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Synthesis and structural characterization of some cathode materials for lithium-ion batteries

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Authors
Jugović, Dragana
Contributors
Gadow, Rainer
Mitic, Vojislav V.
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Abstract
Lithium-ion batteries are under intense scrutiny as alternative energy/power sources. Their electrochemistry is based on intercalation/deintercalation reactions of lithium ions within a crystal structure of an electrode material. Therefore, the structure itself determines both the electrode operating voltage and the transport pathways for lithium ions. Some oxide- and polyanion-based materials are synthesized by using ultrasonic spray pyrolysis method. The crystal structure refinement was based on the Rietveld full profile method. All relevant structural and microstructural crystal parameters that could be significant for electrochemical intercalation/deintercalation processes were determined. It was also shown that the structural and microstructural properties are significantly dependent on the synthesis condition. Electrochemical performances as cathode materials for lithium-ion batteries were examined through galvanostatic charge/discharge cycling. Galvanostatic cycling revealed var...iation in discharge curve profiles. It comes from different mechanism of lithium intercalation and also from the degree of structural order. Structural analyses revealed difference in the dimensionality of lithium-ion motion.

Keywords:
cathode materials / lithium-ion batteries / galvanostatic cycling
Source:
Advanced Ceramics and Applications, 2021, 123-154
Publisher:
  • Walter de Gruyter GmbH
Funding / projects:
  • Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 200175 (Institute of Technical Sciences of SASA, Belgrade) (RS-200175)

DOI: 10.1515/9783110627992-011

ISBN: 9783110627992

[ Google Scholar ]
Handle
https://hdl.handle.net/21.15107/rcub_dais_12400
URI
https://dais.sanu.ac.rs/123456789/12400
Collections
  • ИТН САНУ - Општа колекција / ITS SASA - General collection
Institution/Community
Институт техничких наука САНУ / Institute of Technical Sciences of SASA
TY  - CHAP
AU  - Jugović, Dragana
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/12400
AB  - Lithium-ion batteries are under intense scrutiny as alternative energy/power sources. Their electrochemistry is based on intercalation/deintercalation reactions of lithium ions within a crystal structure of an electrode material. Therefore, the structure itself determines both the electrode operating voltage and the transport pathways for lithium ions. Some oxide- and polyanion-based materials are synthesized by using ultrasonic spray pyrolysis method. The crystal structure refinement was based on the Rietveld full profile method. All relevant structural and microstructural crystal parameters that could be significant for electrochemical intercalation/deintercalation processes were determined. It was also shown that the structural and microstructural properties are significantly dependent on the synthesis condition. Electrochemical performances as cathode materials for lithium-ion batteries were examined through galvanostatic charge/discharge cycling. Galvanostatic cycling revealed variation in discharge curve profiles. It comes from different mechanism of lithium intercalation and also from the degree of structural order. Structural analyses revealed difference in the dimensionality of lithium-ion motion.
PB  - Walter de Gruyter GmbH
T2  - Advanced Ceramics and Applications
T1  - Synthesis and structural characterization of some cathode materials for lithium-ion batteries
SP  - 123
EP  - 154
DO  - 10.1515/9783110627992-011
UR  - https://hdl.handle.net/21.15107/rcub_dais_12400
ER  - 
@inbook{
editor = "Gadow, Rainer, Mitic, Vojislav V.",
author = "Jugović, Dragana",
year = "2021",
abstract = "Lithium-ion batteries are under intense scrutiny as alternative energy/power sources. Their electrochemistry is based on intercalation/deintercalation reactions of lithium ions within a crystal structure of an electrode material. Therefore, the structure itself determines both the electrode operating voltage and the transport pathways for lithium ions. Some oxide- and polyanion-based materials are synthesized by using ultrasonic spray pyrolysis method. The crystal structure refinement was based on the Rietveld full profile method. All relevant structural and microstructural crystal parameters that could be significant for electrochemical intercalation/deintercalation processes were determined. It was also shown that the structural and microstructural properties are significantly dependent on the synthesis condition. Electrochemical performances as cathode materials for lithium-ion batteries were examined through galvanostatic charge/discharge cycling. Galvanostatic cycling revealed variation in discharge curve profiles. It comes from different mechanism of lithium intercalation and also from the degree of structural order. Structural analyses revealed difference in the dimensionality of lithium-ion motion.",
publisher = "Walter de Gruyter GmbH",
journal = "Advanced Ceramics and Applications",
booktitle = "Synthesis and structural characterization of some cathode materials for lithium-ion batteries",
pages = "123-154",
doi = "10.1515/9783110627992-011",
url = "https://hdl.handle.net/21.15107/rcub_dais_12400"
}
Gadow, R., Mitic, V. V.,& Jugović, D.. (2021). Synthesis and structural characterization of some cathode materials for lithium-ion batteries. in Advanced Ceramics and Applications
Walter de Gruyter GmbH., 123-154.
https://doi.org/10.1515/9783110627992-011
https://hdl.handle.net/21.15107/rcub_dais_12400
Gadow R, Mitic VV, Jugović D. Synthesis and structural characterization of some cathode materials for lithium-ion batteries. in Advanced Ceramics and Applications. 2021;:123-154.
doi:10.1515/9783110627992-011
https://hdl.handle.net/21.15107/rcub_dais_12400 .
Gadow, Rainer, Mitic, Vojislav V., Jugović, Dragana, "Synthesis and structural characterization of some cathode materials for lithium-ion batteries" in Advanced Ceramics and Applications (2021):123-154,
https://doi.org/10.1515/9783110627992-011 .,
https://hdl.handle.net/21.15107/rcub_dais_12400 .

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