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ZnTiO3 ceramic nanopowder microstructure changes during compaction

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2013
186.pdf (765.7Kb)
Authors
Labus, Nebojša
Krstić, Jugoslav
Marković, Smilja
Vasiljević Radović, Dana
Nikolić, Maria Vesna
Pavlović, V.
Article (Published version)
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Abstract
ZnTiO3 nanopowder as a constitutive component in compact production was primarily characterized. Scanning electron micrographs of as received powder were recorded. Mercury porosimetry and nitrogen adsorption were also performed on loose powder. Particle size distribution in a water powder suspension was determined with a laser particle size analyser. Compaction was performed on different pressures in a range from 100 to 400 MPa using the uniaxial double sided compaction technique without binder and lubricant. Micrographs of compacted specimens were obtained using scanning electron microscopy and atomic force microscopy. Pore size distribution was also determined by mercury porosimetry and nitrogen adsorption. Results revealed that with increasing pressure during compaction interagglomerate pores diminish in size until they reach some critical diameter related to the intra-agglomerate pore size.
Keywords:
compaction / nanopowders / pore size distribution / nitrogen adsorption / mercury porosimetry / ZnTiO3 / zinc titanate
Source:
Science of Sintering, 2013, 45, 2, 209-221
Publisher:
  • Belgrade : International Institute for the Science of Sintering
Funding / projects:
  • Directed synthesis, structure and properties of multifunctional materials (RS-172057)

DOI: 10.2298/SOS1302209L

ISSN: 1820-7413 (Online); 0350-820X

WoS: 000323550700010

Scopus: 2-s2.0-84881537663
[ Google Scholar ]
5
4
Handle
https://hdl.handle.net/21.15107/rcub_dais_189
URI
https://dais.sanu.ac.rs/123456789/189
Collections
  • ИТН САНУ - Општа колекција / ITS SASA - General collection
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - JOUR
AU  - Labus, Nebojša
AU  - Krstić, Jugoslav
AU  - Marković, Smilja
AU  - Vasiljević Radović, Dana
AU  - Nikolić, Maria Vesna
AU  - Pavlović, V.
PY  - 2013
UR  - https://dais.sanu.ac.rs/123456789/189
AB  - ZnTiO3 nanopowder as a constitutive component in compact production was primarily characterized. Scanning electron micrographs of as received powder were recorded. Mercury porosimetry and nitrogen adsorption were also performed on loose powder. Particle size distribution in a water powder suspension was determined with a laser particle size analyser. Compaction was performed on different pressures in a range from 100 to 400 MPa using the uniaxial double sided compaction technique without binder and lubricant. Micrographs of compacted specimens were obtained using scanning electron microscopy and atomic force microscopy. Pore size distribution was also determined by mercury porosimetry and nitrogen adsorption. Results revealed that with increasing pressure during compaction interagglomerate pores diminish in size until they reach some critical diameter related to the intra-agglomerate pore size.
PB  - Belgrade : International Institute for the Science of Sintering
T2  - Science of Sintering
T1  - ZnTiO3 ceramic nanopowder microstructure changes during compaction
SP  - 209
EP  - 221
VL  - 45
IS  - 2
DO  - 10.2298/SOS1302209L
UR  - https://hdl.handle.net/21.15107/rcub_dais_189
ER  - 
@article{
author = "Labus, Nebojša and Krstić, Jugoslav and Marković, Smilja and Vasiljević Radović, Dana and Nikolić, Maria Vesna and Pavlović, V.",
year = "2013",
abstract = "ZnTiO3 nanopowder as a constitutive component in compact production was primarily characterized. Scanning electron micrographs of as received powder were recorded. Mercury porosimetry and nitrogen adsorption were also performed on loose powder. Particle size distribution in a water powder suspension was determined with a laser particle size analyser. Compaction was performed on different pressures in a range from 100 to 400 MPa using the uniaxial double sided compaction technique without binder and lubricant. Micrographs of compacted specimens were obtained using scanning electron microscopy and atomic force microscopy. Pore size distribution was also determined by mercury porosimetry and nitrogen adsorption. Results revealed that with increasing pressure during compaction interagglomerate pores diminish in size until they reach some critical diameter related to the intra-agglomerate pore size.",
publisher = "Belgrade : International Institute for the Science of Sintering",
journal = "Science of Sintering",
title = "ZnTiO3 ceramic nanopowder microstructure changes during compaction",
pages = "209-221",
volume = "45",
number = "2",
doi = "10.2298/SOS1302209L",
url = "https://hdl.handle.net/21.15107/rcub_dais_189"
}
Labus, N., Krstić, J., Marković, S., Vasiljević Radović, D., Nikolić, M. V.,& Pavlović, V.. (2013). ZnTiO3 ceramic nanopowder microstructure changes during compaction. in Science of Sintering
Belgrade : International Institute for the Science of Sintering., 45(2), 209-221.
https://doi.org/10.2298/SOS1302209L
https://hdl.handle.net/21.15107/rcub_dais_189
Labus N, Krstić J, Marković S, Vasiljević Radović D, Nikolić MV, Pavlović V. ZnTiO3 ceramic nanopowder microstructure changes during compaction. in Science of Sintering. 2013;45(2):209-221.
doi:10.2298/SOS1302209L
https://hdl.handle.net/21.15107/rcub_dais_189 .
Labus, Nebojša, Krstić, Jugoslav, Marković, Smilja, Vasiljević Radović, Dana, Nikolić, Maria Vesna, Pavlović, V., "ZnTiO3 ceramic nanopowder microstructure changes during compaction" in Science of Sintering, 45, no. 2 (2013):209-221,
https://doi.org/10.2298/SOS1302209L .,
https://hdl.handle.net/21.15107/rcub_dais_189 .

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