Metastable nanopowder ZnTiO3 was pressed into cylindrical compacts at 200 MPa. Compacts were treated by conventional heating with isothermal holding at 931°C for 10 minutes, 25 minutes and 40 minutes. ZnTiO3 compacts were also heated with a two-step sintering schedule with maximal 913°C and isothermal holding at 896°C, for approximately the same holding times as the isothermal schedule. Shrinkage during heating was monitored with a dilatometric device, while microstructure was determined with atomic force microscopy. XRD patterns were collected for the most interesting samples. Microstructures of sintered specimens showed differences introduced during the last sintering stage by the two different heating schedules. Goal of the presented work was to discuss the possible sintering mechanisms for the two step sintering schedulle according to the presented results
TY - JOUR
AU - Labus, Nebojša
AU - Vasiljević, Zorka Ž.
AU - Vasiljević Radović, Dana
AU - Rakić, Srđan
AU - Nikolić, Maria Vesna
PY - 2017
UR - http://dais.sanu.ac.rs/123456789/2364
AB - Metastable nanopowder ZnTiO3 was pressed into cylindrical compacts at 200 MPa. Compacts were treated by conventional heating with isothermal holding at 931°C for 10 minutes, 25 minutes and 40 minutes. ZnTiO3 compacts were also heated with a two-step sintering schedule with maximal 913°C and isothermal holding at 896°C, for approximately the same holding times as the isothermal schedule. Shrinkage during heating was monitored with a dilatometric device, while microstructure was determined with atomic force microscopy. XRD patterns were collected for the most interesting samples. Microstructures of sintered specimens showed differences introduced during the last sintering stage by the two different heating schedules. Goal of the presented work was to discuss the possible sintering mechanisms for the two step sintering schedulle according to the presented results
PB - Belgrade : International Institute for the Science of Sintering
T2 - Science of Sintering
T1 - Two step sintering of ZnTiO3 nanopowder
SP - 51
EP - 60
VL - 49
IS - 1
DO - 10.2298/SOS1701051L
ER -
@article{
author = "Labus, Nebojša and Vasiljević, Zorka Ž. and Vasiljević Radović, Dana and Rakić, Srđan and Nikolić, Maria Vesna",
year = "2017",
url = "http://dais.sanu.ac.rs/123456789/2364",
abstract = "Metastable nanopowder ZnTiO3 was pressed into cylindrical compacts at 200 MPa. Compacts were treated by conventional heating with isothermal holding at 931°C for 10 minutes, 25 minutes and 40 minutes. ZnTiO3 compacts were also heated with a two-step sintering schedule with maximal 913°C and isothermal holding at 896°C, for approximately the same holding times as the isothermal schedule. Shrinkage during heating was monitored with a dilatometric device, while microstructure was determined with atomic force microscopy. XRD patterns were collected for the most interesting samples. Microstructures of sintered specimens showed differences introduced during the last sintering stage by the two different heating schedules. Goal of the presented work was to discuss the possible sintering mechanisms for the two step sintering schedulle according to the presented results",
publisher = "Belgrade : International Institute for the Science of Sintering",
journal = "Science of Sintering",
title = "Two step sintering of ZnTiO3 nanopowder",
pages = "51-60",
volume = "49",
number = "1",
doi = "10.2298/SOS1701051L"
}
Labus N, Vasiljević ZŽ, Vasiljević Radović D, Rakić S, Nikolić MV. Two step sintering of ZnTiO3 nanopowder. Science of Sintering. 2017;49(1):51-60
Labus, N., Vasiljević, Z. Ž., Vasiljević Radović, D., Rakić, S.,& Nikolić, M. V. (2017). Two step sintering of ZnTiO3 nanopowder.
Science of SinteringBelgrade : International Institute for the Science of Sintering., 49(1), 51-60.
https://doi.org/10.2298/SOS1701051L
Labus Nebojša, Vasiljević Zorka Ž., Vasiljević Radović Dana, Rakić Srđan, Nikolić Maria Vesna, "Two step sintering of ZnTiO3 nanopowder" 49, no. 1 (2017):51-60,
https://doi.org/10.2298/SOS1701051L .
