Reka, Arianit A.

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Fabrication of Ceramic Monoliths from Diatomaceous Earth: Effects of Calcination Temperature on Silica Phase Transformation

Reka, Arianit A.; Kosanović, Darko; Ademi, Egzon; Aggrey, Patrick; Berisha, Avni; Pavlovski, Blagoj; Jovanovski, Gligor; Rexhepi, Besnik; Jashari, Ahmed; Makreski, Petre

(2022)

TY  - JOUR
AU  - Reka, Arianit A.
AU  - Kosanović, Darko
AU  - Ademi, Egzon
AU  - Aggrey, Patrick
AU  - Berisha, Avni
AU  - Pavlovski, Blagoj
AU  - Jovanovski, Gligor
AU  - Rexhepi, Besnik
AU  - Jashari, Ahmed
AU  - Makreski, Petre
PY  - 2022
UR  - https://dais.sanu.ac.rs/123456789/13518
AB  - The raw diatomaceous earth from the vicinity of Bitola (North Macedonia) showed low bulk density (0.61–0.69 g/cm3), high-water absorption (75–81%) and porosity (66–72%). The chemical composition was determined with ICP-MS, revealing the following results for the diatomaceous earth: SiO2 (63.69 wt%), Al2O3 (11.79 wt%), Fe2O3 (5.95 wt%), MnO (0.15 wt%), TiO2 (0.65 wt%), CaO (1.51 wt%), MgO (2.24 wt%), P2O5 (0.13 wt%), K2O (1.64 wt%), Na2O (0.93 wt%), LOI (11.21 wt%). XRPD data of the examined sample of clayey diatomite mainly depicted crystalline behavior with a small presence of amorphous phase. The crystalline mineral phases mainly comprise: silica (quartz), feldspars (plagioclase), mica (muscovite), chlorites and dolomite. SEM and TEM results show cased presence of micro- and nanostructures with pores ranging from 250 to 600 nm. The clayey diatomite was sintered at three temperatures (900, 1000 and 1100ºC) for a period of 1 h. XRPD of the sintered samples at 1100ºC showed certain thermal stability and formation of new phases (mullite and tridymite) that makes the analyzed diatomaceous earth suitable for production of various types of ceramic, construction and thermal insulating materials.
T2  - Science of Sintering
T2  - Science of Sintering
T1  - Fabrication of Ceramic Monoliths from Diatomaceous Earth: Effects of Calcination Temperature on Silica Phase Transformation
VL  - 54
IS  - 4
DO  - 10.2298/SOS2204495R
UR  - https://hdl.handle.net/21.15107/rcub_dais_13518
ER  - 
@article{
author = "Reka, Arianit A. and Kosanović, Darko and Ademi, Egzon and Aggrey, Patrick and Berisha, Avni and Pavlovski, Blagoj and Jovanovski, Gligor and Rexhepi, Besnik and Jashari, Ahmed and Makreski, Petre",
year = "2022",
abstract = "The raw diatomaceous earth from the vicinity of Bitola (North Macedonia) showed low bulk density (0.61–0.69 g/cm3), high-water absorption (75–81%) and porosity (66–72%). The chemical composition was determined with ICP-MS, revealing the following results for the diatomaceous earth: SiO2 (63.69 wt%), Al2O3 (11.79 wt%), Fe2O3 (5.95 wt%), MnO (0.15 wt%), TiO2 (0.65 wt%), CaO (1.51 wt%), MgO (2.24 wt%), P2O5 (0.13 wt%), K2O (1.64 wt%), Na2O (0.93 wt%), LOI (11.21 wt%). XRPD data of the examined sample of clayey diatomite mainly depicted crystalline behavior with a small presence of amorphous phase. The crystalline mineral phases mainly comprise: silica (quartz), feldspars (plagioclase), mica (muscovite), chlorites and dolomite. SEM and TEM results show cased presence of micro- and nanostructures with pores ranging from 250 to 600 nm. The clayey diatomite was sintered at three temperatures (900, 1000 and 1100ºC) for a period of 1 h. XRPD of the sintered samples at 1100ºC showed certain thermal stability and formation of new phases (mullite and tridymite) that makes the analyzed diatomaceous earth suitable for production of various types of ceramic, construction and thermal insulating materials.",
journal = "Science of Sintering, Science of Sintering",
title = "Fabrication of Ceramic Monoliths from Diatomaceous Earth: Effects of Calcination Temperature on Silica Phase Transformation",
volume = "54",
number = "4",
doi = "10.2298/SOS2204495R",
url = "https://hdl.handle.net/21.15107/rcub_dais_13518"
}
Reka, A. A., Kosanović, D., Ademi, E., Aggrey, P., Berisha, A., Pavlovski, B., Jovanovski, G., Rexhepi, B., Jashari, A.,& Makreski, P.. (2022). Fabrication of Ceramic Monoliths from Diatomaceous Earth: Effects of Calcination Temperature on Silica Phase Transformation. in Science of Sintering, 54(4).
https://doi.org/10.2298/SOS2204495R
https://hdl.handle.net/21.15107/rcub_dais_13518
Reka AA, Kosanović D, Ademi E, Aggrey P, Berisha A, Pavlovski B, Jovanovski G, Rexhepi B, Jashari A, Makreski P. Fabrication of Ceramic Monoliths from Diatomaceous Earth: Effects of Calcination Temperature on Silica Phase Transformation. in Science of Sintering. 2022;54(4).
doi:10.2298/SOS2204495R
https://hdl.handle.net/21.15107/rcub_dais_13518 .
Reka, Arianit A., Kosanović, Darko, Ademi, Egzon, Aggrey, Patrick, Berisha, Avni, Pavlovski, Blagoj, Jovanovski, Gligor, Rexhepi, Besnik, Jashari, Ahmed, Makreski, Petre, "Fabrication of Ceramic Monoliths from Diatomaceous Earth: Effects of Calcination Temperature on Silica Phase Transformation" in Science of Sintering, 54, no. 4 (2022),
https://doi.org/10.2298/SOS2204495R .,
https://hdl.handle.net/21.15107/rcub_dais_13518 .