Study of the Synthesis, Structure and Activity of Natural and Synthetic Organic Compounds

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Study of the Synthesis, Structure and Activity of Natural and Synthetic Organic Compounds (en)
Проучавање синтезе, структуре и активности органских једињења природног и синтетског порекла (sr)
Proučavanje sinteze, strukture i aktivnosti organskih jedinjenja prirodnog i sintetskog porekla (sr_RS)
Authors

Publications

On the synthesis of 3-cyano-6-hydroxy-4-methyl-2-pyridone at room temperature

Zdujić, Miodrag; Petrović, Slobodan D.; Valentić, Nataša V.; Mijin, Dušan

(Belgrade : Engineers Society of Corrosion, 2019)

TY  - JOUR
AU  - Zdujić, Miodrag
AU  - Petrović, Slobodan D.
AU  - Valentić, Nataša V.
AU  - Mijin, Dušan
PY  - 2019
UR  - https://scindeks.ceon.rs/article.aspx?artid=0351-94651903229Z
UR  - http://www.ncbi.nlm.nih.gov/pubmed/0351-94651903229Z
UR  - http://dais.sanu.ac.rs/123456789/6954
AB  - Milling of cyanoacetamide and acetoacetic ester as reactants, in the presence of KOH as the catalyst and ethanol as a viscous control agent (VCA) was performed in a planetary ball mill with the goal of investigating the effect of mechanochemical treatment for the synthesis of 3-cyano-6hydroxy-4-methyl-2-pyridone at room temperature. The mechanochemical synthesis was performed under various milling parameters, i.e. milling time up to 4 h, number and size of balls, angular velocity as well as molar ratio of reactants and the amount of catalyst. The obtained product was characterized by m.p., UV, IR and NMR data. It was fond that the dominant process parameter is the milling time while others are of less importance. The highest isolated yield after milling was up to 56%. The combination of milling and aging increase yield over 60%.
PB  - Belgrade : Engineers Society of Corrosion
T2  - Zaštita materijala
T1  - On the synthesis of 3-cyano-6-hydroxy-4-methyl-2-pyridone at room temperature
SP  - 229
EP  - 236
VL  - 60
IS  - 3
DO  - 10.5937/zasmat1903229Z
UR  - https://hdl.handle.net/21.15107/rcub_dais_6954
ER  - 
@article{
author = "Zdujić, Miodrag and Petrović, Slobodan D. and Valentić, Nataša V. and Mijin, Dušan",
year = "2019",
abstract = "Milling of cyanoacetamide and acetoacetic ester as reactants, in the presence of KOH as the catalyst and ethanol as a viscous control agent (VCA) was performed in a planetary ball mill with the goal of investigating the effect of mechanochemical treatment for the synthesis of 3-cyano-6hydroxy-4-methyl-2-pyridone at room temperature. The mechanochemical synthesis was performed under various milling parameters, i.e. milling time up to 4 h, number and size of balls, angular velocity as well as molar ratio of reactants and the amount of catalyst. The obtained product was characterized by m.p., UV, IR and NMR data. It was fond that the dominant process parameter is the milling time while others are of less importance. The highest isolated yield after milling was up to 56%. The combination of milling and aging increase yield over 60%.",
publisher = "Belgrade : Engineers Society of Corrosion",
journal = "Zaštita materijala",
title = "On the synthesis of 3-cyano-6-hydroxy-4-methyl-2-pyridone at room temperature",
pages = "229-236",
volume = "60",
number = "3",
doi = "10.5937/zasmat1903229Z",
url = "https://hdl.handle.net/21.15107/rcub_dais_6954"
}
Zdujić, M., Petrović, S. D., Valentić, N. V.,& Mijin, D.. (2019). On the synthesis of 3-cyano-6-hydroxy-4-methyl-2-pyridone at room temperature. in Zaštita materijala
Belgrade : Engineers Society of Corrosion., 60(3), 229-236.
https://doi.org/10.5937/zasmat1903229Z
https://hdl.handle.net/21.15107/rcub_dais_6954
Zdujić M, Petrović SD, Valentić NV, Mijin D. On the synthesis of 3-cyano-6-hydroxy-4-methyl-2-pyridone at room temperature. in Zaštita materijala. 2019;60(3):229-236.
doi:10.5937/zasmat1903229Z
https://hdl.handle.net/21.15107/rcub_dais_6954 .
Zdujić, Miodrag, Petrović, Slobodan D., Valentić, Nataša V., Mijin, Dušan, "On the synthesis of 3-cyano-6-hydroxy-4-methyl-2-pyridone at room temperature" in Zaštita materijala, 60, no. 3 (2019):229-236,
https://doi.org/10.5937/zasmat1903229Z .,
https://hdl.handle.net/21.15107/rcub_dais_6954 .

