Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved.
TY - JOUR
AU - Nikčević, Irena
AU - Jokanović, Vukoman
AU - Mitrić, Miodrag
AU - Nedić, Z
AU - Makovec, Darko
AU - Uskoković, Dragan
PY - 2004
UR - http://dais.sanu.ac.rs/123456789/3288
AB - Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved.
T2 - Journal of Solid State Chemistry
T1 - Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite
SP - 2565
EP - 2574
VL - 177
IS - 7
DO - 10.1016/j.jssc.2004.03.024
ER -
@article{
author = "Nikčević, Irena and Jokanović, Vukoman and Mitrić, Miodrag and Nedić, Z and Makovec, Darko and Uskoković, Dragan",
year = "2004",
url = "http://dais.sanu.ac.rs/123456789/3288",
abstract = "Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved.",
journal = "Journal of Solid State Chemistry",
title = "Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite",
pages = "2565-2574",
volume = "177",
number = "7",
doi = "10.1016/j.jssc.2004.03.024"
}
Nikčević I, Jokanović V, Mitrić M, Nedić Z, Makovec D, Uskoković D. Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite. Journal of Solid State Chemistry. 2004;177(7):2565-2574
Nikčević, I., Jokanović, V., Mitrić, M., Nedić, Z., Makovec, D.,& Uskoković, D. (2004). Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite.
Journal of Solid State Chemistry, 177(7), 2565-2574.
https://doi.org/10.1016/j.jssc.2004.03.024
