Sknepnek, A., Filipović, S., Pavlović, V. B., Mirković, N., Miletić, D., Gržetić, J.,& Mirković, M.. (2024). Effects of Synthesis Parameters on Structure and Antimicrobial Properties of Bacterial Cellulose/Hydroxyapatite/TiO2 Polymer–Ceramic Composite Material. in Polymers
Basel : MDPI AG., 16(4), 470.
https://doi.org/10.3390/polym16040470
https://hdl.handle.net/21.15107/rcub_dais_16384

Sknepnek A, Filipović S, Pavlović VB, Mirković N, Miletić D, Gržetić J, Mirković M. Effects of Synthesis Parameters on Structure and Antimicrobial Properties of Bacterial Cellulose/Hydroxyapatite/TiO2 Polymer–Ceramic Composite Material. in Polymers. 2024;16(4):470.
doi:10.3390/polym16040470
https://hdl.handle.net/21.15107/rcub_dais_16384 .

Sknepnek, Aleksandra, Filipović, Suzana, Pavlović, Vladimir B., Mirković, Nemanja, Miletić, Dunja, Gržetić, Jelena, Mirković, Miljana, "Effects of Synthesis Parameters on Structure and Antimicrobial Properties of Bacterial Cellulose/Hydroxyapatite/TiO2 Polymer–Ceramic Composite Material" in Polymers, 16, no. 4 (2024):470,
https://doi.org/10.3390/polym16040470 .,
https://hdl.handle.net/21.15107/rcub_dais_16384 .

TY  - JOUR
AU  - Obradović, Nina
AU  - Feng, Lun
AU  - Filipović, Suzana
AU  - Mirković, Miljana
AU  - Kosanović, Darko
AU  - Rogan, Jelena
AU  - Fahrenholtz, William G.
PY  - 2023
UR  - https://dais.sanu.ac.rs/123456789/14877
AB  - Zirconium carbide ceramics were prepared by carbothermal reduction of ZrO2 and C that were mixed by high-energy ball milling. Powders were milled for times from 0 to 120 min in air. As milling time increased, the surface area of the powders increased, indicating significant particle size reduction. Milled powders were reacted at 1600 °C and then densified by spark plasma sintering at 2000 °C, which was sufficient to convert the starting powders to zirconium carbide. Unmilled powders did not reach full density. Milled powders reached full density, but ZrO2 impurities were found for specimens prepared from powders milled for 60 and 120 min. Microstructure analysis showed that grain size was less than 2 µm for ceramics produced from powder milled for 15 min. Based on densification onset temperature and impurity levels, a milling time of 15 min gives the best balance of particle size reduction to promote densification while minimizing impurity levels.
PB  - Elsevier BV
T2  - Journal of the European Ceramic Society
T1  - Effect of mechanical activation on carbothermal synthesis and densification of ZrC
SP  - 7306
EP  - 7313
VL  - 43
DO  - 10.1016/j.jeurceramsoc.2023.08.007
UR  - https://hdl.handle.net/21.15107/rcub_dais_14877
ER  - 

@article{
author = "Obradović, Nina and Feng, Lun and Filipović, Suzana and Mirković, Miljana and Kosanović, Darko and Rogan, Jelena and Fahrenholtz, William G.",
year = "2023",
abstract = "Zirconium carbide ceramics were prepared by carbothermal reduction of ZrO2 and C that were mixed by high-energy ball milling. Powders were milled for times from 0 to 120 min in air. As milling time increased, the surface area of the powders increased, indicating significant particle size reduction. Milled powders were reacted at 1600 °C and then densified by spark plasma sintering at 2000 °C, which was sufficient to convert the starting powders to zirconium carbide. Unmilled powders did not reach full density. Milled powders reached full density, but ZrO2 impurities were found for specimens prepared from powders milled for 60 and 120 min. Microstructure analysis showed that grain size was less than 2 µm for ceramics produced from powder milled for 15 min. Based on densification onset temperature and impurity levels, a milling time of 15 min gives the best balance of particle size reduction to promote densification while minimizing impurity levels.",
publisher = "Elsevier BV",
journal = "Journal of the European Ceramic Society",
title = "Effect of mechanical activation on carbothermal synthesis and densification of ZrC",
pages = "7306-7313",
volume = "43",
doi = "10.1016/j.jeurceramsoc.2023.08.007",
url = "https://hdl.handle.net/21.15107/rcub_dais_14877"
}

Obradović, N., Feng, L., Filipović, S., Mirković, M., Kosanović, D., Rogan, J.,& Fahrenholtz, W. G.. (2023). Effect of mechanical activation on carbothermal synthesis and densification of ZrC. in Journal of the European Ceramic Society
Elsevier BV., 43, 7306-7313.
https://doi.org/10.1016/j.jeurceramsoc.2023.08.007
https://hdl.handle.net/21.15107/rcub_dais_14877

Obradović N, Feng L, Filipović S, Mirković M, Kosanović D, Rogan J, Fahrenholtz WG. Effect of mechanical activation on carbothermal synthesis and densification of ZrC. in Journal of the European Ceramic Society. 2023;43:7306-7313.
doi:10.1016/j.jeurceramsoc.2023.08.007
https://hdl.handle.net/21.15107/rcub_dais_14877 .

Obradović, Nina, Feng, Lun, Filipović, Suzana, Mirković, Miljana, Kosanović, Darko, Rogan, Jelena, Fahrenholtz, William G., "Effect of mechanical activation on carbothermal synthesis and densification of ZrC" in Journal of the European Ceramic Society, 43 (2023):7306-7313,
https://doi.org/10.1016/j.jeurceramsoc.2023.08.007 .,
https://hdl.handle.net/21.15107/rcub_dais_14877 .

TY  - JOUR
AU  - Janićijević, Aleksandra
AU  - Filipović, Suzana
AU  - Sknepnek, Aleksandra
AU  - Vlahović, Branislav
AU  - Đorđević, Nenad
AU  - Kovacević, Danijela
AU  - Mirković, Miljana
AU  - Petronijević, Ivan
AU  - Živković, Predrag
AU  - Rogan, Jelena
AU  - Pavlović, Vladimir B.
PY  - 2023
UR  - https://dais.sanu.ac.rs/123456789/15363
AB  - In the search for environmentally friendly materials with a wide range of properties, polymer composites have emerged as a promising alternative due to their multifunctional properties. This study focuses on the synthesis of composite materials consisting of four components: bacterial nanocellulose (BNC) modified with magnetic Fe3O4, and a mixture of BaTiO3 (BT) and polyvinylidene fluoride (PVDF). The BT powder was mechanically activated prior to mixing with PVDF. The influence of BT mechanical activation and BNC with magnetic particles on the PVDF matrix was investigated. The obtained composite films’ structural characteristics, morphology, and dielectric properties are presented. This research provides insights into the relationship between mechanical activation of the filler and structural and dielectric properties in the PVDF/BT/BNC/Fe3O4 system, creating the way for the development of materials with a wide range of diverse properties that support the concept of green technologies.
PB  - Basel : MDPI
T2  - Polymers
T1  - Dielectric and Structural Properties of the Hybrid Material Polyvinylidene Fluoride-Bacterial Nanocellulose-Based Composite
SP  - 4080
VL  - 15
IS  - 20
DO  - 10.3390/polym15204080
UR  - https://hdl.handle.net/21.15107/rcub_dais_15363
ER  - 

@article{
author = "Janićijević, Aleksandra and Filipović, Suzana and Sknepnek, Aleksandra and Vlahović, Branislav and Đorđević, Nenad and Kovacević, Danijela and Mirković, Miljana and Petronijević, Ivan and Živković, Predrag and Rogan, Jelena and Pavlović, Vladimir B.",
year = "2023",
abstract = "In the search for environmentally friendly materials with a wide range of properties, polymer composites have emerged as a promising alternative due to their multifunctional properties. This study focuses on the synthesis of composite materials consisting of four components: bacterial nanocellulose (BNC) modified with magnetic Fe3O4, and a mixture of BaTiO3 (BT) and polyvinylidene fluoride (PVDF). The BT powder was mechanically activated prior to mixing with PVDF. The influence of BT mechanical activation and BNC with magnetic particles on the PVDF matrix was investigated. The obtained composite films’ structural characteristics, morphology, and dielectric properties are presented. This research provides insights into the relationship between mechanical activation of the filler and structural and dielectric properties in the PVDF/BT/BNC/Fe3O4 system, creating the way for the development of materials with a wide range of diverse properties that support the concept of green technologies.",
publisher = "Basel : MDPI",
journal = "Polymers",
title = "Dielectric and Structural Properties of the Hybrid Material Polyvinylidene Fluoride-Bacterial Nanocellulose-Based Composite",
pages = "4080",
volume = "15",
number = "20",
doi = "10.3390/polym15204080",
url = "https://hdl.handle.net/21.15107/rcub_dais_15363"
}

Janićijević, A., Filipović, S., Sknepnek, A., Vlahović, B., Đorđević, N., Kovacević, D., Mirković, M., Petronijević, I., Živković, P., Rogan, J.,& Pavlović, V. B.. (2023). Dielectric and Structural Properties of the Hybrid Material Polyvinylidene Fluoride-Bacterial Nanocellulose-Based Composite. in Polymers
Basel : MDPI., 15(20), 4080.
https://doi.org/10.3390/polym15204080
https://hdl.handle.net/21.15107/rcub_dais_15363

Janićijević A, Filipović S, Sknepnek A, Vlahović B, Đorđević N, Kovacević D, Mirković M, Petronijević I, Živković P, Rogan J, Pavlović VB. Dielectric and Structural Properties of the Hybrid Material Polyvinylidene Fluoride-Bacterial Nanocellulose-Based Composite. in Polymers. 2023;15(20):4080.
doi:10.3390/polym15204080
https://hdl.handle.net/21.15107/rcub_dais_15363 .

