Reheating of zinc-titanate sintered specimens
Authors
Labus, Nebojša
Mentus, Slavko

Rakić, Srđan
Đurić, Zorka Ž.

Vujančević, Jelena

Nikolić, Maria Vesna

Article (Published version)
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The scope of this work was observing dimensional and heat transfer changes in ZnTiO3 samples during heating in nitrogen and air atmosphere. Interactions of bulk specimens with gaseous surrounding induce microstructure changes during heating. Sintered ZnTiO3 nanopowder samples were submitted to subsequent heating. Dilatation curves and thermogravimetric with simultaneous differential thermal analysis TGA/DTA curves were recorded. Reheating was performed in air and nitrogen atmospheres. Reheated samples obtained at different characteristic temperatures in air were analyzed by X-ray diffraction (XRD). Microstructures obtained by scanning electron microscopy (SEM) of reheated sintered samples are presented and compared. Reheating in a different atmosphere induced different microstructures. The goal was indicating possible causes leading to the microstructure changes. © 2015 International Institute for the Science of Sintering (IISS). All rights reserved.
Keywords:
dilatometry / sinteringSource:
Science of Sintering, 2015, 47, 1, 71-81Publisher:
- Belgrade : International Institute for the Science of Sintering
Funding / projects:
- Directed synthesis, structure and properties of multifunctional materials (RS-172057)
- Lithium-ion batteries and fuel cells - research and development (RS-45014)
DOI: 10.2298/SOS1501071L
ISSN: 0350-820X (Print); 1820-7413
WoS: 000355226700009
Scopus: 2-s2.0-84928801997
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - JOUR AU - Labus, Nebojša AU - Mentus, Slavko AU - Rakić, Srđan AU - Đurić, Zorka Ž. AU - Vujančević, Jelena AU - Nikolić, Maria Vesna PY - 2015 UR - https://dais.sanu.ac.rs/123456789/3537 AB - The scope of this work was observing dimensional and heat transfer changes in ZnTiO3 samples during heating in nitrogen and air atmosphere. Interactions of bulk specimens with gaseous surrounding induce microstructure changes during heating. Sintered ZnTiO3 nanopowder samples were submitted to subsequent heating. Dilatation curves and thermogravimetric with simultaneous differential thermal analysis TGA/DTA curves were recorded. Reheating was performed in air and nitrogen atmospheres. Reheated samples obtained at different characteristic temperatures in air were analyzed by X-ray diffraction (XRD). Microstructures obtained by scanning electron microscopy (SEM) of reheated sintered samples are presented and compared. Reheating in a different atmosphere induced different microstructures. The goal was indicating possible causes leading to the microstructure changes. © 2015 International Institute for the Science of Sintering (IISS). All rights reserved. PB - Belgrade : International Institute for the Science of Sintering T2 - Science of Sintering T1 - Reheating of zinc-titanate sintered specimens SP - 71 EP - 81 VL - 47 IS - 1 DO - 10.2298/SOS1501071L UR - https://hdl.handle.net/21.15107/rcub_dais_3537 ER -
@article{ author = "Labus, Nebojša and Mentus, Slavko and Rakić, Srđan and Đurić, Zorka Ž. and Vujančević, Jelena and Nikolić, Maria Vesna", year = "2015", abstract = "The scope of this work was observing dimensional and heat transfer changes in ZnTiO3 samples during heating in nitrogen and air atmosphere. Interactions of bulk specimens with gaseous surrounding induce microstructure changes during heating. Sintered ZnTiO3 nanopowder samples were submitted to subsequent heating. Dilatation curves and thermogravimetric with simultaneous differential thermal analysis TGA/DTA curves were recorded. Reheating was performed in air and nitrogen atmospheres. Reheated samples obtained at different characteristic temperatures in air were analyzed by X-ray diffraction (XRD). Microstructures obtained by scanning electron microscopy (SEM) of reheated sintered samples are presented and compared. Reheating in a different atmosphere induced different microstructures. The goal was indicating possible causes leading to the microstructure changes. © 2015 International Institute for the Science of Sintering (IISS). All rights reserved.", publisher = "Belgrade : International Institute for the Science of Sintering", journal = "Science of Sintering", title = "Reheating of zinc-titanate sintered specimens", pages = "71-81", volume = "47", number = "1", doi = "10.2298/SOS1501071L", url = "https://hdl.handle.net/21.15107/rcub_dais_3537" }
Labus, N., Mentus, S., Rakić, S., Đurić, Z. Ž., Vujančević, J.,& Nikolić, M. V.. (2015). Reheating of zinc-titanate sintered specimens. in Science of Sintering Belgrade : International Institute for the Science of Sintering., 47(1), 71-81. https://doi.org/10.2298/SOS1501071L https://hdl.handle.net/21.15107/rcub_dais_3537
Labus N, Mentus S, Rakić S, Đurić ZŽ, Vujančević J, Nikolić MV. Reheating of zinc-titanate sintered specimens. in Science of Sintering. 2015;47(1):71-81. doi:10.2298/SOS1501071L https://hdl.handle.net/21.15107/rcub_dais_3537 .
Labus, Nebojša, Mentus, Slavko, Rakić, Srđan, Đurić, Zorka Ž., Vujančević, Jelena, Nikolić, Maria Vesna, "Reheating of zinc-titanate sintered specimens" in Science of Sintering, 47, no. 1 (2015):71-81, https://doi.org/10.2298/SOS1501071L ., https://hdl.handle.net/21.15107/rcub_dais_3537 .