TY  - JOUR
AU  - Jeremić, Dejan
AU  - Anđelković, Ljubica
AU  - Milenković, Milica R.
AU  - Šuljagić, Marija
AU  - Šumar Ristović, Maja
AU  - Ostojić, Sanja
AU  - Nikolić, Aleksandar S.
AU  - Vulić, Predrag
AU  - Brčeski, Ilija
AU  - Pavlović, Vladimir B.
PY  - 2020
UR  - https://dais.sanu.ac.rs/123456789/12085
AB  - This work is the first report of a very simple and fast one-pot synthesis of nickel oxide (NiO) and hematite (α-Fe2O3) nanoparticles by thermal decomposition of transition metal aqua complexes with camphor sulfonate anions. Obtained nanopowders were characterized by X-ray powder diffraction, Fourier transform IR analysis, scanning electron microscopy, and Energy-dispersive X-ray spectroscopy. X-ray powder diffraction confirmed the formation of high purity NiO and α-Fe2O3 crystal phases. In the case of α-Fe2O3, about five times larger average crystallite size was obtained. Fourier transform IR spectra of synthesized materials showed characteristic peaks for NiO and α-Fe2O3 nanostructures. To visualize the morphology and the chemical composition of the final products Scanning electron microscopy and Energy-dispersive X-ray spectroscopy were performed. The thermogravimetric analysis was done for a better understanding of the general thermal behavior of precursor compounds. This easy-to-perform and fast preparation method opens a broad range of obtained materials’ usage, particularly due to its economic viability
T2  - Science of Sintering
T1  - One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles
SP  - 481
EP  - 490
VL  - 52
IS  - 4
DO  - 10.2298/SOS2004481J
UR  - https://hdl.handle.net/21.15107/rcub_dais_12085
ER  - 

@article{
author = "Jeremić, Dejan and Anđelković, Ljubica and Milenković, Milica R. and Šuljagić, Marija and Šumar Ristović, Maja and Ostojić, Sanja and Nikolić, Aleksandar S. and Vulić, Predrag and Brčeski, Ilija and Pavlović, Vladimir B.",
year = "2020",
abstract = "This work is the first report of a very simple and fast one-pot synthesis of nickel oxide (NiO) and hematite (α-Fe2O3) nanoparticles by thermal decomposition of transition metal aqua complexes with camphor sulfonate anions. Obtained nanopowders were characterized by X-ray powder diffraction, Fourier transform IR analysis, scanning electron microscopy, and Energy-dispersive X-ray spectroscopy. X-ray powder diffraction confirmed the formation of high purity NiO and α-Fe2O3 crystal phases. In the case of α-Fe2O3, about five times larger average crystallite size was obtained. Fourier transform IR spectra of synthesized materials showed characteristic peaks for NiO and α-Fe2O3 nanostructures. To visualize the morphology and the chemical composition of the final products Scanning electron microscopy and Energy-dispersive X-ray spectroscopy were performed. The thermogravimetric analysis was done for a better understanding of the general thermal behavior of precursor compounds. This easy-to-perform and fast preparation method opens a broad range of obtained materials’ usage, particularly due to its economic viability",
journal = "Science of Sintering",
title = "One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles",
pages = "481-490",
volume = "52",
number = "4",
doi = "10.2298/SOS2004481J",
url = "https://hdl.handle.net/21.15107/rcub_dais_12085"
}

Jeremić, D., Anđelković, L., Milenković, M. R., Šuljagić, M., Šumar Ristović, M., Ostojić, S., Nikolić, A. S., Vulić, P., Brčeski, I.,& Pavlović, V. B.. (2020). One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles. in Science of Sintering, 52(4), 481-490.
https://doi.org/10.2298/SOS2004481J
https://hdl.handle.net/21.15107/rcub_dais_12085

Jeremić D, Anđelković L, Milenković MR, Šuljagić M, Šumar Ristović M, Ostojić S, Nikolić AS, Vulić P, Brčeski I, Pavlović VB. One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles. in Science of Sintering. 2020;52(4):481-490.
doi:10.2298/SOS2004481J
https://hdl.handle.net/21.15107/rcub_dais_12085 .

Jeremić, Dejan, Anđelković, Ljubica, Milenković, Milica R., Šuljagić, Marija, Šumar Ristović, Maja, Ostojić, Sanja, Nikolić, Aleksandar S., Vulić, Predrag, Brčeski, Ilija, Pavlović, Vladimir B., "One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles" in Science of Sintering, 52, no. 4 (2020):481-490,
https://doi.org/10.2298/SOS2004481J .,
https://hdl.handle.net/21.15107/rcub_dais_12085 .

