Antić, Vesna

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Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities

Obradović, Nina; Filipović, Suzana; Marković, Smilja; Mitrić, Miodrag; Rusmirović, Jelena; Marinković, Aleksandar; Antić, Vesna; Pavlović, Vladimir B.

(Elsevier, 2017)

TY  - JOUR
AU  - Obradović, Nina
AU  - Filipović, Suzana
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Rusmirović, Jelena
AU  - Marinković, Aleksandar
AU  - Antić, Vesna
AU  - Pavlović, Vladimir B.
PY  - 2017
UR  - https://dais.sanu.ac.rs/123456789/2370
AB  - In this study, porous macro- and micro-cellular wollastonite-based ceramics was synthesized. A ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as a starting material. After 20 min of ultrasound treatment, and calcination at 250 °C for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, the sintering regime was set up. The prepared mixtures were pressed into pallets and sintered at 900 °C. During the sintering regime, porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples, as well as the microstructures, were analyzed by using X-ray diffraction and SEM. A two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that the addition of different pore-forming agents resulted in significantly different microstructures. In a batch test, the influence of pH, the contact time and the initial ion concentration on the adsorption efficiency of As+5, Cr+6and phosphate ions on the synthesized adsorbents were studied. Time-dependent adsorption is best described by the pseudo-second-order kinetic model and the Weber-Morris model, which predict intra-particle diffusion as a rate-controlling step of the overall process. High adsorption capacities, 21.93, 23.88, and 27.29 mg g–1, were obtained for the CaCO3-siloxane-nanocellulose sorbent, and similar/lower capacities were obtained for the CaCO3-siloxane-PMMA and CaCO3-siloxane-cotton wool adsorbents.
PB  - Elsevier
T2  - Ceramics International
T1  - Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities
SP  - 7461
EP  - 7468
VL  - 43
IS  - 10
DO  - 10.1016/j.ceramint.2017.03.021
UR  - https://hdl.handle.net/21.15107/rcub_dais_2370
ER  - 
@article{
author = "Obradović, Nina and Filipović, Suzana and Marković, Smilja and Mitrić, Miodrag and Rusmirović, Jelena and Marinković, Aleksandar and Antić, Vesna and Pavlović, Vladimir B.",
year = "2017",
abstract = "In this study, porous macro- and micro-cellular wollastonite-based ceramics was synthesized. A ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as a starting material. After 20 min of ultrasound treatment, and calcination at 250 °C for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, the sintering regime was set up. The prepared mixtures were pressed into pallets and sintered at 900 °C. During the sintering regime, porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples, as well as the microstructures, were analyzed by using X-ray diffraction and SEM. A two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that the addition of different pore-forming agents resulted in significantly different microstructures. In a batch test, the influence of pH, the contact time and the initial ion concentration on the adsorption efficiency of As+5, Cr+6and phosphate ions on the synthesized adsorbents were studied. Time-dependent adsorption is best described by the pseudo-second-order kinetic model and the Weber-Morris model, which predict intra-particle diffusion as a rate-controlling step of the overall process. High adsorption capacities, 21.93, 23.88, and 27.29 mg g–1, were obtained for the CaCO3-siloxane-nanocellulose sorbent, and similar/lower capacities were obtained for the CaCO3-siloxane-PMMA and CaCO3-siloxane-cotton wool adsorbents.",
publisher = "Elsevier",
journal = "Ceramics International",
title = "Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities",
pages = "7461-7468",
volume = "43",
number = "10",
doi = "10.1016/j.ceramint.2017.03.021",
url = "https://hdl.handle.net/21.15107/rcub_dais_2370"
}
Obradović, N., Filipović, S., Marković, S., Mitrić, M., Rusmirović, J., Marinković, A., Antić, V.,& Pavlović, V. B.. (2017). Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities. in Ceramics International
Elsevier., 43(10), 7461-7468.
https://doi.org/10.1016/j.ceramint.2017.03.021
https://hdl.handle.net/21.15107/rcub_dais_2370
Obradović N, Filipović S, Marković S, Mitrić M, Rusmirović J, Marinković A, Antić V, Pavlović VB. Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities. in Ceramics International. 2017;43(10):7461-7468.
doi:10.1016/j.ceramint.2017.03.021
https://hdl.handle.net/21.15107/rcub_dais_2370 .
Obradović, Nina, Filipović, Suzana, Marković, Smilja, Mitrić, Miodrag, Rusmirović, Jelena, Marinković, Aleksandar, Antić, Vesna, Pavlović, Vladimir B., "Influence of different pore-forming agents on wollastonite microstructures and adsorption capacities" in Ceramics International, 43, no. 10 (2017):7461-7468,
https://doi.org/10.1016/j.ceramint.2017.03.021 .,
https://hdl.handle.net/21.15107/rcub_dais_2370 .
13
13
17

Influence of different pore-forming agents on wollastonite microstructures

Obradović, Nina; Filipović, Suzana; Marković, Smilja; Mitrić, Miodrag; Antić, Vesna; Pavlović, Vladimir B.

