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Polyacrilic Acid and Chitosan Assisted Solvothermal Synthesis of Up-converting NaYF4: Yb,Er Particles

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2018
Vukovic-ELMINA-2018.pdf (256.8Kb)
Authors
Vuković, Marina
Dinić, Ivana
Mančić, Lidija
Nikolić, Marko G.
Rabasović, Mihailo D.
Milošević, Olivera
Conference object (Published version)
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Abstract
There is a growing interest for development of a facile and reproducible approach for the synthesis of biocompatible lanthanide doped up-converting nanoparticles (UCNPs) for deep tissue imaging and targeted drug delivery. Synthesis of such particles is usually performed through the decomposition of organometallic compounds, followed either with a ligands exchange or with a biocompatible layer coating. In this work, biocompatible NaYF4:Yb,Er (17 mol% Yb; 3 mol% Er) nanoparticles were synthesized by one-pot hydrothermal processing with an assistance of chitosan (Ch) or polyacrylic acid (PAA). Obtained powders were analyzed by X-ray powder diffraction (XRPD, Bruker D8 Discovery), field emission scanning electron microscopy (FE-SEM, Zeiss, DSM 960), transmission electron microscopy (TEM, JEOL JEM 2010), Fourier transform infrared (FTIR, Thermo Scientific Nicolet 6700) and photoluminescence (PL, Spex Fluorolog with C31034 cooled photomultiplier) spectroscopy. The results showed that althou...gh both powders crystallize in the same crystal arrangement (cubic, Fm-3m), particles size, shape and optical properties are dependent on the polymer used.

Keywords:
up-conversion / solvothermal synthesis / chitosan / NaYF4:Yb,Er / polyacrylic acid
Source:
Program and Book of Abstracts / First International Conference on Electron Microscopy of Nanostructures ELMINA 2018, August 27-29, 2018, Belgrade, Serbia, 2018, 195-197
Publisher:
  • Belgrade : Serbian Academy of Sciences and Arts
Projects:
  • Rational design and synthesis of biologically active and coordination compounds and functional materials, relevant for (bio)nanotechnology (RS-172035)
[ Google Scholar ]
URI
http://dais.sanu.ac.rs/123456789/3627
Collections
  • ITN SANU - Opšta kolekcija / ITS SASA - General collection
Institution
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - CONF
AU  - Vuković, Marina
AU  - Dinić, Ivana
AU  - Mančić, Lidija
AU  - Nikolić, Marko G.
AU  - Rabasović, Mihailo D.
AU  - Milošević, Olivera
PY  - 2018
UR  - http://dais.sanu.ac.rs/123456789/3627
AB  - There is a growing interest for development of a facile and reproducible approach  for the synthesis of biocompatible lanthanide doped up-converting nanoparticles (UCNPs) for deep tissue imaging and targeted drug delivery. Synthesis of such particles is usually performed through the decomposition of organometallic compounds, followed either with a ligands exchange or with a biocompatible layer coating. In this work, biocompatible NaYF4:Yb,Er (17 mol% Yb; 3 mol% Er) nanoparticles were synthesized by one-pot hydrothermal processing with an assistance of chitosan (Ch) or polyacrylic acid (PAA). Obtained powders were analyzed by X-ray powder diffraction (XRPD, Bruker D8 Discovery), field emission scanning electron microscopy (FE-SEM, Zeiss, DSM 960), transmission electron microscopy (TEM, JEOL JEM 2010), Fourier transform infrared (FTIR, Thermo Scientific Nicolet 6700) and photoluminescence (PL, Spex Fluorolog with C31034 cooled photomultiplier) spectroscopy. The results showed that although both powders crystallize in the same crystal arrangement (cubic, Fm-3m), particles size, shape and optical properties are dependent on the polymer used.
PB  - Belgrade : Serbian Academy of Sciences and Arts
C3  - Program and Book of Abstracts / First International Conference on Electron Microscopy of Nanostructures ELMINA 2018, August 27-29, 2018, Belgrade, Serbia
T1  - Polyacrilic Acid and Chitosan Assisted Solvothermal Synthesis of Up-converting NaYF4: Yb,Er Particles
SP  - 195
EP  - 197
ER  - 
@conference{
author = "Vuković, Marina and Dinić, Ivana and Mančić, Lidija and Nikolić, Marko G. and Rabasović, Mihailo D. and Milošević, Olivera",
year = "2018",
url = "http://dais.sanu.ac.rs/123456789/3627",
abstract = "There is a growing interest for development of a facile and reproducible approach  for the synthesis of biocompatible lanthanide doped up-converting nanoparticles (UCNPs) for deep tissue imaging and targeted drug delivery. Synthesis of such particles is usually performed through the decomposition of organometallic compounds, followed either with a ligands exchange or with a biocompatible layer coating. In this work, biocompatible NaYF4:Yb,Er (17 mol% Yb; 3 mol% Er) nanoparticles were synthesized by one-pot hydrothermal processing with an assistance of chitosan (Ch) or polyacrylic acid (PAA). Obtained powders were analyzed by X-ray powder diffraction (XRPD, Bruker D8 Discovery), field emission scanning electron microscopy (FE-SEM, Zeiss, DSM 960), transmission electron microscopy (TEM, JEOL JEM 2010), Fourier transform infrared (FTIR, Thermo Scientific Nicolet 6700) and photoluminescence (PL, Spex Fluorolog with C31034 cooled photomultiplier) spectroscopy. The results showed that although both powders crystallize in the same crystal arrangement (cubic, Fm-3m), particles size, shape and optical properties are dependent on the polymer used.",
publisher = "Belgrade : Serbian Academy of Sciences and Arts",
journal = "Program and Book of Abstracts / First International Conference on Electron Microscopy of Nanostructures ELMINA 2018, August 27-29, 2018, Belgrade, Serbia",
title = "Polyacrilic Acid and Chitosan Assisted Solvothermal Synthesis of Up-converting NaYF4: Yb,Er Particles",
pages = "195-197"
}
Vuković M, Dinić I, Mančić L, Nikolić MG, Rabasović MD, Milošević O. Polyacrilic Acid and Chitosan Assisted Solvothermal Synthesis of Up-converting NaYF4: Yb,Er Particles. Program and Book of Abstracts / First International Conference on Electron Microscopy of Nanostructures ELMINA 2018, August 27-29, 2018, Belgrade, Serbia. 2018;:195-197
Vuković, M., Dinić, I., Mančić, L., Nikolić, M. G., Rabasović, M. D.,& Milošević, O. (2018). Polyacrilic Acid and Chitosan Assisted Solvothermal Synthesis of Up-converting NaYF4: Yb,Er Particles.
Program and Book of Abstracts / First International Conference on Electron Microscopy of Nanostructures ELMINA 2018, August 27-29, 2018, Belgrade, SerbiaBelgrade : Serbian Academy of Sciences and Arts., null, 195-197. 
Vuković Marina, Dinić Ivana, Mančić Lidija, Nikolić Marko G., Rabasović Mihailo D., Milošević Olivera, "Polyacrilic Acid and Chitosan Assisted Solvothermal Synthesis of Up-converting NaYF4: Yb,Er Particles" null (2018):195-197

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