Marinković, Zorica

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Authority KeyName Variants
orcid::0000-0002-1666-5758
  • Marinković, Zorica (9)
  • Marinković Stanojević, Zorica (7)
  • Marinković-Stanojević, Zorica (1)
Projects

Author's Bibliography

Structural, ferroelectric and magnetic properties of BiFeO3 synthesized by sonochemically assisted hydrothermal and hydro-evaporation chemical methods

Luković Golić, Danijela; Radojković, Aleksandar; Ćirković, Jovana; Dapčević, Aleksandra; Pajić, Damir; Tasić, Nikola B.; Savić, Slavica M.; Počuča Nešić, Milica; Marković, Smilja; Branković, Goran; Marinković Stanojević, Zorica; Branković, Zorica

(Elsevier, 2016)

TY  - JOUR
AU  - Luković Golić, Danijela
AU  - Radojković, Aleksandar
AU  - Ćirković, Jovana
AU  - Dapčević, Aleksandra
AU  - Pajić, Damir
AU  - Tasić, Nikola B.
AU  - Savić, Slavica M.
AU  - Počuča Nešić, Milica
AU  - Marković, Smilja
AU  - Branković, Goran
AU  - Marinković Stanojević, Zorica
AU  - Branković, Zorica
PY  - 2016
UR  - https://dais.sanu.ac.rs/123456789/2320
AB  - BiFeO3 powders were synthesized by sonochemically assisted hydrothermal and hydro-evaporation methods. The X-ray diffraction confirmed the presence of secondary phases, Bi25FeO39 and Bi2Fe4O9, in as prepared BiFeO3 powders. Optimization of sintering conditions indicated that temperature of 800 °C and time of 2 h after pressing at 9 t/cm2 provided ceramics samples with the highest density (up to 96% of theoretical density) and the lowest content of secondary phases. Ferroelectric and magnetic characterization was performed on two selected ceramics samples with the highest densities. Ceramics obtained from the powder synthesized by the hydrothermal method showed greater lattice distortion along [1 1 1] axis and smaller grains, which resulted in larger values of electric polarization at room temperature. It also exhibited less Fe(3d)–O(2p) orbital overlapping due to a larger FeOFe bond angle, causing lower antiferromagnetic ordering and weak ferromagnetic behavior at low temperatures.
PB  - Elsevier
T2  - Journal of the European Ceramic Society
T1  - Structural, ferroelectric and magnetic properties of BiFeO3 synthesized by sonochemically assisted hydrothermal and hydro-evaporation chemical methods
SP  - 1623
EP  - 1631
VL  - 36
IS  - 7
DO  - 10.1016/j.jeurceramsoc.2016.01.031
UR  - https://hdl.handle.net/21.15107/rcub_dais_2320
ER  - 
@article{
author = "Luković Golić, Danijela and Radojković, Aleksandar and Ćirković, Jovana and Dapčević, Aleksandra and Pajić, Damir and Tasić, Nikola B. and Savić, Slavica M. and Počuča Nešić, Milica and Marković, Smilja and Branković, Goran and Marinković Stanojević, Zorica and Branković, Zorica",
year = "2016",
abstract = "BiFeO3 powders were synthesized by sonochemically assisted hydrothermal and hydro-evaporation methods. The X-ray diffraction confirmed the presence of secondary phases, Bi25FeO39 and Bi2Fe4O9, in as prepared BiFeO3 powders. Optimization of sintering conditions indicated that temperature of 800 °C and time of 2 h after pressing at 9 t/cm2 provided ceramics samples with the highest density (up to 96% of theoretical density) and the lowest content of secondary phases. Ferroelectric and magnetic characterization was performed on two selected ceramics samples with the highest densities. Ceramics obtained from the powder synthesized by the hydrothermal method showed greater lattice distortion along [1 1 1] axis and smaller grains, which resulted in larger values of electric polarization at room temperature. It also exhibited less Fe(3d)–O(2p) orbital overlapping due to a larger FeOFe bond angle, causing lower antiferromagnetic ordering and weak ferromagnetic behavior at low temperatures.",
publisher = "Elsevier",
journal = "Journal of the European Ceramic Society",
title = "Structural, ferroelectric and magnetic properties of BiFeO3 synthesized by sonochemically assisted hydrothermal and hydro-evaporation chemical methods",
pages = "1623-1631",
volume = "36",
number = "7",
doi = "10.1016/j.jeurceramsoc.2016.01.031",
url = "https://hdl.handle.net/21.15107/rcub_dais_2320"
}
Luković Golić, D., Radojković, A., Ćirković, J., Dapčević, A., Pajić, D., Tasić, N. B., Savić, S. M., Počuča Nešić, M., Marković, S., Branković, G., Marinković Stanojević, Z.,& Branković, Z.. (2016). Structural, ferroelectric and magnetic properties of BiFeO3 synthesized by sonochemically assisted hydrothermal and hydro-evaporation chemical methods. in Journal of the European Ceramic Society
Elsevier., 36(7), 1623-1631.
https://doi.org/10.1016/j.jeurceramsoc.2016.01.031
https://hdl.handle.net/21.15107/rcub_dais_2320
Luković Golić D, Radojković A, Ćirković J, Dapčević A, Pajić D, Tasić NB, Savić SM, Počuča Nešić M, Marković S, Branković G, Marinković Stanojević Z, Branković Z. Structural, ferroelectric and magnetic properties of BiFeO3 synthesized by sonochemically assisted hydrothermal and hydro-evaporation chemical methods. in Journal of the European Ceramic Society. 2016;36(7):1623-1631.
doi:10.1016/j.jeurceramsoc.2016.01.031
https://hdl.handle.net/21.15107/rcub_dais_2320 .
Luković Golić, Danijela, Radojković, Aleksandar, Ćirković, Jovana, Dapčević, Aleksandra, Pajić, Damir, Tasić, Nikola B., Savić, Slavica M., Počuča Nešić, Milica, Marković, Smilja, Branković, Goran, Marinković Stanojević, Zorica, Branković, Zorica, "Structural, ferroelectric and magnetic properties of BiFeO3 synthesized by sonochemically assisted hydrothermal and hydro-evaporation chemical methods" in Journal of the European Ceramic Society, 36, no. 7 (2016):1623-1631,
https://doi.org/10.1016/j.jeurceramsoc.2016.01.031 .,
https://hdl.handle.net/21.15107/rcub_dais_2320 .
24
21
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Mechanochemical synthesis of bismuth ferrite

Marinković Stanojević, Zorica; Mančić, Lidija; Srećković, Tatjana; Stojanović, B.

