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Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite

Authorized Users Only
2004
Authors
Nikčević, Irena
Jokanović, Vukoman
Mitrić, Miodrag
Nedić, Z
Makovec, Darko
Uskoković, Dragan
Article (Published version)
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Abstract
Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved.
Keywords:
fluorapatitie / carbonated fluorhydroxyapatite / hydroxyapatite / mechanochemical synthesis
Source:
Journal of Solid State Chemistry, 2004, 177, 7, 2565-2574

DOI: 10.1016/j.jssc.2004.03.024

ISSN: 0022-4596 (Print)

WoS: 000222314700047

Scopus: 2-s2.0-2942654770
[ Google Scholar ]
78
80
URI
http://dais.sanu.ac.rs/123456789/3288
Collections
  • ITN SANU - Opšta kolekcija / ITS SASA - General collection
Institution
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - JOUR
AU  - Nikčević, Irena
AU  - Jokanović, Vukoman
AU  - Mitrić, Miodrag
AU  - Nedić, Z
AU  - Makovec, Darko
AU  - Uskoković, Dragan
PY  - 2004
UR  - http://dais.sanu.ac.rs/123456789/3288
AB  - Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved.
T2  - Journal of Solid State Chemistry
T1  - Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite
SP  - 2565
EP  - 2574
VL  - 177
IS  - 7
DO  - 10.1016/j.jssc.2004.03.024
ER  - 
@article{
author = "Nikčević, Irena and Jokanović, Vukoman and Mitrić, Miodrag and Nedić, Z and Makovec, Darko and Uskoković, Dragan",
year = "2004",
url = "http://dais.sanu.ac.rs/123456789/3288",
abstract = "Powder mixture of Ca(OH)(2)-P2O5-CaF2 were milled in planetary ball mill. A carbonated fluorhydroxyapatite, FHA Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(OH)(2-2x1)(F)(2x1) was formed after 5 h of milling and carbonated fluoroapatite Ca-10(PO4)(1-y)(CO3)(y)(PO4)(5)(F)(2) was formed after 9 h of milling. Complete transformation of the carbonated form of FA into then single phase of FA occurred after 9 h milling and thermally treating. The various experimental techniques like X-ray Diffraction (XRD), Differential Thermal Analysis (DTA), Infrared Spectroscopy (IR), Transmission Electron Microscopy and Scanning Electron Microscopy (SEM) were used to characterize the synthesized powders and to postulate reaction mechanisms steps- transformations of reactants involved. (C) 2004 Elsevier Inc. All rights reserved.",
journal = "Journal of Solid State Chemistry",
title = "Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite",
pages = "2565-2574",
volume = "177",
number = "7",
doi = "10.1016/j.jssc.2004.03.024"
}
Nikčević I, Jokanović V, Mitrić M, Nedić Z, Makovec D, Uskoković D. Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite. Journal of Solid State Chemistry. 2004;177(7):2565-2574
Nikčević, I., Jokanović, V., Mitrić, M., Nedić, Z., Makovec, D.,& Uskoković, D. (2004). Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite.
Journal of Solid State Chemistry, 177(7), 2565-2574. 
https://doi.org/10.1016/j.jssc.2004.03.024
Nikčević Irena, Jokanović Vukoman, Mitrić Miodrag, Nedić Z, Makovec Darko, Uskoković Dragan, "Mechanochemical synthesis of nanostructured fluorapatite/fluorhydroxyapatite and carbonated fluorapatite/fluorhydroxyapatite" 177, no. 7 (2004):2565-2574,
https://doi.org/10.1016/j.jssc.2004.03.024 .

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