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The influence of mechanochemical activation and thermal treatment on magnetic properties of the BaTiO3 -FexOy powder mixture

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2015
Ristanovic_2015_Science-of-Sintering_47_3.pdf (669.7Kb)
Authors
Ristanović, Z.
Kalezić Glišović, Aleksandra
Mitrović, Nebojša
Đukić, S.
Kosanović, Darko
Maričić, Aleksa
Article (Published version)
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Abstract
Powder mixture of 50 mass % of barium titanate (BaTiO3) and 50 mass % of iron (Fe) was prepared by solid-state reaction technique, i.e. ball milled in air for 60 min, 80 min, 100 min, 120 min and 150 min. During mechanochemical activation it was observed the iron powder transitsion to iron oxides. Depending on the activation time the content of iron oxides FeO, Fe2 O3 and Fe3O4 varies. Simultaneously, with the content change of the activated system, magnetic properties change as well. The XRD analysis of milled samples shown that as the activation time increase, the iron oxide percentage increases to, whereby the percentage of BaTiO3 in a total sample mass decreases. The percentage of iron oxides and BaTiO3 in annealed samples changes depending on annealing temperature. The thermomagnetic measurements performed by Faraday method shown that the powder mixture milled for 100 minutes exhibit maximum magnetization prior to annealing. The increase of magnetization maximum was observed after... annealing at 540 oC with all milled samples, and at room temperature it has enhancement from 10 % to 22 % depending on the activation time. The samples milled for 100 min and 150 min and then sintered at 1200 oC exhibit magnetoelectric properties. © 2015 International Institute for the Science of Sintering (IISS). All rights reserved.

Keywords:
BaTiO3-FexOy powder mixture / magnetoelectric properties / mechanochemical activation / thermomagnetic properties
Source:
Science of Sintering, 2015, 47, 1, 3-14
Publisher:
  • Belgrade : International Institute for the Science of Sintering
Funding / projects:
  • Directed synthesis, structure and properties of multifunctional materials (RS-172057)

DOI: 10.2298/SOS141121001R

ISSN: 0350-820X

WoS: 000366333700003

Scopus: 2-s2.0-84928797631
[ Google Scholar ]
15
Handle
https://hdl.handle.net/21.15107/rcub_dais_3534
URI
https://dais.sanu.ac.rs/123456789/3534
Collections
  • ИТН САНУ - Општа колекција / ITS SASA - General collection
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - JOUR
AU  - Ristanović, Z.
AU  - Kalezić Glišović, Aleksandra
AU  - Mitrović, Nebojša
AU  - Đukić, S.
AU  - Kosanović, Darko
AU  - Maričić, Aleksa
PY  - 2015
UR  - https://dais.sanu.ac.rs/123456789/3534
AB  - Powder mixture of 50 mass % of barium titanate (BaTiO3) and 50 mass % of iron (Fe) was prepared by solid-state reaction technique, i.e. ball milled in air for 60 min, 80 min, 100 min, 120 min and 150 min. During mechanochemical activation it was observed the iron powder transitsion to iron oxides. Depending on the activation time the content of iron oxides FeO, Fe2 O3 and Fe3O4 varies. Simultaneously, with the content change of the activated system, magnetic properties change as well. The XRD analysis of milled samples shown that as the activation time increase, the iron oxide percentage increases to, whereby the percentage of BaTiO3 in a total sample mass decreases. The percentage of iron oxides and BaTiO3 in annealed samples changes depending on annealing temperature. The thermomagnetic measurements performed by Faraday method shown that the powder mixture milled for 100 minutes exhibit maximum magnetization prior to annealing. The increase of magnetization maximum was observed after annealing at 540 oC with all milled samples, and at room temperature it has enhancement from 10 % to 22 % depending on the activation time. The samples milled for 100 min and 150 min and then sintered at 1200 oC exhibit magnetoelectric properties. © 2015 International Institute for the Science of Sintering (IISS). All rights reserved.
PB  - Belgrade : International Institute for the Science of Sintering
T2  - Science of Sintering
T1  - The influence of mechanochemical activation and thermal treatment on magnetic properties of the BaTiO3 -FexOy powder mixture
SP  - 3
EP  - 14
VL  - 47
IS  - 1
DO  - 10.2298/SOS141121001R
UR  - https://hdl.handle.net/21.15107/rcub_dais_3534
ER  - 
@article{
author = "Ristanović, Z. and Kalezić Glišović, Aleksandra and Mitrović, Nebojša and Đukić, S. and Kosanović, Darko and Maričić, Aleksa",
year = "2015",
abstract = "Powder mixture of 50 mass % of barium titanate (BaTiO3) and 50 mass % of iron (Fe) was prepared by solid-state reaction technique, i.e. ball milled in air for 60 min, 80 min, 100 min, 120 min and 150 min. During mechanochemical activation it was observed the iron powder transitsion to iron oxides. Depending on the activation time the content of iron oxides FeO, Fe2 O3 and Fe3O4 varies. Simultaneously, with the content change of the activated system, magnetic properties change as well. The XRD analysis of milled samples shown that as the activation time increase, the iron oxide percentage increases to, whereby the percentage of BaTiO3 in a total sample mass decreases. The percentage of iron oxides and BaTiO3 in annealed samples changes depending on annealing temperature. The thermomagnetic measurements performed by Faraday method shown that the powder mixture milled for 100 minutes exhibit maximum magnetization prior to annealing. The increase of magnetization maximum was observed after annealing at 540 oC with all milled samples, and at room temperature it has enhancement from 10 % to 22 % depending on the activation time. The samples milled for 100 min and 150 min and then sintered at 1200 oC exhibit magnetoelectric properties. © 2015 International Institute for the Science of Sintering (IISS). All rights reserved.",
publisher = "Belgrade : International Institute for the Science of Sintering",
journal = "Science of Sintering",
title = "The influence of mechanochemical activation and thermal treatment on magnetic properties of the BaTiO3 -FexOy powder mixture",
pages = "3-14",
volume = "47",
number = "1",
doi = "10.2298/SOS141121001R",
url = "https://hdl.handle.net/21.15107/rcub_dais_3534"
}
Ristanović, Z., Kalezić Glišović, A., Mitrović, N., Đukić, S., Kosanović, D.,& Maričić, A.. (2015). The influence of mechanochemical activation and thermal treatment on magnetic properties of the BaTiO3 -FexOy powder mixture. in Science of Sintering
Belgrade : International Institute for the Science of Sintering., 47(1), 3-14.
https://doi.org/10.2298/SOS141121001R
https://hdl.handle.net/21.15107/rcub_dais_3534
Ristanović Z, Kalezić Glišović A, Mitrović N, Đukić S, Kosanović D, Maričić A. The influence of mechanochemical activation and thermal treatment on magnetic properties of the BaTiO3 -FexOy powder mixture. in Science of Sintering. 2015;47(1):3-14.
doi:10.2298/SOS141121001R
https://hdl.handle.net/21.15107/rcub_dais_3534 .
Ristanović, Z., Kalezić Glišović, Aleksandra, Mitrović, Nebojša, Đukić, S., Kosanović, Darko, Maričić, Aleksa, "The influence of mechanochemical activation and thermal treatment on magnetic properties of the BaTiO3 -FexOy powder mixture" in Science of Sintering, 47, no. 1 (2015):3-14,
https://doi.org/10.2298/SOS141121001R .,
https://hdl.handle.net/21.15107/rcub_dais_3534 .

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