(Technical Faculty - Copper Institute, Bor, 2013)

TY  - JOUR
AU  - Marinković Stanojević, Zorica
AU  - Mančić, Lidija
AU  - Srećković, Tatjana
AU  - Stojanović, B.
PY  - 2013
UR  - https://dais.sanu.ac.rs/123456789/363
AB  - A powder mixture of Bi2O3 and Fe2O3 was mechanically treated in a planetary ball mill in an air from 30 to 720 minutes. It was shown that the mechanochemical formation of BiFeO3 (BFO) phase was initiated after 60 min and its amount increased gradually with increasing milling time. A detailed XRPD structural analysis is realized by Rietveld’s structure refinement method. The resulting lattice parameters, relative phase abundances, crystallite sizes and crystal lattice microstrains were determined as a function of milling time. Microstructural analysis showed a little difference in morphology of obtained powders. The primary particles, irregular in shape and smaller than 400 nm are observed clearly, although they have assembled together to form agglomerates with varying size and morphology. Dense BFO ceramics were prepared by conventional solid-state reaction at the temperature of 810ºC for 1h followed immediately by quenching process. [Projekat Ministarstva nauke Republike Srbije, br. III45007: Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing
PB  - Technical Faculty - Copper Institute, Bor
T2  - Journal of Mining and Metallurgy, Section B: Metallurgy
T1  - Mechanochemical synthesis of bismuth ferrite
SP  - 27
EP  - 31
VL  - 49
IS  - 1
DO  - 10.2298/JMMB120430039M
UR  - https://hdl.handle.net/21.15107/rcub_dais_363
ER  - 
@article{
author = "Marinković Stanojević, Zorica and Mančić, Lidija and Srećković, Tatjana and Stojanović, B.",
year = "2013",
abstract = "A powder mixture of Bi2O3 and Fe2O3 was mechanically treated in a planetary ball mill in an air from 30 to 720 minutes. It was shown that the mechanochemical formation of BiFeO3 (BFO) phase was initiated after 60 min and its amount increased gradually with increasing milling time. A detailed XRPD structural analysis is realized by Rietveld’s structure refinement method. The resulting lattice parameters, relative phase abundances, crystallite sizes and crystal lattice microstrains were determined as a function of milling time. Microstructural analysis showed a little difference in morphology of obtained powders. The primary particles, irregular in shape and smaller than 400 nm are observed clearly, although they have assembled together to form agglomerates with varying size and morphology. Dense BFO ceramics were prepared by conventional solid-state reaction at the temperature of 810ºC for 1h followed immediately by quenching process. [Projekat Ministarstva nauke Republike Srbije, br. III45007: Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing",
publisher = "Technical Faculty - Copper Institute, Bor",
journal = "Journal of Mining and Metallurgy, Section B: Metallurgy",
title = "Mechanochemical synthesis of bismuth ferrite",
pages = "27-31",
volume = "49",
number = "1",
doi = "10.2298/JMMB120430039M",
url = "https://hdl.handle.net/21.15107/rcub_dais_363"
}
Marinković Stanojević, Z., Mančić, L., Srećković, T.,& Stojanović, B.. (2013). Mechanochemical synthesis of bismuth ferrite. in Journal of Mining and Metallurgy, Section B: Metallurgy
Technical Faculty - Copper Institute, Bor., 49(1), 27-31.
https://doi.org/10.2298/JMMB120430039M
https://hdl.handle.net/21.15107/rcub_dais_363
Marinković Stanojević Z, Mančić L, Srećković T, Stojanović B. Mechanochemical synthesis of bismuth ferrite. in Journal of Mining and Metallurgy, Section B: Metallurgy. 2013;49(1):27-31.
doi:10.2298/JMMB120430039M
https://hdl.handle.net/21.15107/rcub_dais_363 .
Marinković Stanojević, Zorica, Mančić, Lidija, Srećković, Tatjana, Stojanović, B., "Mechanochemical synthesis of bismuth ferrite" in Journal of Mining and Metallurgy, Section B: Metallurgy, 49, no. 1 (2013):27-31,
https://doi.org/10.2298/JMMB120430039M .,
https://hdl.handle.net/21.15107/rcub_dais_363 .
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Nanostructured Fe2O3/TiO2 thick films prepared by screen printing

Aleksić, Obrad S.; Đurić, Zorka Ž.; Nikolić, Maria Vesna; Tasić, Nikola B.; Vuković, Marina; Marinković Stanojević, Zorica; Nikolić, Nenad; Nikolić, Pantelija M.

(Novi Sad : University of Novi Sad, Faculty of Technology, 2013)

TY  - JOUR
AU  - Aleksić, Obrad S.
AU  - Đurić, Zorka Ž.
AU  - Nikolić, Maria Vesna
AU  - Tasić, Nikola B.
AU  - Vuković, Marina
AU  - Marinković Stanojević, Zorica
AU  - Nikolić, Nenad
AU  - Nikolić, Pantelija M.
PY  - 2013
UR  - https://dais.sanu.ac.rs/123456789/368
AB  - Nanostructured single layered (pure TiO2 , pure α-Fe2O3 and mixed Fe2O3 /TiO2 with two different oxide ratios, 2 : 3 and 3 : 2) and double layered (TiO2 layer over a Fe2O3 layer) thick films have been fabricated by screen printing technology on a glass substrate. The pastes used for film preparation were obtained by adding an organic vehicle to the oxide powders together with a small percentage of binding glass frit. Samples were dried up to 100 °C and sintered at 650 °C/60 minutes. Structural, morphological and optical studies have been carried out using XRD, SEM analyses and UV/Vis spectroscopy. The prepared pure and mixed Fe2O3 /TiO2 thick films had a homogenous nanostructure without secondary phases. Indirect band gaps were determined from the measured transmission spectra and the obtained values are in the range of literature data. [Projekat Ministarstva nauke Republike Srbije, br. III45007]
PB  - Novi Sad : University of Novi Sad, Faculty of Technology
T2  - Processing and Application of Ceramics
T1  - Nanostructured Fe2O3/TiO2 thick films prepared by screen printing
SP  - 129
EP  - 134
VL  - 7
IS  - 3
DO  - 10.2298/PAC1303129A
UR  - https://hdl.handle.net/21.15107/rcub_dais_368
ER  - 
@article{
author = "Aleksić, Obrad S. and Đurić, Zorka Ž. and Nikolić, Maria Vesna and Tasić, Nikola B. and Vuković, Marina and Marinković Stanojević, Zorica and Nikolić, Nenad and Nikolić, Pantelija M.",
year = "2013",
abstract = "Nanostructured single layered (pure TiO2 , pure α-Fe2O3 and mixed Fe2O3 /TiO2 with two different oxide ratios, 2 : 3 and 3 : 2) and double layered (TiO2 layer over a Fe2O3 layer) thick films have been fabricated by screen printing technology on a glass substrate. The pastes used for film preparation were obtained by adding an organic vehicle to the oxide powders together with a small percentage of binding glass frit. Samples were dried up to 100 °C and sintered at 650 °C/60 minutes. Structural, morphological and optical studies have been carried out using XRD, SEM analyses and UV/Vis spectroscopy. The prepared pure and mixed Fe2O3 /TiO2 thick films had a homogenous nanostructure without secondary phases. Indirect band gaps were determined from the measured transmission spectra and the obtained values are in the range of literature data. [Projekat Ministarstva nauke Republike Srbije, br. III45007]",
publisher = "Novi Sad : University of Novi Sad, Faculty of Technology",
journal = "Processing and Application of Ceramics",
title = "Nanostructured Fe2O3/TiO2 thick films prepared by screen printing",
pages = "129-134",
volume = "7",
number = "3",
doi = "10.2298/PAC1303129A",
url = "https://hdl.handle.net/21.15107/rcub_dais_368"
}
Aleksić, O. S., Đurić, Z. Ž., Nikolić, M. V., Tasić, N. B., Vuković, M., Marinković Stanojević, Z., Nikolić, N.,& Nikolić, P. M.. (2013). Nanostructured Fe2O3/TiO2 thick films prepared by screen printing. in Processing and Application of Ceramics
Novi Sad : University of Novi Sad, Faculty of Technology., 7(3), 129-134.
https://doi.org/10.2298/PAC1303129A
https://hdl.handle.net/21.15107/rcub_dais_368
Aleksić OS, Đurić ZŽ, Nikolić MV, Tasić NB, Vuković M, Marinković Stanojević Z, Nikolić N, Nikolić PM. Nanostructured Fe2O3/TiO2 thick films prepared by screen printing. in Processing and Application of Ceramics. 2013;7(3):129-134.
doi:10.2298/PAC1303129A
https://hdl.handle.net/21.15107/rcub_dais_368 .
Aleksić, Obrad S., Đurić, Zorka Ž., Nikolić, Maria Vesna, Tasić, Nikola B., Vuković, Marina, Marinković Stanojević, Zorica, Nikolić, Nenad, Nikolić, Pantelija M., "Nanostructured Fe2O3/TiO2 thick films prepared by screen printing" in Processing and Application of Ceramics, 7, no. 3 (2013):129-134,
https://doi.org/10.2298/PAC1303129A .,
https://hdl.handle.net/21.15107/rcub_dais_368 .

