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YAG:Ce3+ nanostructured particles obtained via spray pyrolysis of polymeric precursor solution

Authorized Users Only
2010
Authors
Mančić, Lidija
Marinković, Katarina
Marinković, Bojan A.
Dramićanin, Miroslav
Milošević, Olivera
Article (Published version)
Metadata
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Abstract
Cerium-doped yttrium aluminum garnet (YAG:Ce3+) powder phosphor is synthesized via spray pyrolysis of polymeric precursor solution obtained by dissolving the corresponding nitrates in ethylenediaminetetraacetic acid (EDTA). Ultrasonically generated aerosol droplets are decomposed at 600 °C in argon atmosphere. Following the initial attempt in providing pure YAG:Ce3+ phase generation the particles were additionally thermally treated for 3 h in air at 1000 and 1100 °C. The powder morphology is followed with scanning electron microscopy (SEM), while inner particle structure is analysed by analytical and high-resolution transmission electron microscopy (TEM). Phase identification is performed by X-ray powder diffraction (XRPD) based on which a structural refinement through Rietveld method was done. The spherical submicronic particles have grained sub-structure comprising clustered garnet monocrystals sized below 100 nm. The YAG:Ce3+ emission shows wide peak in the range 470-600 nm with the... maximum near 520 nm. © 2009 Elsevier Ltd. All rights reserved.

Keywords:
spray pyrolysis / X-ray methods / garnet / polymeric precursor
Source:
Journal of the European Ceramic Society, 2010, 30, 2, 577-582
Publisher:
  • Elsevier
Funding / projects:
  • Synthesis, characterization and activity of organic and coordination composition and their application in (bio) nanotechnology (RS-142010)
  • MPNS COST Action 539 - Electroceramics from Nanopowders Produced by Innovative Methods (ELENA)

DOI: 10.1016/j.jeurceramsoc.2009.05.037

ISSN: 0955-2219

WoS: 000272455600079

Scopus: 2-s2.0-70449523438
[ Google Scholar ]
58
58
Handle
https://hdl.handle.net/21.15107/rcub_dais_3438
URI
https://dais.sanu.ac.rs/123456789/3438
Collections
  • ИТН САНУ - Општа колекција / ITS SASA - General collection
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - JOUR
AU  - Mančić, Lidija
AU  - Marinković, Katarina
AU  - Marinković, Bojan A.
AU  - Dramićanin, Miroslav
AU  - Milošević, Olivera
PY  - 2010
UR  - https://dais.sanu.ac.rs/123456789/3438
AB  - Cerium-doped yttrium aluminum garnet (YAG:Ce3+) powder phosphor is synthesized via spray pyrolysis of polymeric precursor solution obtained by dissolving the corresponding nitrates in ethylenediaminetetraacetic acid (EDTA). Ultrasonically generated aerosol droplets are decomposed at 600 °C in argon atmosphere. Following the initial attempt in providing pure YAG:Ce3+ phase generation the particles were additionally thermally treated for 3 h in air at 1000 and 1100 °C. The powder morphology is followed with scanning electron microscopy (SEM), while inner particle structure is analysed by analytical and high-resolution transmission electron microscopy (TEM). Phase identification is performed by X-ray powder diffraction (XRPD) based on which a structural refinement through Rietveld method was done. The spherical submicronic particles have grained sub-structure comprising clustered garnet monocrystals sized below 100 nm. The YAG:Ce3+ emission shows wide peak in the range 470-600 nm with the maximum near 520 nm. © 2009 Elsevier Ltd. All rights reserved.
PB  - Elsevier
T2  - Journal of the European Ceramic Society
T1  - YAG:Ce3+ nanostructured particles obtained via spray pyrolysis of polymeric precursor solution
SP  - 577
EP  - 582
VL  - 30
IS  - 2
DO  - 10.1016/j.jeurceramsoc.2009.05.037
UR  - https://hdl.handle.net/21.15107/rcub_dais_3438
ER  - 
@article{
author = "Mančić, Lidija and Marinković, Katarina and Marinković, Bojan A. and Dramićanin, Miroslav and Milošević, Olivera",
year = "2010",
abstract = "Cerium-doped yttrium aluminum garnet (YAG:Ce3+) powder phosphor is synthesized via spray pyrolysis of polymeric precursor solution obtained by dissolving the corresponding nitrates in ethylenediaminetetraacetic acid (EDTA). Ultrasonically generated aerosol droplets are decomposed at 600 °C in argon atmosphere. Following the initial attempt in providing pure YAG:Ce3+ phase generation the particles were additionally thermally treated for 3 h in air at 1000 and 1100 °C. The powder morphology is followed with scanning electron microscopy (SEM), while inner particle structure is analysed by analytical and high-resolution transmission electron microscopy (TEM). Phase identification is performed by X-ray powder diffraction (XRPD) based on which a structural refinement through Rietveld method was done. The spherical submicronic particles have grained sub-structure comprising clustered garnet monocrystals sized below 100 nm. The YAG:Ce3+ emission shows wide peak in the range 470-600 nm with the maximum near 520 nm. © 2009 Elsevier Ltd. All rights reserved.",
publisher = "Elsevier",
journal = "Journal of the European Ceramic Society",
title = "YAG:Ce3+ nanostructured particles obtained via spray pyrolysis of polymeric precursor solution",
pages = "577-582",
volume = "30",
number = "2",
doi = "10.1016/j.jeurceramsoc.2009.05.037",
url = "https://hdl.handle.net/21.15107/rcub_dais_3438"
}
Mančić, L., Marinković, K., Marinković, B. A., Dramićanin, M.,& Milošević, O.. (2010). YAG:Ce3+ nanostructured particles obtained via spray pyrolysis of polymeric precursor solution. in Journal of the European Ceramic Society
Elsevier., 30(2), 577-582.
https://doi.org/10.1016/j.jeurceramsoc.2009.05.037
https://hdl.handle.net/21.15107/rcub_dais_3438
Mančić L, Marinković K, Marinković BA, Dramićanin M, Milošević O. YAG:Ce3+ nanostructured particles obtained via spray pyrolysis of polymeric precursor solution. in Journal of the European Ceramic Society. 2010;30(2):577-582.
doi:10.1016/j.jeurceramsoc.2009.05.037
https://hdl.handle.net/21.15107/rcub_dais_3438 .
Mančić, Lidija, Marinković, Katarina, Marinković, Bojan A., Dramićanin, Miroslav, Milošević, Olivera, "YAG:Ce3+ nanostructured particles obtained via spray pyrolysis of polymeric precursor solution" in Journal of the European Ceramic Society, 30, no. 2 (2010):577-582,
https://doi.org/10.1016/j.jeurceramsoc.2009.05.037 .,
https://hdl.handle.net/21.15107/rcub_dais_3438 .

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