Janićijević, Aleksandra, Filipović, Suzana, Sknepnek, Aleksandra, Vlahović, Branislav, Đorđević, Nenad, Kovacević, Danijela, Mirković, Miljana, Petronijević, Ivan, Živković, Predrag, Rogan, Jelena, Pavlović, Vladimir B., "Dielectric and Structural Properties of the Hybrid Material Polyvinylidene Fluoride-Bacterial Nanocellulose-Based Composite" in Polymers, 15, no. 20 (2023):4080,
https://doi.org/10.3390/polym15204080 .,
https://hdl.handle.net/21.15107/rcub_dais_15363 .

TY  - JOUR
AU  - Obradović, Nina
AU  - Feng, Lun
AU  - Filipović, Suzana
AU  - Mirković, Miljana
AU  - Kosanović, Darko
AU  - Rogan, Jelena
AU  - Fahrenholtz, William G.
PY  - 2023
UR  - https://dais.sanu.ac.rs/123456789/14890
AB  - Zirconium carbide ceramics were prepared by carbothermal reduction of ZrO2 and C that were mixed by high-energy ball milling. Powders were milled for times from 0 to 120 min in air. As milling time increased, the surface area of the powders increased, indicating significant particle size reduction. Milled powders were reacted at 1600 °C and then densified by spark plasma sintering at 2000 °C, which was sufficient to convert the starting powders to zirconium carbide. Unmilled powders did not reach full density. Milled powders reached full density, but ZrO2 impurities were found for specimens prepared from powders milled for 60 and 120 min. Microstructure analysis showed that grain size was less than 2 µm for ceramics produced from powder milled for 15 min. Based on densification onset temperature and impurity levels, a milling time of 15 min gives the best balance of particle size reduction to promote densification while minimizing impurity levels.
PB  - Elsevier BV
T2  - Journal of the European Ceramic Society
T1  - Effect of mechanical activation on carbothermal synthesis and densification of ZrC
SP  - 7306
EP  - 7313
DO  - 10.1016/j.jeurceramsoc.2023.08.007
UR  - https://hdl.handle.net/21.15107/rcub_dais_14890
ER  - 

@article{
author = "Obradović, Nina and Feng, Lun and Filipović, Suzana and Mirković, Miljana and Kosanović, Darko and Rogan, Jelena and Fahrenholtz, William G.",
year = "2023",
abstract = "Zirconium carbide ceramics were prepared by carbothermal reduction of ZrO2 and C that were mixed by high-energy ball milling. Powders were milled for times from 0 to 120 min in air. As milling time increased, the surface area of the powders increased, indicating significant particle size reduction. Milled powders were reacted at 1600 °C and then densified by spark plasma sintering at 2000 °C, which was sufficient to convert the starting powders to zirconium carbide. Unmilled powders did not reach full density. Milled powders reached full density, but ZrO2 impurities were found for specimens prepared from powders milled for 60 and 120 min. Microstructure analysis showed that grain size was less than 2 µm for ceramics produced from powder milled for 15 min. Based on densification onset temperature and impurity levels, a milling time of 15 min gives the best balance of particle size reduction to promote densification while minimizing impurity levels.",
publisher = "Elsevier BV",
journal = "Journal of the European Ceramic Society",
title = "Effect of mechanical activation on carbothermal synthesis and densification of ZrC",
pages = "7306-7313",
doi = "10.1016/j.jeurceramsoc.2023.08.007",
url = "https://hdl.handle.net/21.15107/rcub_dais_14890"
}

Obradović, N., Feng, L., Filipović, S., Mirković, M., Kosanović, D., Rogan, J.,& Fahrenholtz, W. G.. (2023). Effect of mechanical activation on carbothermal synthesis and densification of ZrC. in Journal of the European Ceramic Society
Elsevier BV., 7306-7313.
https://doi.org/10.1016/j.jeurceramsoc.2023.08.007
https://hdl.handle.net/21.15107/rcub_dais_14890

Obradović N, Feng L, Filipović S, Mirković M, Kosanović D, Rogan J, Fahrenholtz WG. Effect of mechanical activation on carbothermal synthesis and densification of ZrC. in Journal of the European Ceramic Society. 2023;:7306-7313.
doi:10.1016/j.jeurceramsoc.2023.08.007
https://hdl.handle.net/21.15107/rcub_dais_14890 .

Obradović, Nina, Feng, Lun, Filipović, Suzana, Mirković, Miljana, Kosanović, Darko, Rogan, Jelena, Fahrenholtz, William G., "Effect of mechanical activation on carbothermal synthesis and densification of ZrC" in Journal of the European Ceramic Society (2023):7306-7313,
https://doi.org/10.1016/j.jeurceramsoc.2023.08.007 .,
https://hdl.handle.net/21.15107/rcub_dais_14890 .

TY  - JOUR
AU  - Mirković, Miljana
AU  - Filipović, Suzana
AU  - Kalijadis, Ana
AU  - Mašković, Pavle
AU  - Mašković, Jelena
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2022
UR  - https://dais.sanu.ac.rs/123456789/13153
AB  - Due to the growing number of people infected with the new coronavirus globally, which weakens immunity, there has been an increase in bacterial infections. Hence, knowledge about simple and low-cost synthesis methods of materials with good structural and antimicrobial properties is of great importance. A material obtained through the combination of a nanoscale hydroxyapatite material (with good biocompatibility) and titanium dioxide (with good degradation properties of organic molecules) can absorb and decompose bacteria. In this investigation, three different synthesis routes used to prepare hydroxyapatite/titanium dioxide nanomaterials are examined. The morphology and semiquantitative chemical composition are characterized by scanning electron microscopy with energy dispersive X-ray analysis (SEM-EDX). The obtained materials’ phase and structural characterization are determined using the X-ray powder diffraction method (XRD). The crystallite sizes of the obtained materials are in the range of 8 nm to 15 nm. Based on XRD peak positions, the hexagonal hydroxyapatite phases are formed in all samples along with TiO2 anatase and rutile phases. According to SEM and TEM analyses, the morphology of the prepared samples differs depending on the synthesis route. The EDX analysis confirmed the presence of Ti, Ca, P, and O in the obtained materials. The IR spectroscopy verified the vibration bands characteristic for HAp and titanium. The investigated materials show excellent antimicrobial and photocatalytic properties.
T2  - Antibiotics
T1  - Hydroxyapatite/TiO2 Nanomaterial with Defined Microstructural and Good Antimicrobial Properties
SP  - 592
VL  - 11
IS  - 5
DO  - 10.3390/antibiotics11050592
UR  - https://hdl.handle.net/21.15107/rcub_dais_13153
ER  - 

@article{
author = "Mirković, Miljana and Filipović, Suzana and Kalijadis, Ana and Mašković, Pavle and Mašković, Jelena and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2022",
abstract = "Due to the growing number of people infected with the new coronavirus globally, which weakens immunity, there has been an increase in bacterial infections. Hence, knowledge about simple and low-cost synthesis methods of materials with good structural and antimicrobial properties is of great importance. A material obtained through the combination of a nanoscale hydroxyapatite material (with good biocompatibility) and titanium dioxide (with good degradation properties of organic molecules) can absorb and decompose bacteria. In this investigation, three different synthesis routes used to prepare hydroxyapatite/titanium dioxide nanomaterials are examined. The morphology and semiquantitative chemical composition are characterized by scanning electron microscopy with energy dispersive X-ray analysis (SEM-EDX). The obtained materials’ phase and structural characterization are determined using the X-ray powder diffraction method (XRD). The crystallite sizes of the obtained materials are in the range of 8 nm to 15 nm. Based on XRD peak positions, the hexagonal hydroxyapatite phases are formed in all samples along with TiO2 anatase and rutile phases. According to SEM and TEM analyses, the morphology of the prepared samples differs depending on the synthesis route. The EDX analysis confirmed the presence of Ti, Ca, P, and O in the obtained materials. The IR spectroscopy verified the vibration bands characteristic for HAp and titanium. The investigated materials show excellent antimicrobial and photocatalytic properties.",
journal = "Antibiotics",
title = "Hydroxyapatite/TiO2 Nanomaterial with Defined Microstructural and Good Antimicrobial Properties",
pages = "592",
volume = "11",
number = "5",
doi = "10.3390/antibiotics11050592",
url = "https://hdl.handle.net/21.15107/rcub_dais_13153"
}

Mirković, M., Filipović, S., Kalijadis, A., Mašković, P., Mašković, J., Vlahović, B.,& Pavlović, V. B.. (2022). Hydroxyapatite/TiO2 Nanomaterial with Defined Microstructural and Good Antimicrobial Properties. in Antibiotics, 11(5), 592.
https://doi.org/10.3390/antibiotics11050592
https://hdl.handle.net/21.15107/rcub_dais_13153

Mirković M, Filipović S, Kalijadis A, Mašković P, Mašković J, Vlahović B, Pavlović VB. Hydroxyapatite/TiO2 Nanomaterial with Defined Microstructural and Good Antimicrobial Properties. in Antibiotics. 2022;11(5):592.
doi:10.3390/antibiotics11050592
https://hdl.handle.net/21.15107/rcub_dais_13153 .

Mirković, Miljana, Filipović, Suzana, Kalijadis, Ana, Mašković, Pavle, Mašković, Jelena, Vlahović, Branislav, Pavlović, Vladimir B., "Hydroxyapatite/TiO2 Nanomaterial with Defined Microstructural and Good Antimicrobial Properties" in Antibiotics, 11, no. 5 (2022):592,
https://doi.org/10.3390/antibiotics11050592 .,
https://hdl.handle.net/21.15107/rcub_dais_13153 .