Mechanochemical Synthesis of Nanocrystalline Multiferroics Based on Bismuth Manganite

Marinković Stanojević, Zorica; Mančić, Lidija; Jagodič, Marko; Jagličić, Zvonko; Rečnik, Aleksander; Branković, Zorica; Branković, Goran

(Belgrade : Serbian Ceramic Society, 2012)

TY  - CONF
AU  - Marinković Stanojević, Zorica
AU  - Mančić, Lidija
AU  - Jagodič, Marko
AU  - Jagličić, Zvonko
AU  - Rečnik, Aleksander
AU  - Branković, Zorica
AU  - Branković, Goran
PY  - 2012
UR  - https://dais.sanu.ac.rs/123456789/515
AB  - Multiferroic materials simultaneously possess two or more ferroic orders, and enable a coupling interaction between them. Multiferroic bismuth manganite is known as a material that exhibits both ferromagnetic and ferroelectric properties making it interesting for various technological applications. Unfortunately, preparation of BiMnO3 is not possible by conventional solid state reaction and BiMnO3 has been synthesized from the mixture of oxides only at high pressures (>40 kbar). The aim of this work was to synthesize BiMnO3 (BMO) without additional heating or application of high pressures. Nanocrystalline single-phased BMnO3 was prepared for the first time by mechanochemical synthesis directly from the highly activated constituent oxides, Bi2O3 and Mn2O3, in a planetary ball mill. The obtained materials were characterized by X-ray diffraction, SEM with EDS analysis, HRTEM and magnetization measurements. All the samples were found to be tetragonal perovskite with P4mm crystallographic group. The broad maxima reflections of BMO samples can be ascribed to an amorphous/disordered phase. HRTEM micrographs give clear evidence of core-shell structure with amorphous shell around the nanocrystalline BMO particles. The magnetic hysteresis behavior is similar to that of a soft ferromagnet. The magnetic properties of the obtained BMO powders were found to change as a function of milling time in a manner consistent with the variation in the nanocomposite microstructure.
PB  - Belgrade : Serbian Ceramic Society
C3  - The First Serbian Ceramic Society Conference "Advanced Ceramics and Application" May 10-11, 2012: Program and the Book of Abstracts
T1  - Mechanochemical Synthesis of Nanocrystalline Multiferroics Based on Bismuth Manganite
SP  - 15
EP  - 15
UR  - https://hdl.handle.net/21.15107/rcub_dais_515
ER  - 
@conference{
author = "Marinković Stanojević, Zorica and Mančić, Lidija and Jagodič, Marko and Jagličić, Zvonko and Rečnik, Aleksander and Branković, Zorica and Branković, Goran",
year = "2012",
abstract = "Multiferroic materials simultaneously possess two or more ferroic orders, and enable a coupling interaction between them. Multiferroic bismuth manganite is known as a material that exhibits both ferromagnetic and ferroelectric properties making it interesting for various technological applications. Unfortunately, preparation of BiMnO3 is not possible by conventional solid state reaction and BiMnO3 has been synthesized from the mixture of oxides only at high pressures (>40 kbar). The aim of this work was to synthesize BiMnO3 (BMO) without additional heating or application of high pressures. Nanocrystalline single-phased BMnO3 was prepared for the first time by mechanochemical synthesis directly from the highly activated constituent oxides, Bi2O3 and Mn2O3, in a planetary ball mill. The obtained materials were characterized by X-ray diffraction, SEM with EDS analysis, HRTEM and magnetization measurements. All the samples were found to be tetragonal perovskite with P4mm crystallographic group. The broad maxima reflections of BMO samples can be ascribed to an amorphous/disordered phase. HRTEM micrographs give clear evidence of core-shell structure with amorphous shell around the nanocrystalline BMO particles. The magnetic hysteresis behavior is similar to that of a soft ferromagnet. The magnetic properties of the obtained BMO powders were found to change as a function of milling time in a manner consistent with the variation in the nanocomposite microstructure.",
publisher = "Belgrade : Serbian Ceramic Society",
journal = "The First Serbian Ceramic Society Conference "Advanced Ceramics and Application" May 10-11, 2012: Program and the Book of Abstracts",
title = "Mechanochemical Synthesis of Nanocrystalline Multiferroics Based on Bismuth Manganite",
pages = "15-15",
url = "https://hdl.handle.net/21.15107/rcub_dais_515"
}
Marinković Stanojević, Z., Mančić, L., Jagodič, M., Jagličić, Z., Rečnik, A., Branković, Z.,& Branković, G.. (2012). Mechanochemical Synthesis of Nanocrystalline Multiferroics Based on Bismuth Manganite. in The First Serbian Ceramic Society Conference "Advanced Ceramics and Application" May 10-11, 2012: Program and the Book of Abstracts
Belgrade : Serbian Ceramic Society., 15-15.
https://hdl.handle.net/21.15107/rcub_dais_515
Marinković Stanojević Z, Mančić L, Jagodič M, Jagličić Z, Rečnik A, Branković Z, Branković G. Mechanochemical Synthesis of Nanocrystalline Multiferroics Based on Bismuth Manganite. in The First Serbian Ceramic Society Conference "Advanced Ceramics and Application" May 10-11, 2012: Program and the Book of Abstracts. 2012;:15-15.
https://hdl.handle.net/21.15107/rcub_dais_515 .
Marinković Stanojević, Zorica, Mančić, Lidija, Jagodič, Marko, Jagličić, Zvonko, Rečnik, Aleksander, Branković, Zorica, Branković, Goran, "Mechanochemical Synthesis of Nanocrystalline Multiferroics Based on Bismuth Manganite" in The First Serbian Ceramic Society Conference "Advanced Ceramics and Application" May 10-11, 2012: Program and the Book of Abstracts (2012):15-15,
https://hdl.handle.net/21.15107/rcub_dais_515 .

Structural and magnetic properties of nanocrystalline bismuth manganite obtained by mechanochemical synthesis

Marinković Stanojević, Zorica; Branković, Zorica; Jagličić, Zvonko; Jagodič, Marko; Mančić, Lidija; Bernik, Slavko; Rečnik, A.; Branković, Goran

(Springer Netherlands, 2011)

