TY  - JOUR
AU  - Zdujić, Miodrag
AU  - Petrović, Slobodan D.
AU  - Valentić, Nataša V.
AU  - Mijin, Dušan
PY  - 2019
UR  - https://scindeks.ceon.rs/article.aspx?artid=0351-94651903229Z
UR  - http://www.ncbi.nlm.nih.gov/pubmed/0351-94651903229Z
UR  - https://dais.sanu.ac.rs/123456789/6954
AB  - Milling of cyanoacetamide and acetoacetic ester as reactants, in the presence of KOH as the catalyst and ethanol as a viscous control agent (VCA) was performed in a planetary ball mill with the goal of investigating the effect of mechanochemical treatment for the synthesis of 3-cyano-6hydroxy-4-methyl-2-pyridone at room temperature. The mechanochemical synthesis was performed under various milling parameters, i.e. milling time up to 4 h, number and size of balls, angular velocity as well as molar ratio of reactants and the amount of catalyst. The obtained product was characterized by m.p., UV, IR and NMR data. It was fond that the dominant process parameter is the milling time while others are of less importance. The highest isolated yield after milling was up to 56%. The combination of milling and aging increase yield over 60%.
PB  - Belgrade : Engineers Society of Corrosion
T2  - Zaštita materijala
T1  - On the synthesis of 3-cyano-6-hydroxy-4-methyl-2-pyridone at room temperature
SP  - 229
EP  - 236
VL  - 60
IS  - 3
DO  - 10.5937/zasmat1903229Z
UR  - https://hdl.handle.net/21.15107/rcub_dais_6954
ER  - 

@article{
author = "Zdujić, Miodrag and Petrović, Slobodan D. and Valentić, Nataša V. and Mijin, Dušan",
year = "2019",
abstract = "Milling of cyanoacetamide and acetoacetic ester as reactants, in the presence of KOH as the catalyst and ethanol as a viscous control agent (VCA) was performed in a planetary ball mill with the goal of investigating the effect of mechanochemical treatment for the synthesis of 3-cyano-6hydroxy-4-methyl-2-pyridone at room temperature. The mechanochemical synthesis was performed under various milling parameters, i.e. milling time up to 4 h, number and size of balls, angular velocity as well as molar ratio of reactants and the amount of catalyst. The obtained product was characterized by m.p., UV, IR and NMR data. It was fond that the dominant process parameter is the milling time while others are of less importance. The highest isolated yield after milling was up to 56%. The combination of milling and aging increase yield over 60%.",
publisher = "Belgrade : Engineers Society of Corrosion",
journal = "Zaštita materijala",
title = "On the synthesis of 3-cyano-6-hydroxy-4-methyl-2-pyridone at room temperature",
pages = "229-236",
volume = "60",
number = "3",
doi = "10.5937/zasmat1903229Z",
url = "https://hdl.handle.net/21.15107/rcub_dais_6954"
}

Zdujić, M., Petrović, S. D., Valentić, N. V.,& Mijin, D.. (2019). On the synthesis of 3-cyano-6-hydroxy-4-methyl-2-pyridone at room temperature. in Zaštita materijala
Belgrade : Engineers Society of Corrosion., 60(3), 229-236.
https://doi.org/10.5937/zasmat1903229Z
https://hdl.handle.net/21.15107/rcub_dais_6954

Zdujić M, Petrović SD, Valentić NV, Mijin D. On the synthesis of 3-cyano-6-hydroxy-4-methyl-2-pyridone at room temperature. in Zaštita materijala. 2019;60(3):229-236.
doi:10.5937/zasmat1903229Z
https://hdl.handle.net/21.15107/rcub_dais_6954 .

Zdujić, Miodrag, Petrović, Slobodan D., Valentić, Nataša V., Mijin, Dušan, "On the synthesis of 3-cyano-6-hydroxy-4-methyl-2-pyridone at room temperature" in Zaštita materijala, 60, no. 3 (2019):229-236,
https://doi.org/10.5937/zasmat1903229Z .,
https://hdl.handle.net/21.15107/rcub_dais_6954 .