TY  - CONF
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Fahrenholtz, William G.
AU  - Smith, Steven
AU  - Mirković, Miljana M.
AU  - Peleš, Adriana
AU  - Đorđević, Antonije
PY  - 2022
UR  - https://dais.sanu.ac.rs/123456789/13118
AB  - MgTiO3 is a material often used in different types of high-frequency capacitors, temperature compensating capacitors, and chip capacitors, so the enhancement of this material is still the focus of many research groups due to its remarkable dielectric properties. Outstanding features can only be achieved when the ceramics are highly dense. Densification of magnesium titanate by Spark Plasma Sintering (SPS) was the aim of this work. Magnesium titanate ceramics were prepared by applying mechanical activation as the first step. Powders prepared in this way were SPS sintered, at 1200 °C with a heating rate of 100 °C/min. After reaching the desired temperature, a uniaxial pressure of 50 MPa was applied. The dwell time at this condition was 5 min, followed by cooling to room temperature at 5°C/min. X-ray diffraction was performed in order to establish the phase composition of milled powders and obtained ceramics. Differences between samples milled in various times intervals, as well as sintered ceramics were examined by means of scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The presence of MgTiz0s phase was detected in XRD and was confirmed by EDS analysis for the non-milled ceramics. In the samples obtained from milled powders, no MgTi2O5 was detected in XRD patterns, but this phase was detected in EDS spectra in a lower amount. Dielectric measurements were performed at a wide range of frequencies, while the hardness of the SPS samples was measured at loads up to 10 N. The highest value of the hardness was obtained from powder milled for 15 min before SPS.
PB  - Belgrade : Innovation Center of Faculty of Mechanical Engineering
C3  - Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2022, 05-08 July 2022, Zlatibor, Serbia
T1  - Spark plasma sintering of mechanically activated MGO-TiO2 system
SP  - 81
EP  - 81
UR  - https://hdl.handle.net/21.15107/rcub_dais_13118
ER  - 

@conference{
author = "Filipović, Suzana and Obradović, Nina and Fahrenholtz, William G. and Smith, Steven and Mirković, Miljana M. and Peleš, Adriana and Đorđević, Antonije",
year = "2022",
abstract = "MgTiO3 is a material often used in different types of high-frequency capacitors, temperature compensating capacitors, and chip capacitors, so the enhancement of this material is still the focus of many research groups due to its remarkable dielectric properties. Outstanding features can only be achieved when the ceramics are highly dense. Densification of magnesium titanate by Spark Plasma Sintering (SPS) was the aim of this work. Magnesium titanate ceramics were prepared by applying mechanical activation as the first step. Powders prepared in this way were SPS sintered, at 1200 °C with a heating rate of 100 °C/min. After reaching the desired temperature, a uniaxial pressure of 50 MPa was applied. The dwell time at this condition was 5 min, followed by cooling to room temperature at 5°C/min. X-ray diffraction was performed in order to establish the phase composition of milled powders and obtained ceramics. Differences between samples milled in various times intervals, as well as sintered ceramics were examined by means of scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The presence of MgTiz0s phase was detected in XRD and was confirmed by EDS analysis for the non-milled ceramics. In the samples obtained from milled powders, no MgTi2O5 was detected in XRD patterns, but this phase was detected in EDS spectra in a lower amount. Dielectric measurements were performed at a wide range of frequencies, while the hardness of the SPS samples was measured at loads up to 10 N. The highest value of the hardness was obtained from powder milled for 15 min before SPS.",
publisher = "Belgrade : Innovation Center of Faculty of Mechanical Engineering",
journal = "Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2022, 05-08 July 2022, Zlatibor, Serbia",
title = "Spark plasma sintering of mechanically activated MGO-TiO2 system",
pages = "81-81",
url = "https://hdl.handle.net/21.15107/rcub_dais_13118"
}

Filipović, S., Obradović, N., Fahrenholtz, W. G., Smith, S., Mirković, M. M., Peleš, A.,& Đorđević, A.. (2022). Spark plasma sintering of mechanically activated MGO-TiO2 system. in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2022, 05-08 July 2022, Zlatibor, Serbia
Belgrade : Innovation Center of Faculty of Mechanical Engineering., 81-81.
https://hdl.handle.net/21.15107/rcub_dais_13118

Filipović S, Obradović N, Fahrenholtz WG, Smith S, Mirković MM, Peleš A, Đorđević A. Spark plasma sintering of mechanically activated MGO-TiO2 system. in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2022, 05-08 July 2022, Zlatibor, Serbia. 2022;:81-81.
https://hdl.handle.net/21.15107/rcub_dais_13118 .

Filipović, Suzana, Obradović, Nina, Fahrenholtz, William G., Smith, Steven, Mirković, Miljana M., Peleš, Adriana, Đorđević, Antonije, "Spark plasma sintering of mechanically activated MGO-TiO2 system" in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2022, 05-08 July 2022, Zlatibor, Serbia (2022):81-81,
https://hdl.handle.net/21.15107/rcub_dais_13118 .

TY  - JOUR
AU  - Janićijević, Aleksandra
AU  - Sknepnek, Aleksandra
AU  - Mirković, Miljana
AU  - Pavlović, Vladimir
AU  - Filipović, Suzana
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/12342
AB  - Napredak u mnogim oblastima tehnike i tehnologije je blisko povezan sa razvojem novih ili unapređenjem postojećih materijala. Imajući u vidu široku primenu bakterijske nanoceluloze (BNC) u raznim oblastima svakodnevnog života, od biomedicine, ekologije do elektronike, kompoziti na bazi BNC su sve rasprostranjeniji i privlače pažnju naučne zajednice. Posebno je značajno detaljno ispitati parametre sinteze koji utiču na promene u kristalnoj strukturi i morfologiji dobijenih kompozita, imajući u vidu da ove promene imaju značajan uticaj na krajnja funkcionalna svojstva. U ovom radu je proučavan kompozitni materijal zasnovan na bakterijskoj nanocelulozi BNC (kao početnoj komponenti) i feromagnetnom Fe3O4. BNC je dobijena aktivnošću bakterija sirćetnog vrenja nakon 7 dana rasta u odgovarajućem medijuma. Istraživanje je usmereno na optimizaciju uslova precipitacije Fe3O4, koji se odnose na promenu intervala stajanja BNC filmova u rastvoru soli gvožđa. Uticaj različitih uslova sinteze je analiziran metodama SEM-EDS, FTIR i XRD.
AB  - Development in many areas of engineering and technology are closely linked to the development of new or improvement of existing materials. Having in mind wide use of bacterial nanocellulose (BNC) in various areas of everyday life, from biomedicine, ecology to electronics, BNC-based composites are becoming widely used and attracting the attention of the scientific community. It is especially important to examine in detail the synthesis parameters that affect the changes in the crystal structure and morphology of the obtained composites, having in mind that these changes have a crucial influence on their final functional properties. In this paper, a composite material based on bacterial nanocellulose BNC (as the matrix) and ferromagnetic Fe3O4 was studied. BNC was obtained by the activity of acetic fermentation bacteria after 7 days of growth in a suitable medium. The research is aimed to optimization of the Fe3O4 precipitation conditions. It's especially considering the time interval of BNC films spend in the iron salt solution. The influence of the performed synthesis conditions was considered by the SEMEDS, FTIR and XRD methods.
PB  - Beograd : Savez inženjera i tehničara Srbije
T2  - Tehnika
T1  - Optimizacija parametara sinteze nanokompozita na bazi bakterijske nanoceluloze/Fe3O4
SP  - 273
EP  - 278
VL  - 76
IS  - 3
DO  - 10.5937/tehnika2103273J
UR  - https://hdl.handle.net/21.15107/rcub_dais_12342
ER  - 

@article{
author = "Janićijević, Aleksandra and Sknepnek, Aleksandra and Mirković, Miljana and Pavlović, Vladimir and Filipović, Suzana",
year = "2021",
abstract = "Napredak u mnogim oblastima tehnike i tehnologije je blisko povezan sa razvojem novih ili unapređenjem postojećih materijala. Imajući u vidu široku primenu bakterijske nanoceluloze (BNC) u raznim oblastima svakodnevnog života, od biomedicine, ekologije do elektronike, kompoziti na bazi BNC su sve rasprostranjeniji i privlače pažnju naučne zajednice. Posebno je značajno detaljno ispitati parametre sinteze koji utiču na promene u kristalnoj strukturi i morfologiji dobijenih kompozita, imajući u vidu da ove promene imaju značajan uticaj na krajnja funkcionalna svojstva. U ovom radu je proučavan kompozitni materijal zasnovan na bakterijskoj nanocelulozi BNC (kao početnoj komponenti) i feromagnetnom Fe3O4. BNC je dobijena aktivnošću bakterija sirćetnog vrenja nakon 7 dana rasta u odgovarajućem medijuma. Istraživanje je usmereno na optimizaciju uslova precipitacije Fe3O4, koji se odnose na promenu intervala stajanja BNC filmova u rastvoru soli gvožđa. Uticaj različitih uslova sinteze je analiziran metodama SEM-EDS, FTIR i XRD., Development in many areas of engineering and technology are closely linked to the development of new or improvement of existing materials. Having in mind wide use of bacterial nanocellulose (BNC) in various areas of everyday life, from biomedicine, ecology to electronics, BNC-based composites are becoming widely used and attracting the attention of the scientific community. It is especially important to examine in detail the synthesis parameters that affect the changes in the crystal structure and morphology of the obtained composites, having in mind that these changes have a crucial influence on their final functional properties. In this paper, a composite material based on bacterial nanocellulose BNC (as the matrix) and ferromagnetic Fe3O4 was studied. BNC was obtained by the activity of acetic fermentation bacteria after 7 days of growth in a suitable medium. The research is aimed to optimization of the Fe3O4 precipitation conditions. It's especially considering the time interval of BNC films spend in the iron salt solution. The influence of the performed synthesis conditions was considered by the SEMEDS, FTIR and XRD methods.",
publisher = "Beograd : Savez inženjera i tehničara Srbije",
journal = "Tehnika",
title = "Optimizacija parametara sinteze nanokompozita na bazi bakterijske nanoceluloze/Fe3O4",
pages = "273-278",
volume = "76",
number = "3",
doi = "10.5937/tehnika2103273J",
url = "https://hdl.handle.net/21.15107/rcub_dais_12342"
}

Janićijević, A., Sknepnek, A., Mirković, M., Pavlović, V.,& Filipović, S.. (2021). Optimizacija parametara sinteze nanokompozita na bazi bakterijske nanoceluloze/Fe3O4. in Tehnika
Beograd : Savez inženjera i tehničara Srbije., 76(3), 273-278.
https://doi.org/10.5937/tehnika2103273J
https://hdl.handle.net/21.15107/rcub_dais_12342

Janićijević A, Sknepnek A, Mirković M, Pavlović V, Filipović S. Optimizacija parametara sinteze nanokompozita na bazi bakterijske nanoceluloze/Fe3O4. in Tehnika. 2021;76(3):273-278.
doi:10.5937/tehnika2103273J
https://hdl.handle.net/21.15107/rcub_dais_12342 .