TY  - JOUR
AU  - Marinković Stanojević, Zorica
AU  - Branković, Zorica
AU  - Jagličić, Zvonko
AU  - Jagodič, Marko
AU  - Mančić, Lidija
AU  - Bernik, Slavko
AU  - Rečnik, A.
AU  - Branković, Goran
PY  - 2011
UR  - https://dais.sanu.ac.rs/123456789/712
AB  - We have studied the formation of BiMnO3 (BMO) nanocrystalline perovskite powder produced by high-energy milling of the constituent oxides. The crystal structure and the amount of crystalline and amorphous phases in the powder as a function of the milling time were determined with XRPD using Rietveld refinement. BMO perovskite formed directly from highly activated nano-sized constituent oxides after 240 min of milling and subsequently grew during prolonged milling. The morphology, structure, and chemical composition of the powder were investigated by SEM and TEM. A clear ferromagnetic transition was observed at T C ~66 K for a sample milled for 240 min and increased with milling time. The magnetic hysteresis behavior is similar to that of a soft ferromagnet. The magnetic properties of the obtained BMO powders were found to change as a function of milling time in a manner consistent with variations in the nanocomposite microstructure.
PB  - Springer Netherlands
T2  - Journal of Nanoparticle Research
T1  - Structural and magnetic properties of nanocrystalline bismuth manganite obtained by mechanochemical synthesis
SP  - 3431
EP  - 3439
VL  - 13
IS  - 8
DO  - 10.1007/s11051-011-0265-7
UR  - https://hdl.handle.net/21.15107/rcub_dais_712
ER  - 
@article{
author = "Marinković Stanojević, Zorica and Branković, Zorica and Jagličić, Zvonko and Jagodič, Marko and Mančić, Lidija and Bernik, Slavko and Rečnik, A. and Branković, Goran",
year = "2011",
abstract = "We have studied the formation of BiMnO3 (BMO) nanocrystalline perovskite powder produced by high-energy milling of the constituent oxides. The crystal structure and the amount of crystalline and amorphous phases in the powder as a function of the milling time were determined with XRPD using Rietveld refinement. BMO perovskite formed directly from highly activated nano-sized constituent oxides after 240 min of milling and subsequently grew during prolonged milling. The morphology, structure, and chemical composition of the powder were investigated by SEM and TEM. A clear ferromagnetic transition was observed at T C ~66 K for a sample milled for 240 min and increased with milling time. The magnetic hysteresis behavior is similar to that of a soft ferromagnet. The magnetic properties of the obtained BMO powders were found to change as a function of milling time in a manner consistent with variations in the nanocomposite microstructure.",
publisher = "Springer Netherlands",
journal = "Journal of Nanoparticle Research",
title = "Structural and magnetic properties of nanocrystalline bismuth manganite obtained by mechanochemical synthesis",
pages = "3431-3439",
volume = "13",
number = "8",
doi = "10.1007/s11051-011-0265-7",
url = "https://hdl.handle.net/21.15107/rcub_dais_712"
}
Marinković Stanojević, Z., Branković, Z., Jagličić, Z., Jagodič, M., Mančić, L., Bernik, S., Rečnik, A.,& Branković, G.. (2011). Structural and magnetic properties of nanocrystalline bismuth manganite obtained by mechanochemical synthesis. in Journal of Nanoparticle Research
Springer Netherlands., 13(8), 3431-3439.
https://doi.org/10.1007/s11051-011-0265-7
https://hdl.handle.net/21.15107/rcub_dais_712
Marinković Stanojević Z, Branković Z, Jagličić Z, Jagodič M, Mančić L, Bernik S, Rečnik A, Branković G. Structural and magnetic properties of nanocrystalline bismuth manganite obtained by mechanochemical synthesis. in Journal of Nanoparticle Research. 2011;13(8):3431-3439.
doi:10.1007/s11051-011-0265-7
https://hdl.handle.net/21.15107/rcub_dais_712 .
Marinković Stanojević, Zorica, Branković, Zorica, Jagličić, Zvonko, Jagodič, Marko, Mančić, Lidija, Bernik, Slavko, Rečnik, A., Branković, Goran, "Structural and magnetic properties of nanocrystalline bismuth manganite obtained by mechanochemical synthesis" in Journal of Nanoparticle Research, 13, no. 8 (2011):3431-3439,
https://doi.org/10.1007/s11051-011-0265-7 .,
https://hdl.handle.net/21.15107/rcub_dais_712 .
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Mechanochemical synthesis of multiferroic yttrium manganite

Marinković Stanojević, Zorica; Počuča Nešić, Milica; Branković, Zorica; Mančić, Lidija; Bernik, Slavko; Rečnik, A.; Branković, Goran

(Belgrade : Materials Research Society of Serbia, 2011)

TY  - CONF
AU  - Marinković Stanojević, Zorica
AU  - Počuča Nešić, Milica
AU  - Branković, Zorica
AU  - Mančić, Lidija
AU  - Bernik, Slavko
AU  - Rečnik, A.
AU  - Branković, Goran
PY  - 2011
UR  - https://dais.sanu.ac.rs/123456789/671
AB  - Multiferroic yttrium manganite (YMnO3) is known as a material that exhibits both ferromagnetic and ferroelectric properties making it interesting for various technological applications. In this work single-phased YMnO3 was prepared for the first time by mechanochemical synthesis in a planetary ball mill. The YMnO3 can be formed directly from the highly activated constituent oxides, Y2O3 and Mn2O3, after 60 min of milling time and subsequently grows during prolonged milling. The cumulative energy introduced into the system during milling for 60 min was 86 kJ/g. X-ray analysis indicates that the as-prepared samples crystallize majority with hexagonal (P63cm) and minorly with orthorhombic (Pnma) YMnO3 structure. The morphology, structure and chemical composition of the powder were investigated by SEM with EDS and TEM. The magnetic properties of the obtained YMnO3 powders were found to change as a function of milling time in a manner consistent with the variation in the nanocomposite microstructure.
PB  - Belgrade : Materials Research Society of Serbia
C3  - VII International Conference on Mechanochemistry and Mechanical Alloying INCOME 2011: Programme and the Book of Abstracts
T1  - Mechanochemical synthesis of multiferroic yttrium manganite
SP  - 83
EP  - 83
UR  - https://hdl.handle.net/21.15107/rcub_dais_671
ER  - 
@conference{
author = "Marinković Stanojević, Zorica and Počuča Nešić, Milica and Branković, Zorica and Mančić, Lidija and Bernik, Slavko and Rečnik, A. and Branković, Goran",
year = "2011",
abstract = "Multiferroic yttrium manganite (YMnO3) is known as a material that exhibits both ferromagnetic and ferroelectric properties making it interesting for various technological applications. In this work single-phased YMnO3 was prepared for the first time by mechanochemical synthesis in a planetary ball mill. The YMnO3 can be formed directly from the highly activated constituent oxides, Y2O3 and Mn2O3, after 60 min of milling time and subsequently grows during prolonged milling. The cumulative energy introduced into the system during milling for 60 min was 86 kJ/g. X-ray analysis indicates that the as-prepared samples crystallize majority with hexagonal (P63cm) and minorly with orthorhombic (Pnma) YMnO3 structure. The morphology, structure and chemical composition of the powder were investigated by SEM with EDS and TEM. The magnetic properties of the obtained YMnO3 powders were found to change as a function of milling time in a manner consistent with the variation in the nanocomposite microstructure.",
publisher = "Belgrade : Materials Research Society of Serbia",
journal = "VII International Conference on Mechanochemistry and Mechanical Alloying INCOME 2011: Programme and the Book of Abstracts",
title = "Mechanochemical synthesis of multiferroic yttrium manganite",
pages = "83-83",
url = "https://hdl.handle.net/21.15107/rcub_dais_671"
}
Marinković Stanojević, Z., Počuča Nešić, M., Branković, Z., Mančić, L., Bernik, S., Rečnik, A.,& Branković, G.. (2011). Mechanochemical synthesis of multiferroic yttrium manganite. in VII International Conference on Mechanochemistry and Mechanical Alloying INCOME 2011: Programme and the Book of Abstracts
Belgrade : Materials Research Society of Serbia., 83-83.
https://hdl.handle.net/21.15107/rcub_dais_671
Marinković Stanojević Z, Počuča Nešić M, Branković Z, Mančić L, Bernik S, Rečnik A, Branković G. Mechanochemical synthesis of multiferroic yttrium manganite. in VII International Conference on Mechanochemistry and Mechanical Alloying INCOME 2011: Programme and the Book of Abstracts. 2011;:83-83.
https://hdl.handle.net/21.15107/rcub_dais_671 .
Marinković Stanojević, Zorica, Počuča Nešić, Milica, Branković, Zorica, Mančić, Lidija, Bernik, Slavko, Rečnik, A., Branković, Goran, "Mechanochemical synthesis of multiferroic yttrium manganite" in VII International Conference on Mechanochemistry and Mechanical Alloying INCOME 2011: Programme and the Book of Abstracts (2011):83-83,
https://hdl.handle.net/21.15107/rcub_dais_671 .