TY  - JOUR
AU  - Avramov-Ivić, Milka
AU  - Leger, J.M.
AU  - Lamy, C.
AU  - Jović, V.D.
AU  - Petrović, Slobodan
PY  - 1991
UR  - https://dais.sanu.ac.rs/123456789/10664
AB  - In this work, the oxidation of glycerol on a gold single-crystal surface with the (100) orientation has been studied with the aim of investigating the interfacial properties of the electrode surface in the absence and presence of glycerol. The change in the interfacial properties gives useful information about the nature of OH adsorption on a Au (100) electrode and about the process of adsorption and faradaic oxidation of glycerol in 0.1 M NaOH. The electrosorption of glycerol was also investigated at a polycrystalline gold electrode, by programmed potential voltammetry, in order to confirm the results obtained by double-layer capacity measurements.
PB  - Lausanne : Elsevier Science Sa, Lausanne
T2  - Journal of Electroanalytical Chemistry
T1  - The electro-oxidation of glycerol on the gold(100)-oriented single-crystal surface and poly crystalline surface in 0.1 M NaOH
SP  - 309
EP  - 317
VL  - 308
IS  - 1-2
DO  - 10.1016/0022-0728(91)85075-Z
UR  - https://hdl.handle.net/21.15107/rcub_dais_10664
ER  - 

@article{
author = "Avramov-Ivić, Milka and Leger, J.M. and Lamy, C. and Jović, V.D. and Petrović, Slobodan",
year = "1991",
abstract = "In this work, the oxidation of glycerol on a gold single-crystal surface with the (100) orientation has been studied with the aim of investigating the interfacial properties of the electrode surface in the absence and presence of glycerol. The change in the interfacial properties gives useful information about the nature of OH adsorption on a Au (100) electrode and about the process of adsorption and faradaic oxidation of glycerol in 0.1 M NaOH. The electrosorption of glycerol was also investigated at a polycrystalline gold electrode, by programmed potential voltammetry, in order to confirm the results obtained by double-layer capacity measurements.",
publisher = "Lausanne : Elsevier Science Sa, Lausanne",
journal = "Journal of Electroanalytical Chemistry",
title = "The electro-oxidation of glycerol on the gold(100)-oriented single-crystal surface and poly crystalline surface in 0.1 M NaOH",
pages = "309-317",
volume = "308",
number = "1-2",
doi = "10.1016/0022-0728(91)85075-Z",
url = "https://hdl.handle.net/21.15107/rcub_dais_10664"
}

Avramov-Ivić, M., Leger, J.M., Lamy, C., Jović, V.D.,& Petrović, S.. (1991). The electro-oxidation of glycerol on the gold(100)-oriented single-crystal surface and poly crystalline surface in 0.1 M NaOH. in Journal of Electroanalytical Chemistry
Lausanne : Elsevier Science Sa, Lausanne., 308(1-2), 309-317.
https://doi.org/10.1016/0022-0728(91)85075-Z
https://hdl.handle.net/21.15107/rcub_dais_10664

Avramov-Ivić M, Leger J, Lamy C, Jović V, Petrović S. The electro-oxidation of glycerol on the gold(100)-oriented single-crystal surface and poly crystalline surface in 0.1 M NaOH. in Journal of Electroanalytical Chemistry. 1991;308(1-2):309-317.
doi:10.1016/0022-0728(91)85075-Z
https://hdl.handle.net/21.15107/rcub_dais_10664 .

Avramov-Ivić, Milka, Leger, J.M., Lamy, C., Jović, V.D., Petrović, Slobodan, "The electro-oxidation of glycerol on the gold(100)-oriented single-crystal surface and poly crystalline surface in 0.1 M NaOH" in Journal of Electroanalytical Chemistry, 308, no. 1-2 (1991):309-317,
https://doi.org/10.1016/0022-0728(91)85075-Z .,
https://hdl.handle.net/21.15107/rcub_dais_10664 .