Structural and magnetic properties of mechanochemically synthesized nanocrystalline titanium monoxide

2012
Authors
Barudžija, Tanja
Gusev, Alexey A.
Jugović, Dragana

Dramićanin, Miroslav

Zdujić, Miodrag

Jovalekić, Čedomir

Mitrić, Miodrag

Article (Published version)
Metadata
Show full item recordAbstract
Nano-sized titanium monoxide (TiO) powder was prepared by mechanochemical synthesis. A mixture of commercial Ti and TiO2 (rutile) powders with the molar ratio of 1:1 was milled in a planetary ball mill for 5, 10, 20, 30 and 60 min under argon atmosphere. The final single-phase titanium monoxide sample was characterized by X-ray diffraction (XRD), magnetic measurements using a superconducting quantum interference device magnetometer (SQUID) and thermogravimetric analysis (TGA). The temperature dependency of the magnetic susceptibility is characterized by significant contribution of Pauli paramagnetism due to conduction electrons.
Keywords:
titanium monoxide / mechanochemical synthesis / nanomaterials / Rietveld method / magnetic measurementsSource:
Hemijska industrija, 2012, 66, 2, 181-186Publisher:
- Belgrade : Association of the Chemical Engineers of Serbia
Projects:
- Nanostructured Functional and Composite Materials in Catalytic and Sorption Processes (RS-45001)
- Magnetic and radionuclide labeled nanostructured materials for medical applications (RS-45015)
DOI: 10.2298/HEMIND111027090B
ISSN: 0367-598X (Print); 2217-7426 (Online)
WoS: 000306026300004
Scopus: 2-s2.0-84861419737
TY - JOUR AU - Barudžija, Tanja AU - Gusev, Alexey A. AU - Jugović, Dragana AU - Dramićanin, Miroslav AU - Zdujić, Miodrag AU - Jovalekić, Čedomir AU - Mitrić, Miodrag PY - 2012 UR - http://dais.sanu.ac.rs/123456789/257 AB - Nano-sized titanium monoxide (TiO) powder was prepared by mechanochemical synthesis. A mixture of commercial Ti and TiO2 (rutile) powders with the molar ratio of 1:1 was milled in a planetary ball mill for 5, 10, 20, 30 and 60 min under argon atmosphere. The final single-phase titanium monoxide sample was characterized by X-ray diffraction (XRD), magnetic measurements using a superconducting quantum interference device magnetometer (SQUID) and thermogravimetric analysis (TGA). The temperature dependency of the magnetic susceptibility is characterized by significant contribution of Pauli paramagnetism due to conduction electrons. PB - Belgrade : Association of the Chemical Engineers of Serbia T2 - Hemijska industrija T1 - Structural and magnetic properties of mechanochemically synthesized nanocrystalline titanium monoxide SP - 181 EP - 186 VL - 66 VL - 66 IS - 2 DO - 10.2298/HEMIND111027090B ER -
@article{ author = "Barudžija, Tanja and Gusev, Alexey A. and Jugović, Dragana and Dramićanin, Miroslav and Zdujić, Miodrag and Jovalekić, Čedomir and Mitrić, Miodrag", year = "2012", url = "http://dais.sanu.ac.rs/123456789/257", abstract = "Nano-sized titanium monoxide (TiO) powder was prepared by mechanochemical synthesis. A mixture of commercial Ti and TiO2 (rutile) powders with the molar ratio of 1:1 was milled in a planetary ball mill for 5, 10, 20, 30 and 60 min under argon atmosphere. The final single-phase titanium monoxide sample was characterized by X-ray diffraction (XRD), magnetic measurements using a superconducting quantum interference device magnetometer (SQUID) and thermogravimetric analysis (TGA). The temperature dependency of the magnetic susceptibility is characterized by significant contribution of Pauli paramagnetism due to conduction electrons.", publisher = "Belgrade : Association of the Chemical Engineers of Serbia", journal = "Hemijska industrija", title = "Structural and magnetic properties of mechanochemically synthesized nanocrystalline titanium monoxide", pages = "181-186", volume = "66, 66", number = "2", doi = "10.2298/HEMIND111027090B" }
Barudžija T, Gusev AA, Jugović D, Dramićanin M, Zdujić M, Jovalekić Č, Mitrić M. Structural and magnetic properties of mechanochemically synthesized nanocrystalline titanium monoxide. Hemijska industrija. 2012;66(2):181-186
Barudžija, T., Gusev, A. A., Jugović, D., Dramićanin, M., Zdujić, M., Jovalekić, Č.,& Mitrić, M. (2012). Structural and magnetic properties of mechanochemically synthesized nanocrystalline titanium monoxide. Hemijska industrijaBelgrade : Association of the Chemical Engineers of Serbia., 66(2), 181-186. https://doi.org/10.2298/HEMIND111027090B
Barudžija Tanja, Gusev Alexey A., Jugović Dragana, Dramićanin Miroslav, Zdujić Miodrag, Jovalekić Čedomir, Mitrić Miodrag, "Structural and magnetic properties of mechanochemically synthesized nanocrystalline titanium monoxide" 66, no. 2 (2012):181-186, https://doi.org/10.2298/HEMIND111027090B .