Synthesis of BaTiO3 from a mechanically activated BaCO 3-TiO2 system

Pavlović, Vera P.; Stojanović, B. D.; Pavlović, Vladimir B.; Marinković Stanojević, Zorica; Živković, Ljiljana; Ristic, Momčilo M.

(Belgrade : International Institute for the Science of Sintering, 2008)

TY  - JOUR
AU  - Pavlović, Vera P.
AU  - Stojanović, B. D.
AU  - Pavlović, Vladimir B.
AU  - Marinković Stanojević, Zorica
AU  - Živković, Ljiljana
AU  - Ristic, Momčilo M.
PY  - 2008
UR  - https://dais.sanu.ac.rs/123456789/3561
AB  - In this article the solid state reaction of BaTiO3 formation from a mechanically activated BaCO3-TiO2 system has been investigated. An equimolar mixture of BaCO3 and TiO2 powders was activated in a planetary ball mill in a continual regime for 0, 30 and 90 min, pressed and thermally treated up to 1200°C. The efect of the milling and firing regime on the phase formation was investigated by the X-ray diffraction (XRD) method and differential thermal analysis (DTA). Deconvolution of the experimental DTA curve corresponding to the BaTiO3 synthesis process has been performed. The influence of the activation time on the change of characteristic temperature for each elementary step in the complete solid-state reaction of BaTiO3 formation, was analyzed. These results were correlated with the ones obtained by SEM characterization and by XRD analysis.
PB  - Belgrade : International Institute for the Science of Sintering
T2  - Science of Sintering
T1  - Synthesis of BaTiO3 from a mechanically activated BaCO 3-TiO2 system
SP  - 21
EP  - 26
VL  - 40
IS  - 1
DO  - 10.2298/SOS0801021P
UR  - https://hdl.handle.net/21.15107/rcub_dais_3561
ER  - 
@article{
author = "Pavlović, Vera P. and Stojanović, B. D. and Pavlović, Vladimir B. and Marinković Stanojević, Zorica and Živković, Ljiljana and Ristic, Momčilo M.",
year = "2008",
abstract = "In this article the solid state reaction of BaTiO3 formation from a mechanically activated BaCO3-TiO2 system has been investigated. An equimolar mixture of BaCO3 and TiO2 powders was activated in a planetary ball mill in a continual regime for 0, 30 and 90 min, pressed and thermally treated up to 1200°C. The efect of the milling and firing regime on the phase formation was investigated by the X-ray diffraction (XRD) method and differential thermal analysis (DTA). Deconvolution of the experimental DTA curve corresponding to the BaTiO3 synthesis process has been performed. The influence of the activation time on the change of characteristic temperature for each elementary step in the complete solid-state reaction of BaTiO3 formation, was analyzed. These results were correlated with the ones obtained by SEM characterization and by XRD analysis.",
publisher = "Belgrade : International Institute for the Science of Sintering",
journal = "Science of Sintering",
title = "Synthesis of BaTiO3 from a mechanically activated BaCO 3-TiO2 system",
pages = "21-26",
volume = "40",
number = "1",
doi = "10.2298/SOS0801021P",
url = "https://hdl.handle.net/21.15107/rcub_dais_3561"
}
Pavlović, V. P., Stojanović, B. D., Pavlović, V. B., Marinković Stanojević, Z., Živković, L.,& Ristic, M. M.. (2008). Synthesis of BaTiO3 from a mechanically activated BaCO 3-TiO2 system. in Science of Sintering
Belgrade : International Institute for the Science of Sintering., 40(1), 21-26.
https://doi.org/10.2298/SOS0801021P
https://hdl.handle.net/21.15107/rcub_dais_3561
Pavlović VP, Stojanović BD, Pavlović VB, Marinković Stanojević Z, Živković L, Ristic MM. Synthesis of BaTiO3 from a mechanically activated BaCO 3-TiO2 system. in Science of Sintering. 2008;40(1):21-26.
doi:10.2298/SOS0801021P
https://hdl.handle.net/21.15107/rcub_dais_3561 .
Pavlović, Vera P., Stojanović, B. D., Pavlović, Vladimir B., Marinković Stanojević, Zorica, Živković, Ljiljana, Ristic, Momčilo M., "Synthesis of BaTiO3 from a mechanically activated BaCO 3-TiO2 system" in Science of Sintering, 40, no. 1 (2008):21-26,
https://doi.org/10.2298/SOS0801021P .,
https://hdl.handle.net/21.15107/rcub_dais_3561 .
22
23

Phase evolution in Ce-doped yttrium-aluminum-based particles derived from aerosol

Mančić, Lidija; Del Rosario, Gilberte; Marinković-Stanojević, Zorica; Milošević, Olivera

(Oxford : Elsevier Sci, 2007)

TY  - JOUR
AU  - Mančić, Lidija
AU  - Del Rosario, Gilberte
AU  - Marinković-Stanojević, Zorica
AU  - Milošević, Olivera
PY  - 2007
UR  - https://dais.sanu.ac.rs/123456789/12890
AB  - The common nitrates precursor solution leading to the Y3Al5O12:Ce3+ (YAG:Ce) composition with 2 at.% of cerium, is ultrasonically atomised and introduced into the tubular flow reactor at 320 degrees C. Having in mind that extremely high heating rates and short residence time are associated with spray pyrolysis, the low temperature regime is used for aerosol decomposition for the production of segregation-free precursor powder that is additionally heated at 900 and 1000 degrees C (2-6h) for the purpose to determine the phase evolution. Formation of uniform and submicron-sized spherical particles with nano-clustered inner structure is proved by different analysing techniques (X-ray powder diffraction, scanning electron microscopy and energy dispersive spectroscopy). The effect of processing parameters and post-annealing treatment is discussed from the viewpoint of the targeted garnet phase formation.
PB  - Oxford : Elsevier Sci
T2  - Journal of the European Ceramic Society
T1  - Phase evolution in Ce-doped yttrium-aluminum-based particles derived from aerosol
SP  - 4329
EP  - 4332
VL  - 27
IS  - 13-15
DO  - 10.1016/j.jeurceramsoc.2007.02.153
UR  - https://hdl.handle.net/21.15107/rcub_dais_12890
ER  - 
@article{
author = "Mančić, Lidija and Del Rosario, Gilberte and Marinković-Stanojević, Zorica and Milošević, Olivera",
year = "2007",
abstract = "The common nitrates precursor solution leading to the Y3Al5O12:Ce3+ (YAG:Ce) composition with 2 at.% of cerium, is ultrasonically atomised and introduced into the tubular flow reactor at 320 degrees C. Having in mind that extremely high heating rates and short residence time are associated with spray pyrolysis, the low temperature regime is used for aerosol decomposition for the production of segregation-free precursor powder that is additionally heated at 900 and 1000 degrees C (2-6h) for the purpose to determine the phase evolution. Formation of uniform and submicron-sized spherical particles with nano-clustered inner structure is proved by different analysing techniques (X-ray powder diffraction, scanning electron microscopy and energy dispersive spectroscopy). The effect of processing parameters and post-annealing treatment is discussed from the viewpoint of the targeted garnet phase formation.",
publisher = "Oxford : Elsevier Sci",
journal = "Journal of the European Ceramic Society",
title = "Phase evolution in Ce-doped yttrium-aluminum-based particles derived from aerosol",
pages = "4329-4332",
volume = "27",
number = "13-15",
doi = "10.1016/j.jeurceramsoc.2007.02.153",
url = "https://hdl.handle.net/21.15107/rcub_dais_12890"
}
Mančić, L., Del Rosario, G., Marinković-Stanojević, Z.,& Milošević, O.. (2007). Phase evolution in Ce-doped yttrium-aluminum-based particles derived from aerosol. in Journal of the European Ceramic Society
Oxford : Elsevier Sci., 27(13-15), 4329-4332.
https://doi.org/10.1016/j.jeurceramsoc.2007.02.153
https://hdl.handle.net/21.15107/rcub_dais_12890
Mančić L, Del Rosario G, Marinković-Stanojević Z, Milošević O. Phase evolution in Ce-doped yttrium-aluminum-based particles derived from aerosol. in Journal of the European Ceramic Society. 2007;27(13-15):4329-4332.
doi:10.1016/j.jeurceramsoc.2007.02.153
https://hdl.handle.net/21.15107/rcub_dais_12890 .
Mančić, Lidija, Del Rosario, Gilberte, Marinković-Stanojević, Zorica, Milošević, Olivera, "Phase evolution in Ce-doped yttrium-aluminum-based particles derived from aerosol" in Journal of the European Ceramic Society, 27, no. 13-15 (2007):4329-4332,
https://doi.org/10.1016/j.jeurceramsoc.2007.02.153 .,
https://hdl.handle.net/21.15107/rcub_dais_12890 .
14
11
17