TY  - JOUR
AU  - Stefanović, Ivan S.
AU  - Dostanić, Jasmina
AU  - Lončarević, Davor
AU  - Vasiljević Radović, Dana
AU  - Ostojić, Sanja
AU  - Marković, Smilja
AU  - Pergal, Marija V.
PY  - 2019
UR  - https://dais.sanu.ac.rs/123456789/5761
AB  - This work is focused on preparation of poly(urethane-siloxane)/titanium-dioxide nanocomposites (PUSNs) with enhanced features. PUSNs were prepared by the in situ polymerization reaction using titanium-dioxide as a nano-filler in different amounts (1, 2, 3 and 5 wt.%) with respect to the poly(urethane-siloxane) (PUS) matrix. PUS copolymer was based on α,ω-dihy-droxy-ethoxypropyl-poly(dimethylsiloxane), 4,4’-methylenediphenyldiisocyanate and 1,4-bu-tanediole. In order to investigate the influence of TiO 2 content on the structure, UV resistance, thermal properties, hydrophobicity and morphology of the prepared PUSNs, FTIR spectroscopy, UV-Vis diffuse-reflectance spectroscopy, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), contact angle measurements, surface free energy (SFE) analysis, water absorption, scanning electron microscopy (SEM) and atomic force microscopy (AFM) were performed. The PUSNs showed excellent UV resistance, high hydrophobicity, low surface free energy and also higher thermal stability and rougher surface and cross-section relief structure as compared to the pure PUS copolymer. Based on the obtained results it can be concluded that prepared PUSNs could be potentially used as protective coatings. © 2019, Association of Chemists and Chemical Engineers of Serbia. All rights reserved.
PB  - Association of the Chemical Engineers of Serbia
T2  - Hemijska industrija
T1  - Preparation and characterization of poly(Urethane-siloxane)/titanium-dioxide nanocomposites
SP  - 13
EP  - 24
VL  - 73
IS  - 1
DO  - 10.2298/HEMIND180530002S
UR  - https://hdl.handle.net/21.15107/rcub_dais_5761
ER  - 

@article{
author = "Stefanović, Ivan S. and Dostanić, Jasmina and Lončarević, Davor and Vasiljević Radović, Dana and Ostojić, Sanja and Marković, Smilja and Pergal, Marija V.",
year = "2019",
abstract = "This work is focused on preparation of poly(urethane-siloxane)/titanium-dioxide nanocomposites (PUSNs) with enhanced features. PUSNs were prepared by the in situ polymerization reaction using titanium-dioxide as a nano-filler in different amounts (1, 2, 3 and 5 wt.%) with respect to the poly(urethane-siloxane) (PUS) matrix. PUS copolymer was based on α,ω-dihy-droxy-ethoxypropyl-poly(dimethylsiloxane), 4,4’-methylenediphenyldiisocyanate and 1,4-bu-tanediole. In order to investigate the influence of TiO 2 content on the structure, UV resistance, thermal properties, hydrophobicity and morphology of the prepared PUSNs, FTIR spectroscopy, UV-Vis diffuse-reflectance spectroscopy, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), contact angle measurements, surface free energy (SFE) analysis, water absorption, scanning electron microscopy (SEM) and atomic force microscopy (AFM) were performed. The PUSNs showed excellent UV resistance, high hydrophobicity, low surface free energy and also higher thermal stability and rougher surface and cross-section relief structure as compared to the pure PUS copolymer. Based on the obtained results it can be concluded that prepared PUSNs could be potentially used as protective coatings. © 2019, Association of Chemists and Chemical Engineers of Serbia. All rights reserved.",
publisher = "Association of the Chemical Engineers of Serbia",
journal = "Hemijska industrija",
title = "Preparation and characterization of poly(Urethane-siloxane)/titanium-dioxide nanocomposites",
pages = "13-24",
volume = "73",
number = "1",
doi = "10.2298/HEMIND180530002S",
url = "https://hdl.handle.net/21.15107/rcub_dais_5761"
}

Stefanović, I. S., Dostanić, J., Lončarević, D., Vasiljević Radović, D., Ostojić, S., Marković, S.,& Pergal, M. V.. (2019). Preparation and characterization of poly(Urethane-siloxane)/titanium-dioxide nanocomposites. in Hemijska industrija
Association of the Chemical Engineers of Serbia., 73(1), 13-24.
https://doi.org/10.2298/HEMIND180530002S
https://hdl.handle.net/21.15107/rcub_dais_5761

Stefanović IS, Dostanić J, Lončarević D, Vasiljević Radović D, Ostojić S, Marković S, Pergal MV. Preparation and characterization of poly(Urethane-siloxane)/titanium-dioxide nanocomposites. in Hemijska industrija. 2019;73(1):13-24.
doi:10.2298/HEMIND180530002S
https://hdl.handle.net/21.15107/rcub_dais_5761 .

Stefanović, Ivan S., Dostanić, Jasmina, Lončarević, Davor, Vasiljević Radović, Dana, Ostojić, Sanja, Marković, Smilja, Pergal, Marija V., "Preparation and characterization of poly(Urethane-siloxane)/titanium-dioxide nanocomposites" in Hemijska industrija, 73, no. 1 (2019):13-24,
https://doi.org/10.2298/HEMIND180530002S .,
https://hdl.handle.net/21.15107/rcub_dais_5761 .