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Structure analysis of geopolymers synthesized from clay originated from Serbia

Authorized Users Only
2017
Authors
Nenadović, Snežana S.
Kljajević, Ljiljana M.
Nešić, Maja A.
Petković, Marijana
Trivunac, Katarina V.
Pavlović, Vladimir B.
Article (Published version)
Metadata
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Abstract
The paper presents chemical and structural analysis of geopolymer materials which are obtained by alkali-activated calcined clay (metakaolin) originated from Serbia under strictly defined conditions. Characterization of the metakaolin and geopolymers molecular structure has been done using X-ray diffraction, scanning electron microscope, Fourier transform infrared spectroscopy and matrix-assisted laser desorption ionization time-of-flight mass spectrometry. The paper presents the possibility of obtaining geopolymer structure and differences in chemical and structural characterization of these materials taking into account the concentration of NaOH as a variable parameter. The results of MALDI analysis of metakaolin and synthesized geopolymer structures using various matrix system: 2,4,6 trihydroxyacetophenone (THAP), α-cyano-4-hydroxycinnamic, 2,6 dihydroxyacetophenone and laser desorption/ionization, have shown that THAP matrix is the most appropriate for analysing these aluminosilica...te materials.

Keywords:
geopolymers / porous materials / MALDI-TOF / FTIR
Source:
Environmental Earth Sciences, 2017, 79, 76-
Publisher:
  • Springer
Funding / projects:
  • Synthesis, processing and characterization of nanostructured materials for application in the field of energy, mechanical engineering, environmental protection and biomedicine (RS-45012)
  • Mechanistic studies of the reactions of transition metal ion complexes with biologically relevant molecules (RS-172011)
  • COST Action CM1302 - European Network on Smart Inorganic Polymers (SIPs)

DOI: 10.1007/s12665-016-6360-4

ISSN: 1866-6299 (Online); 1866-6280 (Print)

WoS: 000393021400021

Scopus: 2-s2.0-85009159733
[ Google Scholar ]
21
14
Handle
https://hdl.handle.net/21.15107/rcub_dais_2348
URI
https://dais.sanu.ac.rs/123456789/2348
Collections
  • ИТН САНУ - Општа колекција / ITS SASA - General collection
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - JOUR
AU  - Nenadović, Snežana S.
AU  - Kljajević, Ljiljana M.
AU  - Nešić, Maja A.
AU  - Petković, Marijana
AU  - Trivunac, Katarina V.
AU  - Pavlović, Vladimir B.
PY  - 2017
UR  - https://dais.sanu.ac.rs/123456789/2348
AB  - The paper presents chemical and structural analysis of geopolymer materials which are obtained by alkali-activated calcined clay (metakaolin) originated from Serbia under strictly defined conditions. Characterization of the metakaolin and geopolymers molecular structure has been done using X-ray diffraction, scanning electron microscope, Fourier transform infrared spectroscopy and matrix-assisted laser desorption ionization time-of-flight mass spectrometry. The paper presents the possibility of obtaining geopolymer structure and differences in chemical and structural characterization of these materials taking into account the concentration of NaOH as a variable parameter. The results of MALDI analysis of metakaolin and synthesized geopolymer structures using various matrix system: 2,4,6 trihydroxyacetophenone (THAP), α-cyano-4-hydroxycinnamic, 2,6 dihydroxyacetophenone and laser desorption/ionization, have shown that THAP matrix is the most appropriate for analysing these aluminosilicate materials.
PB  - Springer
T2  - Environmental Earth Sciences
T1  - Structure analysis of geopolymers synthesized from clay originated from Serbia
SP  - 76
VL  - 79
DO  - 10.1007/s12665-016-6360-4
UR  - https://hdl.handle.net/21.15107/rcub_dais_2348
ER  - 
@article{
author = "Nenadović, Snežana S. and Kljajević, Ljiljana M. and Nešić, Maja A. and Petković, Marijana and Trivunac, Katarina V. and Pavlović, Vladimir B.",
year = "2017",
abstract = "The paper presents chemical and structural analysis of geopolymer materials which are obtained by alkali-activated calcined clay (metakaolin) originated from Serbia under strictly defined conditions. Characterization of the metakaolin and geopolymers molecular structure has been done using X-ray diffraction, scanning electron microscope, Fourier transform infrared spectroscopy and matrix-assisted laser desorption ionization time-of-flight mass spectrometry. The paper presents the possibility of obtaining geopolymer structure and differences in chemical and structural characterization of these materials taking into account the concentration of NaOH as a variable parameter. The results of MALDI analysis of metakaolin and synthesized geopolymer structures using various matrix system: 2,4,6 trihydroxyacetophenone (THAP), α-cyano-4-hydroxycinnamic, 2,6 dihydroxyacetophenone and laser desorption/ionization, have shown that THAP matrix is the most appropriate for analysing these aluminosilicate materials.",
publisher = "Springer",
journal = "Environmental Earth Sciences",
title = "Structure analysis of geopolymers synthesized from clay originated from Serbia",
pages = "76",
volume = "79",
doi = "10.1007/s12665-016-6360-4",
url = "https://hdl.handle.net/21.15107/rcub_dais_2348"
}
Nenadović, S. S., Kljajević, L. M., Nešić, M. A., Petković, M., Trivunac, K. V.,& Pavlović, V. B.. (2017). Structure analysis of geopolymers synthesized from clay originated from Serbia. in Environmental Earth Sciences
Springer., 79, 76.
https://doi.org/10.1007/s12665-016-6360-4
https://hdl.handle.net/21.15107/rcub_dais_2348
Nenadović SS, Kljajević LM, Nešić MA, Petković M, Trivunac KV, Pavlović VB. Structure analysis of geopolymers synthesized from clay originated from Serbia. in Environmental Earth Sciences. 2017;79:76.
doi:10.1007/s12665-016-6360-4
https://hdl.handle.net/21.15107/rcub_dais_2348 .
Nenadović, Snežana S., Kljajević, Ljiljana M., Nešić, Maja A., Petković, Marijana, Trivunac, Katarina V., Pavlović, Vladimir B., "Structure analysis of geopolymers synthesized from clay originated from Serbia" in Environmental Earth Sciences, 79 (2017):76,
https://doi.org/10.1007/s12665-016-6360-4 .,
https://hdl.handle.net/21.15107/rcub_dais_2348 .

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