Fine nanophased ZnO:Ru and ZnO:Pt powder synthesis through aerosols

Mančić, Lidija; Grgurić-Šipka, Sanja; Đinović, V. M.; Marinković, Zorica; Sabo, Tibor; Milošević, Olivera

(Zurich-Uetikon : Trans Tech Publications Ltd., 2005)

TY  - JOUR
AU  - Mančić, Lidija
AU  - Grgurić-Šipka, Sanja
AU  - Đinović, V. M.
AU  - Marinković, Zorica
AU  - Sabo, Tibor
AU  - Milošević, Olivera
PY  - 2005
UR  - https://dais.sanu.ac.rs/123456789/14740
AB  - Pt/Ru-doped ZnO nanophase particles were synthesized using ultrasonic spray pyrolysis. Particles were obtained through decomposition of zinc nitrate and newly developed Pt(IV) and Ru(III) complexes. The particle morphology, phase composition and chemical structure were revealed in accordance to various analysis methods (XRD, DSC, SEWEDS, TEM) and discussed in terms of precursor chemistry and process parameters. The shape of DSC curves, indicating two exothermic effects above 600 degrees C in both ZnO:Ru and ZnO:Pt, gave an indication of irreversible structural changes and high reactivity of as-prepared powders. The hexagonal wurtzite-type ZnO phase was revealed in both powdered samples. Small content of an intermediate Zn-5(NO3)(2)(OH)(8)(.)2H(2)O and cubic Zn2PtO4 phase were detected in the Pt-doped ZnO particles. Structural refinements, performed by Koalariet-XFit, suggest the composite internal particle structure composed of primary particles sized less than 100 nm. The estimated values for the unit cell parameters and Zn-O bond lengths imply noble metal ions incorporation into ZnO matrix interstitially, probably in octahedral interstitial environment. It has been shown that different particle growing morphologies (either spheroidally or pyramidally shaped) were influenced by the precursor chemistry, processing parameters and the presence of noble metal ions. Among the many parameters, attaining of the particle shape uniformity and homogeneous distribution of the noble metal cations in as-prepared particles are regarded as the most important factors for dominating microstructure evolution.
PB  - Zurich-Uetikon : Trans Tech Publications Ltd.
T2  - Materials Science Forum
T1  - Fine nanophased ZnO:Ru and ZnO:Pt powder synthesis through aerosols
SP  - 149
EP  - 154
VL  - 494
DO  - 10.4028/0-87849-971-7.149
UR  - https://hdl.handle.net/21.15107/rcub_dais_14740
ER  - 
@article{
author = "Mančić, Lidija and Grgurić-Šipka, Sanja and Đinović, V. M. and Marinković, Zorica and Sabo, Tibor and Milošević, Olivera",
year = "2005",
abstract = "Pt/Ru-doped ZnO nanophase particles were synthesized using ultrasonic spray pyrolysis. Particles were obtained through decomposition of zinc nitrate and newly developed Pt(IV) and Ru(III) complexes. The particle morphology, phase composition and chemical structure were revealed in accordance to various analysis methods (XRD, DSC, SEWEDS, TEM) and discussed in terms of precursor chemistry and process parameters. The shape of DSC curves, indicating two exothermic effects above 600 degrees C in both ZnO:Ru and ZnO:Pt, gave an indication of irreversible structural changes and high reactivity of as-prepared powders. The hexagonal wurtzite-type ZnO phase was revealed in both powdered samples. Small content of an intermediate Zn-5(NO3)(2)(OH)(8)(.)2H(2)O and cubic Zn2PtO4 phase were detected in the Pt-doped ZnO particles. Structural refinements, performed by Koalariet-XFit, suggest the composite internal particle structure composed of primary particles sized less than 100 nm. The estimated values for the unit cell parameters and Zn-O bond lengths imply noble metal ions incorporation into ZnO matrix interstitially, probably in octahedral interstitial environment. It has been shown that different particle growing morphologies (either spheroidally or pyramidally shaped) were influenced by the precursor chemistry, processing parameters and the presence of noble metal ions. Among the many parameters, attaining of the particle shape uniformity and homogeneous distribution of the noble metal cations in as-prepared particles are regarded as the most important factors for dominating microstructure evolution.",
publisher = "Zurich-Uetikon : Trans Tech Publications Ltd.",
journal = "Materials Science Forum",
title = "Fine nanophased ZnO:Ru and ZnO:Pt powder synthesis through aerosols",
pages = "149-154",
volume = "494",
doi = "10.4028/0-87849-971-7.149",
url = "https://hdl.handle.net/21.15107/rcub_dais_14740"
}
Mančić, L., Grgurić-Šipka, S., Đinović, V. M., Marinković, Z., Sabo, T.,& Milošević, O.. (2005). Fine nanophased ZnO:Ru and ZnO:Pt powder synthesis through aerosols. in Materials Science Forum
Zurich-Uetikon : Trans Tech Publications Ltd.., 494, 149-154.
https://doi.org/10.4028/0-87849-971-7.149
https://hdl.handle.net/21.15107/rcub_dais_14740
Mančić L, Grgurić-Šipka S, Đinović VM, Marinković Z, Sabo T, Milošević O. Fine nanophased ZnO:Ru and ZnO:Pt powder synthesis through aerosols. in Materials Science Forum. 2005;494:149-154.
doi:10.4028/0-87849-971-7.149
https://hdl.handle.net/21.15107/rcub_dais_14740 .
Mančić, Lidija, Grgurić-Šipka, Sanja, Đinović, V. M., Marinković, Zorica, Sabo, Tibor, Milošević, Olivera, "Fine nanophased ZnO:Ru and ZnO:Pt powder synthesis through aerosols" in Materials Science Forum, 494 (2005):149-154,
https://doi.org/10.4028/0-87849-971-7.149 .,
https://hdl.handle.net/21.15107/rcub_dais_14740 .
3
3

Microstructural characterization of mechanically activated ZnO-Cr2O3 system

Marinković, Zorica; Mančić, Lidija; Vulić, Predrag J.; Milošević, Olivera

(Oxford : Elsevier Sci, 2005)

