Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite
Authorized Users Only
2004
Authors
Nikčević, IrenaJokanović, Vukoman

Mitrić, Miodrag

Nedić, Z
Makovec, Darko
Uskoković, Dragan

Article (Published version)

Metadata
Show full item recordAbstract
Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved.
Keywords:
fluorapatitie / carbonated fluorhydroxyapatite / hydroxyapatite / mechanochemical synthesisSource:
Journal of Solid State Chemistry, 2004, 177, 7, 2565-2574
DOI: 10.1016/j.jssc.2004.03.024
ISSN: 0022-4596 (Print)
WoS: 000222314700047
Scopus: 2-s2.0-2942654770
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - JOUR AU - Nikčević, Irena AU - Jokanović, Vukoman AU - Mitrić, Miodrag AU - Nedić, Z AU - Makovec, Darko AU - Uskoković, Dragan PY - 2004 UR - https://dais.sanu.ac.rs/123456789/3288 AB - Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved. T2 - Journal of Solid State Chemistry T1 - Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite SP - 2565 EP - 2574 VL - 177 IS - 7 DO - 10.1016/j.jssc.2004.03.024 UR - https://hdl.handle.net/21.15107/rcub_dais_3288 ER -
@article{ author = "Nikčević, Irena and Jokanović, Vukoman and Mitrić, Miodrag and Nedić, Z and Makovec, Darko and Uskoković, Dragan", year = "2004", abstract = "Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved.", journal = "Journal of Solid State Chemistry", title = "Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite", pages = "2565-2574", volume = "177", number = "7", doi = "10.1016/j.jssc.2004.03.024", url = "https://hdl.handle.net/21.15107/rcub_dais_3288" }
Nikčević, I., Jokanović, V., Mitrić, M., Nedić, Z., Makovec, D.,& Uskoković, D.. (2004). Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite. in Journal of Solid State Chemistry, 177(7), 2565-2574. https://doi.org/10.1016/j.jssc.2004.03.024 https://hdl.handle.net/21.15107/rcub_dais_3288
Nikčević I, Jokanović V, Mitrić M, Nedić Z, Makovec D, Uskoković D. Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite. in Journal of Solid State Chemistry. 2004;177(7):2565-2574. doi:10.1016/j.jssc.2004.03.024 https://hdl.handle.net/21.15107/rcub_dais_3288 .
Nikčević, Irena, Jokanović, Vukoman, Mitrić, Miodrag, Nedić, Z, Makovec, Darko, Uskoković, Dragan, "Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite" in Journal of Solid State Chemistry, 177, no. 7 (2004):2565-2574, https://doi.org/10.1016/j.jssc.2004.03.024 ., https://hdl.handle.net/21.15107/rcub_dais_3288 .