Distillation products of Stanley plum obtaining

Milojević, Svetomir; Đurović, Boban; Mijailović, Miljojka; Trišović, Tomislav; Vuković, Ivan; Pavićević, Vladimir; Nikolić, Jasmina

(Vrnjačka Banja : Scientific and Technical Center for Intellectual Property, 2014)

TY  - CONF
AU  - Milojević, Svetomir
AU  - Đurović, Boban
AU  - Mijailović, Miljojka
AU  - Trišović, Tomislav
AU  - Vuković, Ivan
AU  - Pavićević, Vladimir
AU  - Nikolić, Jasmina
PY  - 2014
UR  - http://dais.sanu.ac.rs/123456789/586
AB  - The sort of plum used for distillation is Stanley picked in August 2013 in Gračac, Vrnjačka Banja, Serbia. 200 kg of ripe fruit was fermented with 40 dm3 of potable water. Wine was removed from the obtained product, and the solid part was washed with water. The mixture of wine and water, 240 dm was distilled to a soft brandy, where 36 dm3 was obtained with 30 % of ethanol. After that, this soft brandy was redistilled after 44 dm3 of potable water was added. By this procedure, 20 dm3 with 50 % of ethanol was distillated, which means that the yield was 10 dm3 of brandy for 100 kg of plums.
PB  - Vrnjačka Banja : Scientific and Technical Center for Intellectual Property
C3  - 14th International Conference Research and Development in Mechanical Industry - RaDMI 2014, Topola, Serbia, 18-21 September 2014: Proceedings. Vol. 2
T1  - Distillation products of Stanley plum obtaining
SP  - 887
EP  - 892
UR  - https://hdl.handle.net/21.15107/rcub_dais_586
ER  - 
@conference{
author = "Milojević, Svetomir and Đurović, Boban and Mijailović, Miljojka and Trišović, Tomislav and Vuković, Ivan and Pavićević, Vladimir and Nikolić, Jasmina",
year = "2014",
abstract = "The sort of plum used for distillation is Stanley picked in August 2013 in Gračac, Vrnjačka Banja, Serbia. 200 kg of ripe fruit was fermented with 40 dm3 of potable water. Wine was removed from the obtained product, and the solid part was washed with water. The mixture of wine and water, 240 dm was distilled to a soft brandy, where 36 dm3 was obtained with 30 % of ethanol. After that, this soft brandy was redistilled after 44 dm3 of potable water was added. By this procedure, 20 dm3 with 50 % of ethanol was distillated, which means that the yield was 10 dm3 of brandy for 100 kg of plums.",
publisher = "Vrnjačka Banja : Scientific and Technical Center for Intellectual Property",
journal = "14th International Conference Research and Development in Mechanical Industry - RaDMI 2014, Topola, Serbia, 18-21 September 2014: Proceedings. Vol. 2",
title = "Distillation products of Stanley plum obtaining",
pages = "887-892",
url = "https://hdl.handle.net/21.15107/rcub_dais_586"
}
Milojević, S., Đurović, B., Mijailović, M., Trišović, T., Vuković, I., Pavićević, V.,& Nikolić, J.. (2014). Distillation products of Stanley plum obtaining. in 14th International Conference Research and Development in Mechanical Industry - RaDMI 2014, Topola, Serbia, 18-21 September 2014: Proceedings. Vol. 2
Vrnjačka Banja : Scientific and Technical Center for Intellectual Property., 887-892.
https://hdl.handle.net/21.15107/rcub_dais_586
Milojević S, Đurović B, Mijailović M, Trišović T, Vuković I, Pavićević V, Nikolić J. Distillation products of Stanley plum obtaining. in 14th International Conference Research and Development in Mechanical Industry - RaDMI 2014, Topola, Serbia, 18-21 September 2014: Proceedings. Vol. 2. 2014;:887-892.
https://hdl.handle.net/21.15107/rcub_dais_586 .
Milojević, Svetomir, Đurović, Boban, Mijailović, Miljojka, Trišović, Tomislav, Vuković, Ivan, Pavićević, Vladimir, Nikolić, Jasmina, "Distillation products of Stanley plum obtaining" in 14th International Conference Research and Development in Mechanical Industry - RaDMI 2014, Topola, Serbia, 18-21 September 2014: Proceedings. Vol. 2 (2014):887-892,
https://hdl.handle.net/21.15107/rcub_dais_586 .