Janićijević, Aleksandra, Sknepnek, Aleksandra, Mirković, Miljana, Pavlović, Vladimir, Filipović, Suzana, "Optimizacija parametara sinteze nanokompozita na bazi bakterijske nanoceluloze/Fe3O4" in Tehnika, 76, no. 3 (2021):273-278,
https://doi.org/10.5937/tehnika2103273J .,
https://hdl.handle.net/21.15107/rcub_dais_12342 .

TY  - CONF
AU  - Mirković, Miljana
AU  - Filipović, Suzana
AU  - Masković, Pavle
AU  - Pavlović, Vladimir B.
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/12346
AB  - Due to the growing number of people infected with the new corona virus in the world, there is an increase in bacterial infections, which weakens the immunity. New knowledge about simple and low cost synthesis methods of materials with good structural and antimicrobial properties are of great importance nowadays. Combination of bio ceramic Hydroxyapatite material with good biocompatible characteristics and Titanium dioxide material with good degradation properties of organic molecules when combine together has ability to absorb and decompose the bacteria. Hydroxyapatite/titanium dioxide nanomaterials have been prepared by tree different synthesis route. The morphology and semi quantitative chemical analysis were characterized by scanning electron microscopy with energy dispersive X-ray analysis (SEM-EDX). Phase and structural characterization of obtained materials were determined using X-ray powder diffraction method (XRD). The crystallite sizes of the obtained materials were evaluated in the average range from 8 nm to 15 nm. Due to phase analysis by XRD characterization the peak shows presence of anatase phase with hydroxyapatite. Based on XRD peaks positions the hexagonal hydroxyapatite phases are formed in every synthesis route with TiO2 anatase phase. The microstructural studies confirmed that the nanosized HAp coated in a different way with TiO2 depending on a synthesis route. EDX analysis confirmed presence of Ti, Ca, P, O in obtained materials. The IR spectroscopy confirmed vibrational bands characteristic for HAp and titanium with anatase phase. The investigated materials show satisfactory antimicrobial properties.
PB  - Belgrade : Innovation Center of Faculty of Mechanical Engineering
C3  - Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia
T1  - Phase morphological and antimicrobial properties of HAp-TiO2 nanomaterials obtained by different synthesis route
SP  - 14
EP  - 14
UR  - https://hdl.handle.net/21.15107/rcub_dais_12346
ER  - 

@conference{
author = "Mirković, Miljana and Filipović, Suzana and Masković, Pavle and Pavlović, Vladimir B.",
year = "2021",
abstract = "Due to the growing number of people infected with the new corona virus in the world, there is an increase in bacterial infections, which weakens the immunity. New knowledge about simple and low cost synthesis methods of materials with good structural and antimicrobial properties are of great importance nowadays. Combination of bio ceramic Hydroxyapatite material with good biocompatible characteristics and Titanium dioxide material with good degradation properties of organic molecules when combine together has ability to absorb and decompose the bacteria. Hydroxyapatite/titanium dioxide nanomaterials have been prepared by tree different synthesis route. The morphology and semi quantitative chemical analysis were characterized by scanning electron microscopy with energy dispersive X-ray analysis (SEM-EDX). Phase and structural characterization of obtained materials were determined using X-ray powder diffraction method (XRD). The crystallite sizes of the obtained materials were evaluated in the average range from 8 nm to 15 nm. Due to phase analysis by XRD characterization the peak shows presence of anatase phase with hydroxyapatite. Based on XRD peaks positions the hexagonal hydroxyapatite phases are formed in every synthesis route with TiO2 anatase phase. The microstructural studies confirmed that the nanosized HAp coated in a different way with TiO2 depending on a synthesis route. EDX analysis confirmed presence of Ti, Ca, P, O in obtained materials. The IR spectroscopy confirmed vibrational bands characteristic for HAp and titanium with anatase phase. The investigated materials show satisfactory antimicrobial properties.",
publisher = "Belgrade : Innovation Center of Faculty of Mechanical Engineering",
journal = "Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia",
title = "Phase morphological and antimicrobial properties of HAp-TiO2 nanomaterials obtained by different synthesis route",
pages = "14-14",
url = "https://hdl.handle.net/21.15107/rcub_dais_12346"
}

Mirković, M., Filipović, S., Masković, P.,& Pavlović, V. B.. (2021). Phase morphological and antimicrobial properties of HAp-TiO2 nanomaterials obtained by different synthesis route. in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia
Belgrade : Innovation Center of Faculty of Mechanical Engineering., 14-14.
https://hdl.handle.net/21.15107/rcub_dais_12346

Mirković M, Filipović S, Masković P, Pavlović VB. Phase morphological and antimicrobial properties of HAp-TiO2 nanomaterials obtained by different synthesis route. in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia. 2021;:14-14.
https://hdl.handle.net/21.15107/rcub_dais_12346 .

Mirković, Miljana, Filipović, Suzana, Masković, Pavle, Pavlović, Vladimir B., "Phase morphological and antimicrobial properties of HAp-TiO2 nanomaterials obtained by different synthesis route" in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia (2021):14-14,
https://hdl.handle.net/21.15107/rcub_dais_12346 .

TY  - CONF
AU  - Sknepnek, Aleksandra
AU  - Filipović, Suzana
AU  - Masković, Pavle
AU  - Mirković, Miljana
AU  - Miletić, Dunja
AU  - Nikšić, Miomir
AU  - Pavlović, Vladimir B.
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/12348
AB  - Cellulose, as the main constituent of plants, is the most common natural material that is widely used. Bacterial cellulose (BC) is a polymer of β-1,4-glucan chains, extracellularly attached to bacterial cells. It possesses the same structure as plant cellulose but its application has many advantages. BC has tinner threads, better crystallinity, mechanical strength and higher purity. By the means of micro- and nano-pores in the structure, it is possible to retain nano particles and enhance the application of obtained nanostructures. BC lacks antibacterial and antioxidative activity, conductivity and magnetic properties, which lowers the possibility of its application in biomedicine and electronics. To overcome previously mentioned deficiency, it is possible to apply bioactive polymers, nanomaterials or solid particles into the structure. High biocidal potential of TiO2 originates from its photocatalytic properties, and the generation of reactive oxygen species (ROS). At the first site of action, they cause cell membrane damage and afterwards, they attack intracellular components causing cell death. Hydroxyapatite (HAp) is capable to act synergistically with TiO2 and to accelerate its efficiency. Having in mind all characteristics of previously mentioned components, we have investigated the structure, morphology, mechanical properties and antimicrobial activity of advanced ceramics/polymer films. The influence of synthesis duration on BC structure, produced by Komagataeibacter xylinus species, was investigated. Thereafter, the possibility of TiO2/HAp ceramic nanocomposite application in BC was examined. The developed structures were analyzed by SEM and EDS analyzes, as well as XRD and FTIR spectroscopy. Mechanical properties were investigated as well.
PB  - Belgrade : Innovation Center of Faculty of Mechanical Engineering
C3  - Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia
T1  - Effects of synthesis parameters on structure and properties of the ceramic/polymer films based on bacterial cellulose
SP  - 78
EP  - 78
UR  - https://hdl.handle.net/21.15107/rcub_dais_12348
ER  - 

@conference{
author = "Sknepnek, Aleksandra and Filipović, Suzana and Masković, Pavle and Mirković, Miljana and Miletić, Dunja and Nikšić, Miomir and Pavlović, Vladimir B.",
year = "2021",
abstract = "Cellulose, as the main constituent of plants, is the most common natural material that is widely used. Bacterial cellulose (BC) is a polymer of β-1,4-glucan chains, extracellularly attached to bacterial cells. It possesses the same structure as plant cellulose but its application has many advantages. BC has tinner threads, better crystallinity, mechanical strength and higher purity. By the means of micro- and nano-pores in the structure, it is possible to retain nano particles and enhance the application of obtained nanostructures. BC lacks antibacterial and antioxidative activity, conductivity and magnetic properties, which lowers the possibility of its application in biomedicine and electronics. To overcome previously mentioned deficiency, it is possible to apply bioactive polymers, nanomaterials or solid particles into the structure. High biocidal potential of TiO2 originates from its photocatalytic properties, and the generation of reactive oxygen species (ROS). At the first site of action, they cause cell membrane damage and afterwards, they attack intracellular components causing cell death. Hydroxyapatite (HAp) is capable to act synergistically with TiO2 and to accelerate its efficiency. Having in mind all characteristics of previously mentioned components, we have investigated the structure, morphology, mechanical properties and antimicrobial activity of advanced ceramics/polymer films. The influence of synthesis duration on BC structure, produced by Komagataeibacter xylinus species, was investigated. Thereafter, the possibility of TiO2/HAp ceramic nanocomposite application in BC was examined. The developed structures were analyzed by SEM and EDS analyzes, as well as XRD and FTIR spectroscopy. Mechanical properties were investigated as well.",
publisher = "Belgrade : Innovation Center of Faculty of Mechanical Engineering",
journal = "Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia",
title = "Effects of synthesis parameters on structure and properties of the ceramic/polymer films based on bacterial cellulose",
pages = "78-78",
url = "https://hdl.handle.net/21.15107/rcub_dais_12348"
}

Sknepnek, A., Filipović, S., Masković, P., Mirković, M., Miletić, D., Nikšić, M.,& Pavlović, V. B.. (2021). Effects of synthesis parameters on structure and properties of the ceramic/polymer films based on bacterial cellulose. in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia
Belgrade : Innovation Center of Faculty of Mechanical Engineering., 78-78.
https://hdl.handle.net/21.15107/rcub_dais_12348

Sknepnek A, Filipović S, Masković P, Mirković M, Miletić D, Nikšić M, Pavlović VB. Effects of synthesis parameters on structure and properties of the ceramic/polymer films based on bacterial cellulose. in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia. 2021;:78-78.
https://hdl.handle.net/21.15107/rcub_dais_12348 .