TY  - JOUR
AU  - Marinković, Zorica
AU  - Mančić, Lidija
AU  - Vulić, Predrag J.
AU  - Milošević, Olivera
PY  - 2005
UR  - https://dais.sanu.ac.rs/123456789/12882
AB  - An equimolar mixtures of starting ZnO and Cr2O3 powders were mechanically activated by grinding using a planetary ball mill for various periods of time (40-320min). Formation of nanocrystalline ZnCr2O4 as normal spine] structure at room temperature is detected in all samples-after ball-milling. A detailed XRD structural analysis (the relative phase abundances of different phases, lattice parameter changes, site occupancy, the average primary crystallite sizes, crystal lattice microstrains) is realized by the pattern decomposition technique, performed in accordance with the procedure based on Rietveld software KOALARIET-XFIT. Due to the importance of cation distribution on the chemical and physical properties of spinels, a study of site occupation factors of ZnCr2O4 spinels has been undertaken. The calculation based on the atomistic methods for the description of the perfect and defect spinel ZnCr2O4 crystal lattice is applied and the presence of the individual structural defects is determined.
PB  - Oxford : Elsevier Sci
T2  - Journal of the European Ceramic Society
T1  - Microstructural characterization of mechanically activated ZnO-Cr2O3 system
SP  - 2081
EP  - 2084
VL  - 25
IS  - 12
DO  - 10.1016/j.jeurceramsoc.2005.03.085
UR  - https://hdl.handle.net/21.15107/rcub_dais_12882
ER  - 
@article{
author = "Marinković, Zorica and Mančić, Lidija and Vulić, Predrag J. and Milošević, Olivera",
year = "2005",
abstract = "An equimolar mixtures of starting ZnO and Cr2O3 powders were mechanically activated by grinding using a planetary ball mill for various periods of time (40-320min). Formation of nanocrystalline ZnCr2O4 as normal spine] structure at room temperature is detected in all samples-after ball-milling. A detailed XRD structural analysis (the relative phase abundances of different phases, lattice parameter changes, site occupancy, the average primary crystallite sizes, crystal lattice microstrains) is realized by the pattern decomposition technique, performed in accordance with the procedure based on Rietveld software KOALARIET-XFIT. Due to the importance of cation distribution on the chemical and physical properties of spinels, a study of site occupation factors of ZnCr2O4 spinels has been undertaken. The calculation based on the atomistic methods for the description of the perfect and defect spinel ZnCr2O4 crystal lattice is applied and the presence of the individual structural defects is determined.",
publisher = "Oxford : Elsevier Sci",
journal = "Journal of the European Ceramic Society",
title = "Microstructural characterization of mechanically activated ZnO-Cr2O3 system",
pages = "2081-2084",
volume = "25",
number = "12",
doi = "10.1016/j.jeurceramsoc.2005.03.085",
url = "https://hdl.handle.net/21.15107/rcub_dais_12882"
}
Marinković, Z., Mančić, L., Vulić, P. J.,& Milošević, O.. (2005). Microstructural characterization of mechanically activated ZnO-Cr2O3 system. in Journal of the European Ceramic Society
Oxford : Elsevier Sci., 25(12), 2081-2084.
https://doi.org/10.1016/j.jeurceramsoc.2005.03.085
https://hdl.handle.net/21.15107/rcub_dais_12882
Marinković Z, Mančić L, Vulić PJ, Milošević O. Microstructural characterization of mechanically activated ZnO-Cr2O3 system. in Journal of the European Ceramic Society. 2005;25(12):2081-2084.
doi:10.1016/j.jeurceramsoc.2005.03.085
https://hdl.handle.net/21.15107/rcub_dais_12882 .
Marinković, Zorica, Mančić, Lidija, Vulić, Predrag J., Milošević, Olivera, "Microstructural characterization of mechanically activated ZnO-Cr2O3 system" in Journal of the European Ceramic Society, 25, no. 12 (2005):2081-2084,
https://doi.org/10.1016/j.jeurceramsoc.2005.03.085 .,
https://hdl.handle.net/21.15107/rcub_dais_12882 .
6
45
40
49

The synthesis - structure relationship in the ZnO-Cr2O3 system

Mančić, Lidija; Marinković, Zorica; Vulić, Predrag; Milošević, Olivera

(Belgrade : International Institute for the Science of Sintering, 2004)

TY  - JOUR
AU  - Mančić, Lidija
AU  - Marinković, Zorica
AU  - Vulić, Predrag
AU  - Milošević, Olivera
PY  - 2004
UR  - https://dais.sanu.ac.rs/123456789/229
AB  - In this work the development of the spinel phase in the ZnO-Cr2O3 system was discussed from the viewpoint of the synthesis-structure relationship. The nanostructure evolution in particles obtained either via solution-based (spray pyrolysis) or solid-state (mechanical activation) synthesis procedures were investigated by XRD analysis. A detailed structural analysis of the spinel phase lattice parameters, average primary crystallite sizes and micro strains were performed in accordance with a procedure based on the Koalariet-Xfit program. Due to the importance of spinel-phase cat ion distribution for chemical and physical properties, a study of the site occupation factors, i.e. changes in the stoichiometric, of ZnCr2O4 spinals was undertaken. The calculation based on atomistic methods for the description of both perfect and defect spinel ZnCr2O4 crystal lattices has been applied and the presence of individual structural defects was determined.
PB  - Belgrade : International Institute for the Science of Sintering
T2  - Science of Sintering
T1  - The synthesis - structure relationship in the ZnO-Cr2O3 system
SP  - 189
EP  - 196
VL  - 36
IS  - 3
DO  - 10.2298/SOS0403189M
UR  - https://hdl.handle.net/21.15107/rcub_dais_229
ER  - 
@article{
author = "Mančić, Lidija and Marinković, Zorica and Vulić, Predrag and Milošević, Olivera",
year = "2004",
abstract = "In this work the development of the spinel phase in the ZnO-Cr2O3 system was discussed from the viewpoint of the synthesis-structure relationship. The nanostructure evolution in particles obtained either via solution-based (spray pyrolysis) or solid-state (mechanical activation) synthesis procedures were investigated by XRD analysis. A detailed structural analysis of the spinel phase lattice parameters, average primary crystallite sizes and micro strains were performed in accordance with a procedure based on the Koalariet-Xfit program. Due to the importance of spinel-phase cat ion distribution for chemical and physical properties, a study of the site occupation factors, i.e. changes in the stoichiometric, of ZnCr2O4 spinals was undertaken. The calculation based on atomistic methods for the description of both perfect and defect spinel ZnCr2O4 crystal lattices has been applied and the presence of individual structural defects was determined.",
publisher = "Belgrade : International Institute for the Science of Sintering",
journal = "Science of Sintering",
title = "The synthesis - structure relationship in the ZnO-Cr2O3 system",
pages = "189-196",
volume = "36",
number = "3",
doi = "10.2298/SOS0403189M",
url = "https://hdl.handle.net/21.15107/rcub_dais_229"
}
Mančić, L., Marinković, Z., Vulić, P.,& Milošević, O.. (2004). The synthesis - structure relationship in the ZnO-Cr2O3 system. in Science of Sintering
Belgrade : International Institute for the Science of Sintering., 36(3), 189-196.
https://doi.org/10.2298/SOS0403189M
https://hdl.handle.net/21.15107/rcub_dais_229
Mančić L, Marinković Z, Vulić P, Milošević O. The synthesis - structure relationship in the ZnO-Cr2O3 system. in Science of Sintering. 2004;36(3):189-196.
doi:10.2298/SOS0403189M
https://hdl.handle.net/21.15107/rcub_dais_229 .
Mančić, Lidija, Marinković, Zorica, Vulić, Predrag, Milošević, Olivera, "The synthesis - structure relationship in the ZnO-Cr2O3 system" in Science of Sintering, 36, no. 3 (2004):189-196,
https://doi.org/10.2298/SOS0403189M .,
https://hdl.handle.net/21.15107/rcub_dais_229 .
7
4
7

