Two step sintering of ZnTiO3 nanopowder

2017
Authors
Labus, Nebojša
Vasiljević, Zorka Ž.

Vasiljević Radović, Dana

Rakić, Srđan
Nikolić, Maria Vesna

Article (Published version)
Metadata
Show full item recordAbstract
Metastable nanopowder ZnTiO3 was pressed into cylindrical compacts at 200 MPa. Compacts were treated by conventional heating with isothermal holding at 931°C for 10 minutes, 25 minutes and 40 minutes. ZnTiO3 compacts were also heated with a two-step sintering schedule with maximal 913°C and isothermal holding at 896°C, for approximately the same holding times as the isothermal schedule. Shrinkage during heating was monitored with a dilatometric device, while microstructure was determined with atomic force microscopy. XRD patterns were collected for the most interesting samples. Microstructures of sintered specimens showed differences introduced during the last sintering stage by the two different heating schedules. Goal of the presented work was to discuss the possible sintering mechanisms for the two step sintering schedulle according to the presented results
Keywords:
zinc titanate / two-step sintering / ZnTiO3 / nanopowdersSource:
Science of Sintering, 2017, 49, 1, 51-60Publisher:
- Belgrade : International Institute for the Science of Sintering
Funding / projects:
DOI: 10.2298/SOS1701051L
ISSN: 0350-820X (Print); 1820-7413 (Online)
WoS: 000399406900005
Scopus: 2-s2.0-85017174871
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - JOUR AU - Labus, Nebojša AU - Vasiljević, Zorka Ž. AU - Vasiljević Radović, Dana AU - Rakić, Srđan AU - Nikolić, Maria Vesna PY - 2017 UR - https://dais.sanu.ac.rs/123456789/2364 AB - Metastable nanopowder ZnTiO3 was pressed into cylindrical compacts at 200 MPa. Compacts were treated by conventional heating with isothermal holding at 931°C for 10 minutes, 25 minutes and 40 minutes. ZnTiO3 compacts were also heated with a two-step sintering schedule with maximal 913°C and isothermal holding at 896°C, for approximately the same holding times as the isothermal schedule. Shrinkage during heating was monitored with a dilatometric device, while microstructure was determined with atomic force microscopy. XRD patterns were collected for the most interesting samples. Microstructures of sintered specimens showed differences introduced during the last sintering stage by the two different heating schedules. Goal of the presented work was to discuss the possible sintering mechanisms for the two step sintering schedulle according to the presented results PB - Belgrade : International Institute for the Science of Sintering T2 - Science of Sintering T1 - Two step sintering of ZnTiO3 nanopowder SP - 51 EP - 60 VL - 49 IS - 1 DO - 10.2298/SOS1701051L UR - https://hdl.handle.net/21.15107/rcub_dais_2364 ER -
@article{ author = "Labus, Nebojša and Vasiljević, Zorka Ž. and Vasiljević Radović, Dana and Rakić, Srđan and Nikolić, Maria Vesna", year = "2017", abstract = "Metastable nanopowder ZnTiO3 was pressed into cylindrical compacts at 200 MPa. Compacts were treated by conventional heating with isothermal holding at 931°C for 10 minutes, 25 minutes and 40 minutes. ZnTiO3 compacts were also heated with a two-step sintering schedule with maximal 913°C and isothermal holding at 896°C, for approximately the same holding times as the isothermal schedule. Shrinkage during heating was monitored with a dilatometric device, while microstructure was determined with atomic force microscopy. XRD patterns were collected for the most interesting samples. Microstructures of sintered specimens showed differences introduced during the last sintering stage by the two different heating schedules. Goal of the presented work was to discuss the possible sintering mechanisms for the two step sintering schedulle according to the presented results", publisher = "Belgrade : International Institute for the Science of Sintering", journal = "Science of Sintering", title = "Two step sintering of ZnTiO3 nanopowder", pages = "51-60", volume = "49", number = "1", doi = "10.2298/SOS1701051L", url = "https://hdl.handle.net/21.15107/rcub_dais_2364" }
Labus, N., Vasiljević, Z. Ž., Vasiljević Radović, D., Rakić, S.,& Nikolić, M. V.. (2017). Two step sintering of ZnTiO3 nanopowder. in Science of Sintering Belgrade : International Institute for the Science of Sintering., 49(1), 51-60. https://doi.org/10.2298/SOS1701051L https://hdl.handle.net/21.15107/rcub_dais_2364
Labus N, Vasiljević ZŽ, Vasiljević Radović D, Rakić S, Nikolić MV. Two step sintering of ZnTiO3 nanopowder. in Science of Sintering. 2017;49(1):51-60. doi:10.2298/SOS1701051L https://hdl.handle.net/21.15107/rcub_dais_2364 .
Labus, Nebojša, Vasiljević, Zorka Ž., Vasiljević Radović, Dana, Rakić, Srđan, Nikolić, Maria Vesna, "Two step sintering of ZnTiO3 nanopowder" in Science of Sintering, 49, no. 1 (2017):51-60, https://doi.org/10.2298/SOS1701051L ., https://hdl.handle.net/21.15107/rcub_dais_2364 .