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Influence of heating rate on two-step sintering behaviour of different hydroxyapatite nanopowders

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2010
Lukic_YUCOMAT2010_142.pdf (240.5Kb)
Authors
Lukić, Miodrag J.
Stojanović, Zoran S.
Veselinović, Ljiljana
Marković, Smilja
Uskoković, Dragan
Conference object (Published version)
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Abstract
Producing of dense nanostructured calcium phosphate-based bioceramics represents a challenging issue in biomaterial science. High volume fraction of energetically rich grain boundaries contributes to improved attachment of chemical species, which are important in the processes of bone tissue regeneration. Beside that, nanostructured ceramics exhibited better mechanical properties due to changed fracture path. The process of presureless sintering is the most compatible route for industrial fabrication of dense bioceramic materials, but it is often connected with accelerated grain growth in final sintering stage. In the method of two-step sintering (TSS) the difference between kinetics of grain boundary diffusion and grain boundary migration is used to obtain almost full dense, nanostructured ceramics. However, designing of proper sintering parameters is very important in every sintering technique employed. In this study, hydroxyapatite nanopowders were synthesized by different methods, ...precisely, chemical precipitation and hydrothermal processing of precipitate. The prepared powders were pressed in pellets and heated with different heating rates (2, 5, 10 ºC/min), with short isothermal dwell at certain temperature range. From that shrinkage curves the appropriate conditions were selected to design TSS experiments. The impact of heating rate on final density, phase composition, average grain size and microstructural uniformity is discussed. Furthermore, mechanical properties were determined.

Keywords:
calcium phosphate / bioceramics / two-step sintering
Source:
Programme and The Book of Abstracts / Twelfth Annual Conference YUCOMAT 2010, Herceg Novi, September 6–10, 2010, 2010, 142-142
Funding / projects:
  • Sinteza funkcionalnih materijala sa kontrolisanom strukturom na molekularnom i nano nivou (RS-142006)

ISBN: 9788680321189

[ Google Scholar ]
Handle
https://hdl.handle.net/21.15107/rcub_dais_3559
URI
https://dais.sanu.ac.rs/123456789/3559
Collections
  • ИТН САНУ - Општа колекција / ITS SASA - General collection
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - CONF
AU  - Lukić, Miodrag J.
AU  - Stojanović, Zoran S.
AU  - Veselinović, Ljiljana
AU  - Marković, Smilja
AU  - Uskoković, Dragan
PY  - 2010
UR  - https://dais.sanu.ac.rs/123456789/3559
AB  - Producing of dense nanostructured calcium phosphate-based bioceramics represents a challenging issue in biomaterial science. High volume fraction of energetically rich grain boundaries contributes to improved attachment of chemical species, which are important in the processes of bone tissue regeneration. Beside that, nanostructured ceramics exhibited better mechanical properties due to changed fracture path. The process of presureless sintering is the most compatible route for industrial fabrication of dense bioceramic materials, but it is often connected with accelerated grain growth in final sintering stage. In the method of two-step sintering (TSS) the difference between kinetics of grain boundary diffusion and grain boundary migration is used to obtain almost full dense, nanostructured ceramics. However, designing of proper sintering parameters is very important in every sintering technique employed. In this study, hydroxyapatite nanopowders were synthesized by different methods, precisely, chemical precipitation and hydrothermal processing of precipitate. The prepared powders were pressed in pellets and heated with different heating rates (2, 5, 10 ºC/min), with short isothermal dwell at certain temperature range. From that shrinkage curves the appropriate conditions were selected to design TSS experiments. The impact of heating rate on final density, phase composition, average grain size and microstructural uniformity is discussed. Furthermore, mechanical properties were determined.
C3  - Programme and The Book of Abstracts / Twelfth Annual Conference YUCOMAT 2010, Herceg Novi, September 6–10, 2010
T1  - Influence of heating rate on two-step sintering behaviour of different hydroxyapatite nanopowders
SP  - 142
EP  - 142
UR  - https://hdl.handle.net/21.15107/rcub_dais_3559
ER  - 
@conference{
author = "Lukić, Miodrag J. and Stojanović, Zoran S. and Veselinović, Ljiljana and Marković, Smilja and Uskoković, Dragan",
year = "2010",
abstract = "Producing of dense nanostructured calcium phosphate-based bioceramics represents a challenging issue in biomaterial science. High volume fraction of energetically rich grain boundaries contributes to improved attachment of chemical species, which are important in the processes of bone tissue regeneration. Beside that, nanostructured ceramics exhibited better mechanical properties due to changed fracture path. The process of presureless sintering is the most compatible route for industrial fabrication of dense bioceramic materials, but it is often connected with accelerated grain growth in final sintering stage. In the method of two-step sintering (TSS) the difference between kinetics of grain boundary diffusion and grain boundary migration is used to obtain almost full dense, nanostructured ceramics. However, designing of proper sintering parameters is very important in every sintering technique employed. In this study, hydroxyapatite nanopowders were synthesized by different methods, precisely, chemical precipitation and hydrothermal processing of precipitate. The prepared powders were pressed in pellets and heated with different heating rates (2, 5, 10 ºC/min), with short isothermal dwell at certain temperature range. From that shrinkage curves the appropriate conditions were selected to design TSS experiments. The impact of heating rate on final density, phase composition, average grain size and microstructural uniformity is discussed. Furthermore, mechanical properties were determined.",
journal = "Programme and The Book of Abstracts / Twelfth Annual Conference YUCOMAT 2010, Herceg Novi, September 6–10, 2010",
title = "Influence of heating rate on two-step sintering behaviour of different hydroxyapatite nanopowders",
pages = "142-142",
url = "https://hdl.handle.net/21.15107/rcub_dais_3559"
}
Lukić, M. J., Stojanović, Z. S., Veselinović, L., Marković, S.,& Uskoković, D.. (2010). Influence of heating rate on two-step sintering behaviour of different hydroxyapatite nanopowders. in Programme and The Book of Abstracts / Twelfth Annual Conference YUCOMAT 2010, Herceg Novi, September 6–10, 2010, 142-142.
https://hdl.handle.net/21.15107/rcub_dais_3559
Lukić MJ, Stojanović ZS, Veselinović L, Marković S, Uskoković D. Influence of heating rate on two-step sintering behaviour of different hydroxyapatite nanopowders. in Programme and The Book of Abstracts / Twelfth Annual Conference YUCOMAT 2010, Herceg Novi, September 6–10, 2010. 2010;:142-142.
https://hdl.handle.net/21.15107/rcub_dais_3559 .
Lukić, Miodrag J., Stojanović, Zoran S., Veselinović, Ljiljana, Marković, Smilja, Uskoković, Dragan, "Influence of heating rate on two-step sintering behaviour of different hydroxyapatite nanopowders" in Programme and The Book of Abstracts / Twelfth Annual Conference YUCOMAT 2010, Herceg Novi, September 6–10, 2010 (2010):142-142,
https://hdl.handle.net/21.15107/rcub_dais_3559 .

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