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Hydrothermal synthesis of LiFePO4 in presence of different organic additives

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2010
bitstream_11125.pdf (785.6Kb)
Authors
Jović, Maja
Stojanović, Zoran S.
Jugović, Dragana
Škapin, Srečo Davor
Uskoković, Dragan
Conference object (Published version)
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Abstract
In this work we have investigated possibility to obtain pure LiFePO4 powder using different organic additives during hydrothermal synthesis at 180°C. Phase pure phospho olivine was obtained in presence of polyvinylpyrrolidone, while addition of polyvinyl alcohol leads to formation of LiFePO4 with impurities. Impurity phase was successfully avoided by introducing citric acid into reaction vessel. Phase composition was determined by XRPD. Morphology was revealed by particle size analyzer and FESEM.
Keywords:
hydrothermal synthesis / LiFePO4
Source:
Physical Chemistry 2010 : proceedings. Vol. 2 / 10th International Conference on Fundamental and Applied Aspects of Physical Chemistry, 21-24 September 2010, Belgrade, 2010, 441-443
Publisher:
  • Belgrade : Society of Physical Chemists of Serbia
Funding / projects:
  • Sinteza funkcionalnih materijala sa kontrolisanom strukturom na molekularnom i nano nivou (RS-142006)

ISBN: 978-86-82475-18-7

[ Google Scholar ]
Handle
https://hdl.handle.net/21.15107/rcub_dais_3496
URI
https://dais.sanu.ac.rs/123456789/3496
Collections
  • ИТН САНУ - Општа колекција / ITS SASA - General collection
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - CONF
AU  - Jović, Maja
AU  - Stojanović, Zoran S.
AU  - Jugović, Dragana
AU  - Škapin, Srečo Davor
AU  - Uskoković, Dragan
PY  - 2010
UR  - https://dais.sanu.ac.rs/123456789/3496
AB  - In this work we have investigated possibility to obtain pure LiFePO4 powder using different organic additives during hydrothermal synthesis at 180°C. Phase pure phospho olivine was obtained in presence of polyvinylpyrrolidone, while addition of polyvinyl alcohol leads to formation of LiFePO4 with impurities. Impurity phase was successfully avoided by introducing citric acid into reaction vessel. Phase composition was determined by XRPD. Morphology was revealed by particle size analyzer and FESEM.
PB  - Belgrade : Society of Physical Chemists of Serbia
C3  - Physical Chemistry 2010 : proceedings. Vol. 2 / 10th International Conference on Fundamental and Applied Aspects of Physical Chemistry, 21-24 September 2010, Belgrade
T1  - Hydrothermal synthesis of LiFePO4 in presence of different organic additives
SP  - 441
EP  - 443
UR  - https://hdl.handle.net/21.15107/rcub_dais_3496
ER  - 
@conference{
author = "Jović, Maja and Stojanović, Zoran S. and Jugović, Dragana and Škapin, Srečo Davor and Uskoković, Dragan",
year = "2010",
abstract = "In this work we have investigated possibility to obtain pure LiFePO4 powder using different organic additives during hydrothermal synthesis at 180°C. Phase pure phospho olivine was obtained in presence of polyvinylpyrrolidone, while addition of polyvinyl alcohol leads to formation of LiFePO4 with impurities. Impurity phase was successfully avoided by introducing citric acid into reaction vessel. Phase composition was determined by XRPD. Morphology was revealed by particle size analyzer and FESEM.",
publisher = "Belgrade : Society of Physical Chemists of Serbia",
journal = "Physical Chemistry 2010 : proceedings. Vol. 2 / 10th International Conference on Fundamental and Applied Aspects of Physical Chemistry, 21-24 September 2010, Belgrade",
title = "Hydrothermal synthesis of LiFePO4 in presence of different organic additives",
pages = "441-443",
url = "https://hdl.handle.net/21.15107/rcub_dais_3496"
}
Jović, M., Stojanović, Z. S., Jugović, D., Škapin, S. D.,& Uskoković, D.. (2010). Hydrothermal synthesis of LiFePO4 in presence of different organic additives. in Physical Chemistry 2010 : proceedings. Vol. 2 / 10th International Conference on Fundamental and Applied Aspects of Physical Chemistry, 21-24 September 2010, Belgrade
Belgrade : Society of Physical Chemists of Serbia., 441-443.
https://hdl.handle.net/21.15107/rcub_dais_3496
Jović M, Stojanović ZS, Jugović D, Škapin SD, Uskoković D. Hydrothermal synthesis of LiFePO4 in presence of different organic additives. in Physical Chemistry 2010 : proceedings. Vol. 2 / 10th International Conference on Fundamental and Applied Aspects of Physical Chemistry, 21-24 September 2010, Belgrade. 2010;:441-443.
https://hdl.handle.net/21.15107/rcub_dais_3496 .
Jović, Maja, Stojanović, Zoran S., Jugović, Dragana, Škapin, Srečo Davor, Uskoković, Dragan, "Hydrothermal synthesis of LiFePO4 in presence of different organic additives" in Physical Chemistry 2010 : proceedings. Vol. 2 / 10th International Conference on Fundamental and Applied Aspects of Physical Chemistry, 21-24 September 2010, Belgrade (2010):441-443,
https://hdl.handle.net/21.15107/rcub_dais_3496 .

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