Sknepnek, Aleksandra, Filipović, Suzana, Masković, Pavle, Mirković, Miljana, Miletić, Dunja, Nikšić, Miomir, Pavlović, Vladimir B., "Effects of synthesis parameters on structure and properties of the ceramic/polymer films based on bacterial cellulose" in Programme and The Book of Abstracts / International Conference of Experimental and Numerical Investigations and New Technologies - CNN TECH 2021,29 June - 02 July 2021, Zlatibor, Serbia (2021):78-78,
https://hdl.handle.net/21.15107/rcub_dais_12348 .

TY  - CONF
AU  - Janićijević, Aleksandra
AU  - Filipović, Suzana
AU  - Pavlović, Vladimir B.
AU  - Sknepnek, Aleksandra
AU  - Kovačević, Danijela
AU  - Đorđević, Nenad
AU  - Mirković, Miljana
AU  - Živković, Predrag
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/12356
AB  - Kao jedan od najzastupljenijih biopolimera na Zemlji, celuloza je našla primenu u prehrambenoj industriji, biomedicini i biotehnologiji. Dobijanje celuloznih vlakana iz biljaka je praćeno prisustvom nusproizvoda, čije je uklanjanje zahtevan proces. Stoga, materijali na bazi bakterijske nanoceluloze (BCN), nalaze sve širu primenu u svakodnevnici. Imajući u vidu prednosti BCN, u ovom radu su ispitivane promene u strukturi i morfologiji BCN u funkciji parametara sinteze. Analiziran je uticaj vrste i zapremine medijuma, kao i dužine prečišćavanja u NaOH, na promene u prinosu i strukturi BCN. Navedene promene su ispitivane metodama XRD, FTIR, kao i primenom SEM i EDS analize.
AB  - As one of the most common biopolymers on Earth, cellulose has found an important role in food industry, biomedicine andbiotechnology. The process of obtaining cellulose fibers is often followed with the presence of the byproduct, whose removal is required procedure. From that reason, the process of obtaining material on a bacterial cellulose (BC) basis,finds wide application in everyday life. Having in mind her many features, we have investigated the change in structure and morphology of BC depending on the synthesis parameters. The influence of the medium volume and different time intervals of NaOH treatment relative to different BCN yields and structure. The mentioned changes were examined by XRD, FTIR spectroscopy, as well as SEM and EDS analyzes.
PB  - Čačak : Univerzitet u Kragujevcu, Agronomski fakultet
C3  - Zbornik radova [Elektronski izvor] / XXVI savetovanje o biotehnologiji sa međunarodnim učešćem, Čačak, 12 - 13. mart 2021. godine
T1  - Sinteza i struktura bakterijske celuloze primenom bakterija sirćetnog vrenja
SP  - 281
EP  - 289
DO  - 10.46793/SBT26.281J
UR  - https://hdl.handle.net/21.15107/rcub_dais_12356
ER  - 

@conference{
author = "Janićijević, Aleksandra and Filipović, Suzana and Pavlović, Vladimir B. and Sknepnek, Aleksandra and Kovačević, Danijela and Đorđević, Nenad and Mirković, Miljana and Živković, Predrag",
year = "2021",
abstract = "Kao jedan od najzastupljenijih biopolimera na Zemlji, celuloza je našla primenu u prehrambenoj industriji, biomedicini i biotehnologiji. Dobijanje celuloznih vlakana iz biljaka je praćeno prisustvom nusproizvoda, čije je uklanjanje zahtevan proces. Stoga, materijali na bazi bakterijske nanoceluloze (BCN), nalaze sve širu primenu u svakodnevnici. Imajući u vidu prednosti BCN, u ovom radu su ispitivane promene u strukturi i morfologiji BCN u funkciji parametara sinteze. Analiziran je uticaj vrste i zapremine medijuma, kao i dužine prečišćavanja u NaOH, na promene u prinosu i strukturi BCN. Navedene promene su ispitivane metodama XRD, FTIR, kao i primenom SEM i EDS analize., As one of the most common biopolymers on Earth, cellulose has found an important role in food industry, biomedicine andbiotechnology. The process of obtaining cellulose fibers is often followed with the presence of the byproduct, whose removal is required procedure. From that reason, the process of obtaining material on a bacterial cellulose (BC) basis,finds wide application in everyday life. Having in mind her many features, we have investigated the change in structure and morphology of BC depending on the synthesis parameters. The influence of the medium volume and different time intervals of NaOH treatment relative to different BCN yields and structure. The mentioned changes were examined by XRD, FTIR spectroscopy, as well as SEM and EDS analyzes.",
publisher = "Čačak : Univerzitet u Kragujevcu, Agronomski fakultet",
journal = "Zbornik radova [Elektronski izvor] / XXVI savetovanje o biotehnologiji sa međunarodnim učešćem, Čačak, 12 - 13. mart 2021. godine",
title = "Sinteza i struktura bakterijske celuloze primenom bakterija sirćetnog vrenja",
pages = "281-289",
doi = "10.46793/SBT26.281J",
url = "https://hdl.handle.net/21.15107/rcub_dais_12356"
}

Janićijević, A., Filipović, S., Pavlović, V. B., Sknepnek, A., Kovačević, D., Đorđević, N., Mirković, M.,& Živković, P.. (2021). Sinteza i struktura bakterijske celuloze primenom bakterija sirćetnog vrenja. in Zbornik radova [Elektronski izvor] / XXVI savetovanje o biotehnologiji sa međunarodnim učešćem, Čačak, 12 - 13. mart 2021. godine
Čačak : Univerzitet u Kragujevcu, Agronomski fakultet., 281-289.
https://doi.org/10.46793/SBT26.281J
https://hdl.handle.net/21.15107/rcub_dais_12356

Janićijević A, Filipović S, Pavlović VB, Sknepnek A, Kovačević D, Đorđević N, Mirković M, Živković P. Sinteza i struktura bakterijske celuloze primenom bakterija sirćetnog vrenja. in Zbornik radova [Elektronski izvor] / XXVI savetovanje o biotehnologiji sa međunarodnim učešćem, Čačak, 12 - 13. mart 2021. godine. 2021;:281-289.
doi:10.46793/SBT26.281J
https://hdl.handle.net/21.15107/rcub_dais_12356 .

Janićijević, Aleksandra, Filipović, Suzana, Pavlović, Vladimir B., Sknepnek, Aleksandra, Kovačević, Danijela, Đorđević, Nenad, Mirković, Miljana, Živković, Predrag, "Sinteza i struktura bakterijske celuloze primenom bakterija sirćetnog vrenja" in Zbornik radova [Elektronski izvor] / XXVI savetovanje o biotehnologiji sa međunarodnim učešćem, Čačak, 12 - 13. mart 2021. godine (2021):281-289,
https://doi.org/10.46793/SBT26.281J .,
https://hdl.handle.net/21.15107/rcub_dais_12356 .

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Anđelković, Ljubica
AU  - Olćan, Dragan
AU  - Petrović, Jovana
AU  - Mirković, Miljana
AU  - Pavlović, Vladimir B.
AU  - Jeremić, Dejan
AU  - Vlahović, Branislav
AU  - Đorđević, Antonije
PY  - 2021
UR  - https://dais.sanu.ac.rs/123456789/11230
AB  - Solid-state reaction between BaTiO3 and Fe2O3 was used to produce a multiferroic heterostructure composite. Commercial BaTiO3 and Fe(NO3)3•9H2O were suspended in ethanol for 30 minutes in an ultrasound bath. The prepared mixture was thermally processed at 300 oC for 6 h. Sintering at 1300 oC for 1 h resulted in a mixture of different phases, BaTiO3, BaFe12O19 and Ba12Ti28Fe15O84, which were confirmed by x-ray powder diffraction. A dense microstructure with a small volume fraction of closed porosity was indicated by the scanning electron microscopy, while a homogeneous distribution of Fe ions over BaTiO3 phase was visible from energy dispersive spectroscopy mapping. Doping of BaTiO3 with Fe2O3 resulted in formation of magnetic hexaferrite phases, as confirmed by dielectric measurements that showed a broadened maximum of the permittivity measured as a function of temperature.
PB  - Belgrade : International Institute for the Science of Sintering
T2  - Science of Sintering
T1  - Multiferroic Heterostructure BaTiO3/ε-Fe2O3 Composite Obtained by in situ Reaction
SP  - 1
EP  - 8
VL  - 53
DO  - 10.2298/SOS2101001F
UR  - https://hdl.handle.net/21.15107/rcub_dais_11230
ER  - 

