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Densification rate and phase structure changes during sintering of zinc titanate ceramics

Authorized Users Only
2009
Authors
Nikolić, Maria Vesna
Labus, Nebojša
Ristić, Momčilo M.
Article (Published version)
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Abstract
Densification rate and phase structure changes during sintering of nanosized ZnTiO3 were studied. Sintering was performed in a dilatometer in two regimes: the first to 900 °C (heating rates 5, 10 and 15 °C/min) and the second to 1200 °C (heating rates 3, 5 and 10 °C/min). XRD analysis of samples sintered at both temperatures combined with Rietveld structure refinement enabled determination of all phases present and their structure parameters. Samples sintered to 900 °C contained ZnTiO3 and Zn2TiO4 with traces of r-TiO2 (rutile) and Zn2Ti3O8, while samples sintered to1200 °C contained only r-TiO2 and Zn2TiO4. A master sintering curve was defined for sintering to 900 °C enabling determination of the sintering process activation energy as 313 kJ/mol. © 2009 Elsevier Ltd and Techna Group S.r.l.
Keywords:
sintering / X-ray methods / microstructure / zinc titanate
Source:
Ceramics International, 2009, 35, 8, 3217-3220
Publisher:
  • Elsevier
Funding / projects:
  • Investigation of the relation in triad: Synthesis structure-properties for functional materials (RS-142011)

DOI: 10.1016/j.ceramint.2009.05.028

ISSN: 0272-8842

WoS: 000271368100034

Scopus: 2-s2.0-70349420855
[ Google Scholar ]
13
13
Handle
https://hdl.handle.net/21.15107/rcub_dais_3456
URI
https://dais.sanu.ac.rs/123456789/3456
Collections
  • ИТН САНУ - Општа колекција / ITS SASA - General collection
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - JOUR
AU  - Nikolić, Maria Vesna
AU  - Labus, Nebojša
AU  - Ristić, Momčilo M.
PY  - 2009
UR  - https://dais.sanu.ac.rs/123456789/3456
AB  - Densification rate and phase structure changes during sintering of nanosized ZnTiO3 were studied. Sintering was performed in a dilatometer in two regimes: the first to 900 °C (heating rates 5, 10 and 15 °C/min) and the second to 1200 °C (heating rates 3, 5 and 10 °C/min). XRD analysis of samples sintered at both temperatures combined with Rietveld structure refinement enabled determination of all phases present and their structure parameters. Samples sintered to 900 °C contained ZnTiO3 and Zn2TiO4 with traces of r-TiO2 (rutile) and Zn2Ti3O8, while samples sintered to1200 °C contained only r-TiO2 and Zn2TiO4. A master sintering curve was defined for sintering to 900 °C enabling determination of the sintering process activation energy as 313 kJ/mol. © 2009 Elsevier Ltd and Techna Group S.r.l.
PB  - Elsevier
T2  - Ceramics International
T1  - Densification rate and phase structure changes during sintering of zinc titanate ceramics
SP  - 3217
EP  - 3220
VL  - 35
IS  - 8
DO  - 10.1016/j.ceramint.2009.05.028
UR  - https://hdl.handle.net/21.15107/rcub_dais_3456
ER  - 
@article{
author = "Nikolić, Maria Vesna and Labus, Nebojša and Ristić, Momčilo M.",
year = "2009",
abstract = "Densification rate and phase structure changes during sintering of nanosized ZnTiO3 were studied. Sintering was performed in a dilatometer in two regimes: the first to 900 °C (heating rates 5, 10 and 15 °C/min) and the second to 1200 °C (heating rates 3, 5 and 10 °C/min). XRD analysis of samples sintered at both temperatures combined with Rietveld structure refinement enabled determination of all phases present and their structure parameters. Samples sintered to 900 °C contained ZnTiO3 and Zn2TiO4 with traces of r-TiO2 (rutile) and Zn2Ti3O8, while samples sintered to1200 °C contained only r-TiO2 and Zn2TiO4. A master sintering curve was defined for sintering to 900 °C enabling determination of the sintering process activation energy as 313 kJ/mol. © 2009 Elsevier Ltd and Techna Group S.r.l.",
publisher = "Elsevier",
journal = "Ceramics International",
title = "Densification rate and phase structure changes during sintering of zinc titanate ceramics",
pages = "3217-3220",
volume = "35",
number = "8",
doi = "10.1016/j.ceramint.2009.05.028",
url = "https://hdl.handle.net/21.15107/rcub_dais_3456"
}
Nikolić, M. V., Labus, N.,& Ristić, M. M.. (2009). Densification rate and phase structure changes during sintering of zinc titanate ceramics. in Ceramics International
Elsevier., 35(8), 3217-3220.
https://doi.org/10.1016/j.ceramint.2009.05.028
https://hdl.handle.net/21.15107/rcub_dais_3456
Nikolić MV, Labus N, Ristić MM. Densification rate and phase structure changes during sintering of zinc titanate ceramics. in Ceramics International. 2009;35(8):3217-3220.
doi:10.1016/j.ceramint.2009.05.028
https://hdl.handle.net/21.15107/rcub_dais_3456 .
Nikolić, Maria Vesna, Labus, Nebojša, Ristić, Momčilo M., "Densification rate and phase structure changes during sintering of zinc titanate ceramics" in Ceramics International, 35, no. 8 (2009):3217-3220,
https://doi.org/10.1016/j.ceramint.2009.05.028 .,
https://hdl.handle.net/21.15107/rcub_dais_3456 .

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