(Belgrade : Serbian Ceramic Society, 2016)

TY  - CONF
AU  - Obradović, Nina
AU  - Filipović, Suzana
AU  - Marković, Smilja
AU  - Mitrić, Miodrag
AU  - Antić, Vesna
AU  - Pavlović, Vladimir B.
PY  - 2016
UR  - https://dais.sanu.ac.rs/123456789/874
AB  - In this study, highly porous macro- and micro-cellular wollastonite-based ceramics was synthesized. Ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as starting material. After 20 min of ultrasound treatment, and calcination at 250 oC for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, sintering regime was set up. Prepared mixtures were pressed into pallets and sintered at 900 oC. During the sintering regime, highly porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples as well as microstructures was analyzed by the means of X-ray diffraction method and SEM. Two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that addition of different pore-forming agent resulted in significantly different microstructures.
PB  - Belgrade : Serbian Ceramic Society
C3  - Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts : V Serbian Ceramic Society Conference, Sep 21-23 September 2016, Belgrade
T1  - Influence of different pore-forming agents on wollastonite microstructures
SP  - 42
EP  - 42
UR  - https://hdl.handle.net/21.15107/rcub_dais_874
ER  - 
@conference{
author = "Obradović, Nina and Filipović, Suzana and Marković, Smilja and Mitrić, Miodrag and Antić, Vesna and Pavlović, Vladimir B.",
year = "2016",
abstract = "In this study, highly porous macro- and micro-cellular wollastonite-based ceramics was synthesized. Ceramic precursor, methylhydrocyclosiloxane, together with micro-sized CaCO3, was used as starting material. After 20 min of ultrasound treatment, and calcination at 250 oC for 30 min, different pore-forming agents were added to the as-obtained powders. Differential thermal analysis was used to determine characteristic temperatures of processes occurring within powders during heating. Based on the obtained results, sintering regime was set up. Prepared mixtures were pressed into pallets and sintered at 900 oC. During the sintering regime, highly porous wollastonite-based ceramics was obtained. The phase composition of the sintered samples as well as microstructures was analyzed by the means of X-ray diffraction method and SEM. Two-phase system was detected in all samples, CaSiO3 wollastonite and Ca2SiO4 larnite, and their ratio varied with each pore-forming agent. It was observed that addition of different pore-forming agent resulted in significantly different microstructures.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts : V Serbian Ceramic Society Conference, Sep 21-23 September 2016, Belgrade",
title = "Influence of different pore-forming agents on wollastonite microstructures",
pages = "42-42",
url = "https://hdl.handle.net/21.15107/rcub_dais_874"
}
Obradović, N., Filipović, S., Marković, S., Mitrić, M., Antić, V.,& Pavlović, V. B.. (2016). Influence of different pore-forming agents on wollastonite microstructures. in Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts : V Serbian Ceramic Society Conference, Sep 21-23 September 2016, Belgrade
Belgrade : Serbian Ceramic Society., 42-42.
https://hdl.handle.net/21.15107/rcub_dais_874
Obradović N, Filipović S, Marković S, Mitrić M, Antić V, Pavlović VB. Influence of different pore-forming agents on wollastonite microstructures. in Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts : V Serbian Ceramic Society Conference, Sep 21-23 September 2016, Belgrade. 2016;:42-42.
https://hdl.handle.net/21.15107/rcub_dais_874 .
Obradović, Nina, Filipović, Suzana, Marković, Smilja, Mitrić, Miodrag, Antić, Vesna, Pavlović, Vladimir B., "Influence of different pore-forming agents on wollastonite microstructures" in Advanced Ceramics and Application : new frontiers in multifunctional material science and processing : program and the book of abstracts : V Serbian Ceramic Society Conference, Sep 21-23 September 2016, Belgrade (2016):42-42,
https://hdl.handle.net/21.15107/rcub_dais_874 .