@article{
author = "Filipović, Suzana and Obradović, Nina and Anđelković, Ljubica and Olćan, Dragan and Petrović, Jovana and Mirković, Miljana and Pavlović, Vladimir B. and Jeremić, Dejan and Vlahović, Branislav and Đorđević, Antonije",
year = "2021",
abstract = "Solid-state reaction between BaTiO3 and Fe2O3 was used to produce a multiferroic heterostructure composite. Commercial BaTiO3 and Fe(NO3)3•9H2O were suspended in ethanol for 30 minutes in an ultrasound bath. The prepared mixture was thermally processed at 300 oC for 6 h. Sintering at 1300 oC for 1 h resulted in a mixture of different phases, BaTiO3, BaFe12O19 and Ba12Ti28Fe15O84, which were confirmed by x-ray powder diffraction. A dense microstructure with a small volume fraction of closed porosity was indicated by the scanning electron microscopy, while a homogeneous distribution of Fe ions over BaTiO3 phase was visible from energy dispersive spectroscopy mapping. Doping of BaTiO3 with Fe2O3 resulted in formation of magnetic hexaferrite phases, as confirmed by dielectric measurements that showed a broadened maximum of the permittivity measured as a function of temperature.",
publisher = "Belgrade : International Institute for the Science of Sintering",
journal = "Science of Sintering",
title = "Multiferroic Heterostructure BaTiO3/ε-Fe2O3 Composite Obtained by in situ Reaction",
pages = "1-8",
volume = "53",
doi = "10.2298/SOS2101001F",
url = "https://hdl.handle.net/21.15107/rcub_dais_11230"
}

Filipović, S., Obradović, N., Anđelković, L., Olćan, D., Petrović, J., Mirković, M., Pavlović, V. B., Jeremić, D., Vlahović, B.,& Đorđević, A.. (2021). Multiferroic Heterostructure BaTiO3/ε-Fe2O3 Composite Obtained by in situ Reaction. in Science of Sintering
Belgrade : International Institute for the Science of Sintering., 53, 1-8.
https://doi.org/10.2298/SOS2101001F
https://hdl.handle.net/21.15107/rcub_dais_11230

Filipović S, Obradović N, Anđelković L, Olćan D, Petrović J, Mirković M, Pavlović VB, Jeremić D, Vlahović B, Đorđević A. Multiferroic Heterostructure BaTiO3/ε-Fe2O3 Composite Obtained by in situ Reaction. in Science of Sintering. 2021;53:1-8.
doi:10.2298/SOS2101001F
https://hdl.handle.net/21.15107/rcub_dais_11230 .

Filipović, Suzana, Obradović, Nina, Anđelković, Ljubica, Olćan, Dragan, Petrović, Jovana, Mirković, Miljana, Pavlović, Vladimir B., Jeremić, Dejan, Vlahović, Branislav, Đorđević, Antonije, "Multiferroic Heterostructure BaTiO3/ε-Fe2O3 Composite Obtained by in situ Reaction" in Science of Sintering, 53 (2021):1-8,
https://doi.org/10.2298/SOS2101001F .,
https://hdl.handle.net/21.15107/rcub_dais_11230 .

TY  - CONF
AU  - Vukčević, Mira
AU  - Bošković, Ivana
AU  - Nenadović, Snežana S.
AU  - Mirković, Miljana M.
AU  - Gulicovski, Jelena
AU  - Pavlović, Vladimir B.
AU  - Kljajević, Ljiljana M.
PY  - 2019
UR  - https://dais.sanu.ac.rs/123456789/7004
AB  - Hybrid geopolymers represent a new class of composite materials formed by incorporating organic polymer into a geopolymer matrix. The properties of hybrid geopolymer depend on the addition of organic phase and the starting raw material composition (concentration of NaOH in alkaline activator, Si/Al mass ratio and solid/liquid mass ratio). In addition to these relevant parameters, this paper examines the synthesis conditions of these materials through the influence of the type, amount and manner of adding organic modifiers (commercial epoxy resins and 3- (methoxyl) propyl methacrylates) on forming the structure with significantly reduced pore distribution and decreased pore size, which exhibits good mechanical properties. The purpose of this research is to define the optimal conditions of the hybrid geopolymers' synthesis through the examination of relevant parameters. Expected improvement of mechanical properties was confirmed through values of compressive stength. Characterization of hybrid geopolymer composities was performed by XRD analysis, DRIFT spectroscopy and SEM analysis.
PB  - Belgrade : Institute for Multidisciplinary Research
C3  - Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia
T1  - The potential of hybrid geopolymer composites
SP  - 71
EP  - 71
UR  - https://hdl.handle.net/21.15107/rcub_dais_7004
ER  - 

@conference{
author = "Vukčević, Mira and Bošković, Ivana and Nenadović, Snežana S. and Mirković, Miljana M. and Gulicovski, Jelena and Pavlović, Vladimir B. and Kljajević, Ljiljana M.",
year = "2019",
abstract = "Hybrid geopolymers represent a new class of composite materials formed by incorporating organic polymer into a geopolymer matrix. The properties of hybrid geopolymer depend on the addition of organic phase and the starting raw material composition (concentration of NaOH in alkaline activator, Si/Al mass ratio and solid/liquid mass ratio). In addition to these relevant parameters, this paper examines the synthesis conditions of these materials through the influence of the type, amount and manner of adding organic modifiers (commercial epoxy resins and 3- (methoxyl) propyl methacrylates) on forming the structure with significantly reduced pore distribution and decreased pore size, which exhibits good mechanical properties. The purpose of this research is to define the optimal conditions of the hybrid geopolymers' synthesis through the examination of relevant parameters. Expected improvement of mechanical properties was confirmed through values of compressive stength. Characterization of hybrid geopolymer composities was performed by XRD analysis, DRIFT spectroscopy and SEM analysis.",
publisher = "Belgrade : Institute for Multidisciplinary Research",
journal = "Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia",
title = "The potential of hybrid geopolymer composites",
pages = "71-71",
url = "https://hdl.handle.net/21.15107/rcub_dais_7004"
}

Vukčević, M., Bošković, I., Nenadović, S. S., Mirković, M. M., Gulicovski, J., Pavlović, V. B.,& Kljajević, L. M.. (2019). The potential of hybrid geopolymer composites. in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia
Belgrade : Institute for Multidisciplinary Research., 71-71.
https://hdl.handle.net/21.15107/rcub_dais_7004

Vukčević M, Bošković I, Nenadović SS, Mirković MM, Gulicovski J, Pavlović VB, Kljajević LM. The potential of hybrid geopolymer composites. in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia. 2019;:71-71.
https://hdl.handle.net/21.15107/rcub_dais_7004 .

Vukčević, Mira, Bošković, Ivana, Nenadović, Snežana S., Mirković, Miljana M., Gulicovski, Jelena, Pavlović, Vladimir B., Kljajević, Ljiljana M., "The potential of hybrid geopolymer composites" in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia (2019):71-71,
https://hdl.handle.net/21.15107/rcub_dais_7004 .

TY  - CONF
AU  - Đukić, Dunja
AU  - Nenadović, Snežana S.
AU  - Kljajević, Ljiljana M.
AU  - Pavlović, Vladimir B.
AU  - Ivanović, Marija D.
AU  - Nenadović, Miloš T.
AU  - Mirković, Miljana M.
PY  - 2019
UR  - https://dais.sanu.ac.rs/123456789/6964
AB  - In a field of green chemistry, environmental protection and ecological conservation of the environment there are ways to come up with new and more advanced materials using on the one hand natural, recyceled or waste materials and on the other hand syntethic materials obtained by using green chemistry synthesis procedures. The aim of this paper was to synthesize and characterize Brushite-metakaolin-based geopolymer materials and to examine the possibility of using these materials in the fields of construction, cement industry, as well as in environmental protection as potential adsorbents. Initial materials which were used for geopolymer synthesis was Brushite (CaHPO4·2H2O) which was obtained by solutionprecipitation reaction form acetate solutions and Kaolinite clay from Rudovci deposit (Serbia). The obtained mixture powders were dissolved in a strong alcaline solution with addiction of water glass. Produced geopolymers was cast into mods and preserved for 28 days. The starting materials and the synthesized Brushite-metakaolin-based geopolymer material were examined using XRPD, FTIR SEM-EDS methods. The contact angle measurements were made to test hydrophilic and wettable properties of synthesized material.
PB  - Belgrade : Institute of Technical Sciences of SASA
C3  - Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
T1  - Synthesis and characterization of Brushite-metakaolin-based geopolymer materials
SP  - 86
EP  - 86
UR  - https://hdl.handle.net/21.15107/rcub_dais_6964
ER  - 

@conference{
author = "Đukić, Dunja and Nenadović, Snežana S. and Kljajević, Ljiljana M. and Pavlović, Vladimir B. and Ivanović, Marija D. and Nenadović, Miloš T. and Mirković, Miljana M.",
year = "2019",
abstract = "In a field of green chemistry, environmental protection and ecological conservation of the environment there are ways to come up with new and more advanced materials using on the one hand natural, recyceled or waste materials and on the other hand syntethic materials obtained by using green chemistry synthesis procedures. The aim of this paper was to synthesize and characterize Brushite-metakaolin-based geopolymer materials and to examine the possibility of using these materials in the fields of construction, cement industry, as well as in environmental protection as potential adsorbents. Initial materials which were used for geopolymer synthesis was Brushite (CaHPO4·2H2O) which was obtained by solutionprecipitation reaction form acetate solutions and Kaolinite clay from Rudovci deposit (Serbia). The obtained mixture powders were dissolved in a strong alcaline solution with addiction of water glass. Produced geopolymers was cast into mods and preserved for 28 days. The starting materials and the synthesized Brushite-metakaolin-based geopolymer material were examined using XRPD, FTIR SEM-EDS methods. The contact angle measurements were made to test hydrophilic and wettable properties of synthesized material.",
publisher = "Belgrade : Institute of Technical Sciences of SASA",
journal = "Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia",
title = "Synthesis and characterization of Brushite-metakaolin-based geopolymer materials",
pages = "86-86",
url = "https://hdl.handle.net/21.15107/rcub_dais_6964"
}

Đukić, D., Nenadović, S. S., Kljajević, L. M., Pavlović, V. B., Ivanović, M. D., Nenadović, M. T.,& Mirković, M. M.. (2019). Synthesis and characterization of Brushite-metakaolin-based geopolymer materials. in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
Belgrade : Institute of Technical Sciences of SASA., 86-86.
https://hdl.handle.net/21.15107/rcub_dais_6964

Đukić D, Nenadović SS, Kljajević LM, Pavlović VB, Ivanović MD, Nenadović MT, Mirković MM. Synthesis and characterization of Brushite-metakaolin-based geopolymer materials. in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia. 2019;:86-86.
https://hdl.handle.net/21.15107/rcub_dais_6964 .

