Composite Materials in Catalytic and Sorption Processes (RS-45001)
- Magnetic and radionuclide labeled nanostructured materials for medical applications (RS-45015)
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - CONF AU - Aleksić, Jelena AU - Barudžija, Tanja AU - Mitrić, Miodrag AU - Jugović, Dragana AU - Kostić, Ljiljana PY - 2018 UR - https://dais.sanu.ac.rs/123456789/4092 AB - In this work, the polycrystalline samples Y1-xYbxF3 (x = 0.01, 0.05, 0.1, 0.25, 0.5, 0.75 and 1) were synthesized and characterized by X-ray powder diffraction and magnetic measurements. In the first stage of synthesis, mixed sesquioxides (Y1-xYbx)2O3 were obtained by ceramic technology. In the second stage, obtained mixed sesquioxides were treated with an excess of ammonium hydrogen fluoride in air at 170 °C for 20 h. In the third and last stage, Y1-xYbxF3 samples were obtained by heating the product from the second stage of synthesis at 500 °C for 3 h in an inert atmosphere. The X-ray diffraction revealed that the crystal structure of the Y1-xYbxF3 solid solution is orthorhombic (YF3 structural type). The structure refinements were done by the Rietveld full-profile method within Pnma space group. Magnetic susceptibility measurements of all samples were done in a temperature range 2-300 K by SQUID magnetometer. The relation between magnetic and structural properties was discussed. PB - Belgrade : Serbian Ceramic Society C3 - Program and the Book of Abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application VII : New Frontiers in Multifunctional Material Science and Processing, Serbia, Belgrade, 17-19 September 2018 T1 - Structural and magnetic properties of Y1-xYbxF3 solid solution SP - 99 EP - 99 UR - https://hdl.handle.net/21.15107/rcub_dais_4092 ER -
@conference{ author = "Aleksić, Jelena and Barudžija, Tanja and Mitrić, Miodrag and Jugović, Dragana and Kostić, Ljiljana", year = "2018", abstract = "In this work, the polycrystalline samples Y1-xYbxF3 (x = 0.01, 0.05, 0.1, 0.25, 0.5, 0.75 and 1) were synthesized and characterized by X-ray powder diffraction and magnetic measurements. In the first stage of synthesis, mixed sesquioxides (Y1-xYbx)2O3 were obtained by ceramic technology. In the second stage, obtained mixed sesquioxides were treated with an excess of ammonium hydrogen fluoride in air at 170 °C for 20 h. In the third and last stage, Y1-xYbxF3 samples were obtained by heating the product from the second stage of synthesis at 500 °C for 3 h in an inert atmosphere. The X-ray diffraction revealed that the crystal structure of the Y1-xYbxF3 solid solution is orthorhombic (YF3 structural type). The structure refinements were done by the Rietveld full-profile method within Pnma space group. Magnetic susceptibility measurements of all samples were done in a temperature range 2-300 K by SQUID magnetometer. The relation between magnetic and structural properties was discussed.", publisher = "Belgrade : Serbian Ceramic Society", journal = "Program and the Book of Abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application VII : New Frontiers in Multifunctional Material Science and Processing, Serbia, Belgrade, 17-19 September 2018", title = "Structural and magnetic properties of Y1-xYbxF3 solid solution", pages = "99-99", url = "https://hdl.handle.net/21.15107/rcub_dais_4092" }
Aleksić, J., Barudžija, T., Mitrić, M., Jugović, D.,& Kostić, L.. (2018). Structural and magnetic properties of Y1-xYbxF3 solid solution. in Program and the Book of Abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application VII : New Frontiers in Multifunctional Material Science and Processing, Serbia, Belgrade, 17-19 September 2018 Belgrade : Serbian Ceramic Society., 99-99. https://hdl.handle.net/21.15107/rcub_dais_4092
Aleksić J, Barudžija T, Mitrić M, Jugović D, Kostić L. Structural and magnetic properties of Y1-xYbxF3 solid solution. in Program and the Book of Abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application VII : New Frontiers in Multifunctional Material Science and Processing, Serbia, Belgrade, 17-19 September 2018. 2018;:99-99. https://hdl.handle.net/21.15107/rcub_dais_4092 .
Aleksić, Jelena, Barudžija, Tanja, Mitrić, Miodrag, Jugović, Dragana, Kostić, Ljiljana, "Structural and magnetic properties of Y1-xYbxF3 solid solution" in Program and the Book of Abstracts / Serbian Ceramic Society Conference Advanced Ceramics and Application VII : New Frontiers in Multifunctional Material Science and Processing, Serbia, Belgrade, 17-19 September 2018 (2018):99-99, https://hdl.handle.net/21.15107/rcub_dais_4092 .