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dc.creatorNikčevic, Irena
dc.creatorMaravić, Dubravka
dc.creatorIgnjatović, Nenad
dc.creatorMitrić, Miodrag
dc.creatorMakovec, Darko
dc.creatorUskoković, Dragan
dc.date.accessioned2018-03-01T20:00:51Z
dc.date.accessioned2018-05-08T09:54:08Z
dc.date.available2018-03-01T20:00:51Z
dc.date.available2018-05-08T09:54:08Z
dc.date.issued2006
dc.identifier.issn1345-9678 (print)
dc.identifier.issn1347-5320 (electronic)
dc.identifier.urihttp://dais.sanu.ac.rs/123456789/2753
dc.description.abstractBiphasic calcium phosphate/poly-L-lactide granules of 150-200 mu m sizes were subjected to high-energy mechanical milling in a planetary ball mill for up to 480 minutes. Characterization of the material obtained was carried out using X-ray diffraction (XRD), differential scanning calorimetry (DSC), environmentally scanning electronic microscopy (ESEM), transmission electron microscopy (TEM) and infrared spectroscopy (IR). These techniques confirmed that mechanical milling induced significant changes in the biocomposite structure and properties. The most significant changes are reduction of the HAp crystallites size from 99.8 to 26.7 nm and beta-TCP from 97.3 to 29.6, as well as crystallinity of PLLA phases. Homogeneous phase distribution (arrangement) is obtained by extending the duration of mechanical milling.en
dc.relationinfo:eu-repo/grantAgreement/MESTD/MPN2006-2010/142006/RS//
dc.rightsopenAccessen
dc.sourceMaterials Transactions. JIM / Japan Institute of Metalsen
dc.subjectnanostructured biocompositeen
dc.subjectbiphasic calcium phosphateen
dc.subjectpoly-L-lactideen
dc.subjectmechanical millingen
dc.subjectsize of crystallitesen
dc.subjectcrystallinity degreeen
dc.titleThe formation and characterization of nanocrystalline phases by mechanical milling of biphasic calcium phosphate/poly-L-lactide biocompositeen
dc.typearticleen
dc.rights.licenseARR
dcterms.abstractНикчевиц, Ирена; Игњатовић, Ненад; Митрић, Миодраг; Маковец, Дарко; Ускоковић, Драган; Маравић, Дубравка;
dc.citation.spage2980
dc.citation.epage2986
dc.citation.volume47
dc.citation.issue12
dc.identifier.wos000244257900013
dc.identifier.doi10.2320/matertrans.47.2980
dc.identifier.scopus2-s2.0-33847261668
dc.type.versionpublishedVersion
dc.identifier.fulltexthttp://dais.sanu.ac.rs/bitstream/id/20484/2831.pdf


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