Đukić, Dunja, Nenadović, Snežana S., Kljajević, Ljiljana M., Pavlović, Vladimir B., Ivanović, Marija D., Nenadović, Miloš T., Mirković, Miljana M., "Synthesis and characterization of Brushite-metakaolin-based geopolymer materials" in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia (2019):86-86,
https://hdl.handle.net/21.15107/rcub_dais_6964 .

TY  - CONF
AU  - Ivanović, Marija D.
AU  - Đukić, Dunja
AU  - Mladenović, Nataša
AU  - Kljajević, Ljiljana M.
AU  - Pavlović, Vladimir B.
AU  - Nenadović, Snežana S.
AU  - Mirković, Miljana M.
PY  - 2019
UR  - https://dais.sanu.ac.rs/123456789/6965
AB  - In order to optimize process of geopolymerization, the investigation of thermodynamic parameters of alkali activators are important. The aim of this research was to investigate the influence of thermodynamic parameters (density, viscosity, refractive index and sound velocity) of alkaline activators on mechanical properties (compressive strength and hardness) of synthesized geopolymer samples. Geopolymers were synthetized by alkaline activation of metakaolin, having the density 2.524 g/cm3, using the activators at elevated temperature of 60 oC for two days. Based on the obtained results thermodynamic properties has been selected to predict the properties of materials. Four series of alkaline activators have been used. Activators remarked as AA1, AA2, AA3 and AA4 present the mixtures of Na2SiO3 and solutions of NaOH, of different molarities 2M, 4M, 6M and 8M respectively. The volume ratio of Na2SiO3 and aqueous solution of NaOH was the same for all samples. Densities, viscosities and refractive indices of alkaline activators were determined over the temperature range 15-60 oC of process of geopolymerizations. The values of density, viscosity and refractive index decrease with temperature increase over the investigated temperature range. Increasing molarity of alkali activator solutions, the sound velocity of activators is changed. For sample AA2 the values of sound velocity rises from room temperature to 45 °C and then begins to decrease while for the sample AA3 sound velocity grows until 30 °C and then starts to decrease with further increasing of temperature. Four series of geopolymer samples GP1 to GP4 were synthesiyed using the constant ratio of solid and liquid phase. FTIR, XRD, SEM-EDS methods were used for physicochemical further characterization of geopolymer samples.
PB  - Belgrade : Institute of Technical Sciences of SASA
C3  - Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
T1  - The influence of thermodynamic parameters of the alkaline activator on the mechanical properties of geopolymers
SP  - 87
EP  - 87
UR  - https://hdl.handle.net/21.15107/rcub_dais_6965
ER  - 

@conference{
author = "Ivanović, Marija D. and Đukić, Dunja and Mladenović, Nataša and Kljajević, Ljiljana M. and Pavlović, Vladimir B. and Nenadović, Snežana S. and Mirković, Miljana M.",
year = "2019",
abstract = "In order to optimize process of geopolymerization, the investigation of thermodynamic parameters of alkali activators are important. The aim of this research was to investigate the influence of thermodynamic parameters (density, viscosity, refractive index and sound velocity) of alkaline activators on mechanical properties (compressive strength and hardness) of synthesized geopolymer samples. Geopolymers were synthetized by alkaline activation of metakaolin, having the density 2.524 g/cm3, using the activators at elevated temperature of 60 oC for two days. Based on the obtained results thermodynamic properties has been selected to predict the properties of materials. Four series of alkaline activators have been used. Activators remarked as AA1, AA2, AA3 and AA4 present the mixtures of Na2SiO3 and solutions of NaOH, of different molarities 2M, 4M, 6M and 8M respectively. The volume ratio of Na2SiO3 and aqueous solution of NaOH was the same for all samples. Densities, viscosities and refractive indices of alkaline activators were determined over the temperature range 15-60 oC of process of geopolymerizations. The values of density, viscosity and refractive index decrease with temperature increase over the investigated temperature range. Increasing molarity of alkali activator solutions, the sound velocity of activators is changed. For sample AA2 the values of sound velocity rises from room temperature to 45 °C and then begins to decrease while for the sample AA3 sound velocity grows until 30 °C and then starts to decrease with further increasing of temperature. Four series of geopolymer samples GP1 to GP4 were synthesiyed using the constant ratio of solid and liquid phase. FTIR, XRD, SEM-EDS methods were used for physicochemical further characterization of geopolymer samples.",
publisher = "Belgrade : Institute of Technical Sciences of SASA",
journal = "Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia",
title = "The influence of thermodynamic parameters of the alkaline activator on the mechanical properties of geopolymers",
pages = "87-87",
url = "https://hdl.handle.net/21.15107/rcub_dais_6965"
}

Ivanović, M. D., Đukić, D., Mladenović, N., Kljajević, L. M., Pavlović, V. B., Nenadović, S. S.,& Mirković, M. M.. (2019). The influence of thermodynamic parameters of the alkaline activator on the mechanical properties of geopolymers. in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
Belgrade : Institute of Technical Sciences of SASA., 87-87.
https://hdl.handle.net/21.15107/rcub_dais_6965

Ivanović MD, Đukić D, Mladenović N, Kljajević LM, Pavlović VB, Nenadović SS, Mirković MM. The influence of thermodynamic parameters of the alkaline activator on the mechanical properties of geopolymers. in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia. 2019;:87-87.
https://hdl.handle.net/21.15107/rcub_dais_6965 .

Ivanović, Marija D., Đukić, Dunja, Mladenović, Nataša, Kljajević, Ljiljana M., Pavlović, Vladimir B., Nenadović, Snežana S., Mirković, Miljana M., "The influence of thermodynamic parameters of the alkaline activator on the mechanical properties of geopolymers" in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia (2019):87-87,
https://hdl.handle.net/21.15107/rcub_dais_6965 .

TY  - CONF
AU  - Vukčević, Mira
AU  - Bošković, Ivana
AU  - Nenadović, Snežana S.
AU  - Mirković, Miljana M.
AU  - Čalija, Bojan
AU  - Pavlović, Vladimir B.
AU  - Kljajević, Ljiljana M.
PY  - 2017
UR  - https://dais.sanu.ac.rs/123456789/15438
AB  - There is potential use of red mud for synthesis of inorganic polymeric materials through a geopolymerization process as an alternative in the sectors of construction and building materials. By introducing of inorganic and organic modificators of microstructure (calcium hydroxide, bifunctional epoxy resins, or various types of alkoxylanes) during the geopolymer synthesis the enhanced values of ductility and strength can be obtained. Research was performed on alumosilicate material (red mud and metakaolin) and alkali activator raw mixture with defined quantity of modificator. The best sinthesys conditions were identified. Post-synthesis curing also play important role in obtaining of good-performing geopolymers. Characteristics of geopolymers were defined by measuring of compressive strength, N2-physisorption, as well as by SEM analysis, X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR). In addition the lower value of zeta potential was identified as the assisting factor for the specific structure domains formation (within the certain range of pH) accompanied by the high compressive strength.
PB  - Belgrade : Materials Research Society of Serbia
C3  - Programme and The Book of Abstracts / Nineteenth Annual Conference YUCOMAT 2017, Herceg Novi, September 4-8, 2017
T1  - Composition of red mud and/or metakaolin-based modified geopolymers
SP  - 72
EP  - 72
UR  - https://hdl.handle.net/21.15107/rcub_dais_15438
ER  - 

@conference{
author = "Vukčević, Mira and Bošković, Ivana and Nenadović, Snežana S. and Mirković, Miljana M. and Čalija, Bojan and Pavlović, Vladimir B. and Kljajević, Ljiljana M.",
year = "2017",
abstract = "There is potential use of red mud for synthesis of inorganic polymeric materials through a geopolymerization process as an alternative in the sectors of construction and building materials. By introducing of inorganic and organic modificators of microstructure (calcium hydroxide, bifunctional epoxy resins, or various types of alkoxylanes) during the geopolymer synthesis the enhanced values of ductility and strength can be obtained. Research was performed on alumosilicate material (red mud and metakaolin) and alkali activator raw mixture with defined quantity of modificator. The best sinthesys conditions were identified. Post-synthesis curing also play important role in obtaining of good-performing geopolymers. Characteristics of geopolymers were defined by measuring of compressive strength, N2-physisorption, as well as by SEM analysis, X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR). In addition the lower value of zeta potential was identified as the assisting factor for the specific structure domains formation (within the certain range of pH) accompanied by the high compressive strength.",
publisher = "Belgrade : Materials Research Society of Serbia",
journal = "Programme and The Book of Abstracts / Nineteenth Annual Conference YUCOMAT 2017, Herceg Novi, September 4-8, 2017",
title = "Composition of red mud and/or metakaolin-based modified geopolymers",
pages = "72-72",
url = "https://hdl.handle.net/21.15107/rcub_dais_15438"
}

Vukčević, M., Bošković, I., Nenadović, S. S., Mirković, M. M., Čalija, B., Pavlović, V. B.,& Kljajević, L. M.. (2017). Composition of red mud and/or metakaolin-based modified geopolymers. in Programme and The Book of Abstracts / Nineteenth Annual Conference YUCOMAT 2017, Herceg Novi, September 4-8, 2017
Belgrade : Materials Research Society of Serbia., 72-72.
https://hdl.handle.net/21.15107/rcub_dais_15438

Vukčević M, Bošković I, Nenadović SS, Mirković MM, Čalija B, Pavlović VB, Kljajević LM. Composition of red mud and/or metakaolin-based modified geopolymers. in Programme and The Book of Abstracts / Nineteenth Annual Conference YUCOMAT 2017, Herceg Novi, September 4-8, 2017. 2017;:72-72.
https://hdl.handle.net/21.15107/rcub_dais_15438 .

Vukčević, Mira, Bošković, Ivana, Nenadović, Snežana S., Mirković, Miljana M., Čalija, Bojan, Pavlović, Vladimir B., Kljajević, Ljiljana M., "Composition of red mud and/or metakaolin-based modified geopolymers" in Programme and The Book of Abstracts / Nineteenth Annual Conference YUCOMAT 2017, Herceg Novi, September 4-8, 2017 (2017):72-72,
https://hdl.handle.net/21.15107/rcub_dais_15438 .

TY  - CONF
AU  - Omerašević, Mia
AU  - Lukić, Miodrag J.
AU  - Baščarević, Zvezdana
AU  - Orlić, Jovana
AU  - Mirković, Miljana M.
AU  - Savić-Biserčić, Marjetka
AU  - Matović, Ljiljana Lj.
PY  - 2015
UR  - https://dais.sanu.ac.rs/123456789/837
AB  - Cesium aluminosilicate phases are of the great interest as possible host for Cs immobilization in radioactive waste management. The possibility to use zeolite as a host material for radioactive Cs immobilization was investigated. Cs-exchanged forms of clinoptilolite and 13X which were prepared by ion-exchange treatment were compacted. The powders compacts of exchanged zeolites were thermally treated at 1200 °C. The XRD analysis showed that Cs was successfully immobilized after heat treatment by formation of stable cesium-aluminosilicate ceramic forms. Thermal and mechanical properties of the sintered samples were investigated. From the perspective of these characteristics, Cs-exchanged zeolite (clinoptilolite and 13 X) can be considered as a potential material for safe waste disposal.
PB  - Belgrade : Institute of Technical Sciences of SASA
C3  - Program and the Book of Abstracts / Fourteenth Young Researchers' Conference Materials Sciences and Engineering, December 9-11, 2015, Belgrade, Serbia
T1  - Safe trapping of Cs radionuclides in sintered matrix of zeolites
SP  - 45
EP  - 45
UR  - https://hdl.handle.net/21.15107/rcub_dais_837
ER  - 

@conference{
author = "Omerašević, Mia and Lukić, Miodrag J. and Baščarević, Zvezdana and Orlić, Jovana and Mirković, Miljana M. and Savić-Biserčić, Marjetka and Matović, Ljiljana Lj.",
year = "2015",
abstract = "Cesium aluminosilicate phases are of the great interest as possible host for Cs immobilization in radioactive waste management. The possibility to use zeolite as a host material for radioactive Cs immobilization was investigated. Cs-exchanged forms of clinoptilolite and 13X which were prepared by ion-exchange treatment were compacted. The powders compacts of exchanged zeolites were thermally treated at 1200 °C. The XRD analysis showed that Cs was successfully immobilized after heat treatment by formation of stable cesium-aluminosilicate ceramic forms. Thermal and mechanical properties of the sintered samples were investigated. From the perspective of these characteristics, Cs-exchanged zeolite (clinoptilolite and 13 X) can be considered as a potential material for safe waste disposal.",
publisher = "Belgrade : Institute of Technical Sciences of SASA",
journal = "Program and the Book of Abstracts / Fourteenth Young Researchers' Conference Materials Sciences and Engineering, December 9-11, 2015, Belgrade, Serbia",
title = "Safe trapping of Cs radionuclides in sintered matrix of zeolites",
pages = "45-45",
url = "https://hdl.handle.net/21.15107/rcub_dais_837"
}

Omerašević, M., Lukić, M. J., Baščarević, Z., Orlić, J., Mirković, M. M., Savić-Biserčić, M.,& Matović, L. Lj.. (2015). Safe trapping of Cs radionuclides in sintered matrix of zeolites. in Program and the Book of Abstracts / Fourteenth Young Researchers' Conference Materials Sciences and Engineering, December 9-11, 2015, Belgrade, Serbia
Belgrade : Institute of Technical Sciences of SASA., 45-45.
https://hdl.handle.net/21.15107/rcub_dais_837

Omerašević M, Lukić MJ, Baščarević Z, Orlić J, Mirković MM, Savić-Biserčić M, Matović LL. Safe trapping of Cs radionuclides in sintered matrix of zeolites. in Program and the Book of Abstracts / Fourteenth Young Researchers' Conference Materials Sciences and Engineering, December 9-11, 2015, Belgrade, Serbia. 2015;:45-45.
https://hdl.handle.net/21.15107/rcub_dais_837 .

Omerašević, Mia, Lukić, Miodrag J., Baščarević, Zvezdana, Orlić, Jovana, Mirković, Miljana M., Savić-Biserčić, Marjetka, Matović, Ljiljana Lj., "Safe trapping of Cs radionuclides in sintered matrix of zeolites" in Program and the Book of Abstracts / Fourteenth Young Researchers' Conference Materials Sciences and Engineering, December 9-11, 2015, Belgrade, Serbia (2015):45-45,
https://hdl.handle.net/21.15107/rcub_dais_837 .

TY  - JOUR
AU  - Nenadović, Snežana S.
AU  - Kljajević, Ljiljana M.
AU  - Nenadović, Miloš
AU  - Mirković, Miljana M.
AU  - Marković, Smilja
AU  - Rakočević, Zlatko
PY  - 2015
UR  - https://dais.sanu.ac.rs/123456789/3356
AB  - In the present work, remediation of lead-containing solution using raw and modified kaolinite has been presented. The micro and nanostructure of samples has been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and atomic force microscopy (AFM). Laser diffraction and scattering (LDS), was analyzed by particle size analyzer based on laser diffraction and particle size distribution (PSD) was done. The degree of metal adsorption was evaluated analyzing the Pb(II) contaminated samples by inductively coupled plasma atomic emission spectrometry (micro- and nanostructure on immobilization efficiency correlCP AES). The results show the impact of immobilization efficiency and ation between micro- and nanostructure. The thermodynamic data (Delta HA degrees, Delta SA degrees, Delta GA degrees) are calculated from the temperature-dependent sorption isotherms. The results suggest sorption process of Pb(II) on kaolinite as spontaneous and endothermic.
T2  - Environmental Earth Sciences
T1  - Mechanochemical treatment and structural properties of lead adsorption on kaolinite (Rudovci, Serbia)
SP  - 7669
EP  - 7677
VL  - 73
IS  - 11
DO  - 10.1007/s12665-014-3941-y
UR  - https://hdl.handle.net/21.15107/rcub_dais_3356
ER  - 

@article{
author = "Nenadović, Snežana S. and Kljajević, Ljiljana M. and Nenadović, Miloš and Mirković, Miljana M. and Marković, Smilja and Rakočević, Zlatko",
year = "2015",
abstract = "In the present work, remediation of lead-containing solution using raw and modified kaolinite has been presented. The micro and nanostructure of samples has been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and atomic force microscopy (AFM). Laser diffraction and scattering (LDS), was analyzed by particle size analyzer based on laser diffraction and particle size distribution (PSD) was done. The degree of metal adsorption was evaluated analyzing the Pb(II) contaminated samples by inductively coupled plasma atomic emission spectrometry (micro- and nanostructure on immobilization efficiency correlCP AES). The results show the impact of immobilization efficiency and ation between micro- and nanostructure. The thermodynamic data (Delta HA degrees, Delta SA degrees, Delta GA degrees) are calculated from the temperature-dependent sorption isotherms. The results suggest sorption process of Pb(II) on kaolinite as spontaneous and endothermic.",
journal = "Environmental Earth Sciences",
title = "Mechanochemical treatment and structural properties of lead adsorption on kaolinite (Rudovci, Serbia)",
pages = "7669-7677",
volume = "73",
number = "11",
doi = "10.1007/s12665-014-3941-y",
url = "https://hdl.handle.net/21.15107/rcub_dais_3356"
}

Nenadović, S. S., Kljajević, L. M., Nenadović, M., Mirković, M. M., Marković, S.,& Rakočević, Z.. (2015). Mechanochemical treatment and structural properties of lead adsorption on kaolinite (Rudovci, Serbia). in Environmental Earth Sciences, 73(11), 7669-7677.
https://doi.org/10.1007/s12665-014-3941-y
https://hdl.handle.net/21.15107/rcub_dais_3356

Nenadović SS, Kljajević LM, Nenadović M, Mirković MM, Marković S, Rakočević Z. Mechanochemical treatment and structural properties of lead adsorption on kaolinite (Rudovci, Serbia). in Environmental Earth Sciences. 2015;73(11):7669-7677.
doi:10.1007/s12665-014-3941-y
https://hdl.handle.net/21.15107/rcub_dais_3356 .

Nenadović, Snežana S., Kljajević, Ljiljana M., Nenadović, Miloš, Mirković, Miljana M., Marković, Smilja, Rakočević, Zlatko, "Mechanochemical treatment and structural properties of lead adsorption on kaolinite (Rudovci, Serbia)" in Environmental Earth Sciences, 73, no. 11 (2015):7669-7677,
https://doi.org/10.1007/s12665-014-3941-y .,
https://hdl.handle.net/21.15107/rcub_dais_3356 .