The influence of grinding conditions on the mechanochemical synthesis of zinc stannate

Nikolić, Nataša; Marinković, Zorica; Srecković, Tatjana

(Springer, 2004)

TY  - JOUR
AU  - Nikolić, Nataša
AU  - Marinković, Zorica
AU  - Srecković, Tatjana
PY  - 2004
UR  - https://dais.sanu.ac.rs/123456789/14735
AB  - The aim of this work is the investigation of experimental conditions for mechanochemical synthesis of spinel zinc stannate (Zn2SnO4). Application of this material include manufacturing of CO, H2, NO, NO2, i-C4H10 and C2H5OH gas sensors, production of transparent conducting electrodes, window coatings and anode for use in photoelectrochemistry. Starting powder mixtures of zinc oxide and tin oxide in the molar ratio, in accordance with the stoichiometrics of spinel zinc stannate, were mechanically activated by grinding in a planetary mill for various periods of time in the interval of 0 to 160 min. Changes of physico-chemical characteristics and microstructural parameters in the ZnO-SnO2 system after grinding were followed using surface area analysis and X-ray powder diffraction, while thermal behavior was examined by differential thermal analysis and sensitive dilatometer. The beginning of zinc stannate phase formation was noticed after 40 min of grinding, and prolonged grinding leads to the formation of spinel zinc stannate as the major phase with insignificant amount of unreacted zinc oxide and tin oxide. The formation of spinel was accelerated with the increase of sintering temperature, and monophased zinc stannate was obtained when powder mixture was grinded for 160 min followed by sintering at 1200°C.
PB  - Springer
T2  - Journal of Materials Science
T1  - The influence of grinding conditions on the mechanochemical synthesis of zinc stannate
SP  - 5239
EP  - 5242
VL  - 39
IS  - 16/17
DO  - 10.1023/B:JMSC.0000039218.82254.a4
UR  - https://hdl.handle.net/21.15107/rcub_dais_14735
ER  - 
@article{
author = "Nikolić, Nataša and Marinković, Zorica and Srecković, Tatjana",
year = "2004",
abstract = "The aim of this work is the investigation of experimental conditions for mechanochemical synthesis of spinel zinc stannate (Zn2SnO4). Application of this material include manufacturing of CO, H2, NO, NO2, i-C4H10 and C2H5OH gas sensors, production of transparent conducting electrodes, window coatings and anode for use in photoelectrochemistry. Starting powder mixtures of zinc oxide and tin oxide in the molar ratio, in accordance with the stoichiometrics of spinel zinc stannate, were mechanically activated by grinding in a planetary mill for various periods of time in the interval of 0 to 160 min. Changes of physico-chemical characteristics and microstructural parameters in the ZnO-SnO2 system after grinding were followed using surface area analysis and X-ray powder diffraction, while thermal behavior was examined by differential thermal analysis and sensitive dilatometer. The beginning of zinc stannate phase formation was noticed after 40 min of grinding, and prolonged grinding leads to the formation of spinel zinc stannate as the major phase with insignificant amount of unreacted zinc oxide and tin oxide. The formation of spinel was accelerated with the increase of sintering temperature, and monophased zinc stannate was obtained when powder mixture was grinded for 160 min followed by sintering at 1200°C.",
publisher = "Springer",
journal = "Journal of Materials Science",
title = "The influence of grinding conditions on the mechanochemical synthesis of zinc stannate",
pages = "5239-5242",
volume = "39",
number = "16/17",
doi = "10.1023/B:JMSC.0000039218.82254.a4",
url = "https://hdl.handle.net/21.15107/rcub_dais_14735"
}
Nikolić, N., Marinković, Z.,& Srecković, T.. (2004). The influence of grinding conditions on the mechanochemical synthesis of zinc stannate. in Journal of Materials Science
Springer., 39(16/17), 5239-5242.
https://doi.org/10.1023/B:JMSC.0000039218.82254.a4
https://hdl.handle.net/21.15107/rcub_dais_14735
Nikolić N, Marinković Z, Srecković T. The influence of grinding conditions on the mechanochemical synthesis of zinc stannate. in Journal of Materials Science. 2004;39(16/17):5239-5242.
doi:10.1023/B:JMSC.0000039218.82254.a4
https://hdl.handle.net/21.15107/rcub_dais_14735 .
Nikolić, Nataša, Marinković, Zorica, Srecković, Tatjana, "The influence of grinding conditions on the mechanochemical synthesis of zinc stannate" in Journal of Materials Science, 39, no. 16/17 (2004):5239-5242,
https://doi.org/10.1023/B:JMSC.0000039218.82254.a4 .,
https://hdl.handle.net/21.15107/rcub_dais_14735 .
27
20
24

Evolution of the microstructure of disperse ZnO powders obtained by the freeze-drying method

Marinković, Zorica; Milošević, Olivera; Nikolić, Maria Vesna; Kakazey, M. G.; Karpec, M. V.; Tomila, T. V.; Ristić, Momčilo M.

(Lausanne : Elsevier Science, 2004)

TY  - JOUR
AU  - Marinković, Zorica
AU  - Milošević, Olivera
AU  - Nikolić, Maria Vesna
AU  - Kakazey, M. G.
AU  - Karpec, M. V.
AU  - Tomila, T. V.
AU  - Ristić, Momčilo M.
PY  - 2004
UR  - https://dais.sanu.ac.rs/123456789/12881
AB  - Freeze-drying, as a cryochemical powder processing method is applied in the synthesis of ZnO submicrometer to narrosized powders. The process involves rapid freezing of the sprayed precursor solution, drying under vacuum by sublimation of the Solvent and salt decomposition to oxide by thermal treatment. Calcination of dehydrated Zn(NO3)(2) was performed through destruction of the primary crystal structure, i.e. through accumulation of different defect complexes and based on this, the formation of a new state of the ZnO crystal lattice. An analysis of the microstructure evolution of zinc oxide particles in the temperature range from 548 to 898 K is described. The research was performed using differential scanning calorimetry (DSC), scanning electron microscopy (SEM), X-ray powder diffraction (XRPD), electronic paramagnetic resonance (EPR) and infrared spectroscopy (IR). It was shown that the least ("primary") coherent scattering region (580 Angstrom) and the most defective state were ZnO obtained at the lowest calcination temperature (T-c = 548 K). Increase of the calcination temperature (T-c > 548 K) favors uniting of eight closest "primary" domains into "secondary" ones. Unification is accompanied by a pronounced increase in microstrainin "secondary" domains, whose size practically does not depend on the calcination temperature in the region 573-898 K.
PB  - Lausanne : Elsevier Science
T2  - Materials Science and Engineering A-Structural Materials Properties Microstructure and Processing
T1  - Evolution of the microstructure of disperse ZnO powders obtained by the freeze-drying method
SP  - 620
EP  - 624
VL  - 375
DO  - 10.1016/j.msea.2003.10.113
UR  - https://hdl.handle.net/21.15107/rcub_dais_12881
ER  - 
@article{
author = "Marinković, Zorica and Milošević, Olivera and Nikolić, Maria Vesna and Kakazey, M. G. and Karpec, M. V. and Tomila, T. V. and Ristić, Momčilo M.",
year = "2004",
abstract = "Freeze-drying, as a cryochemical powder processing method is applied in the synthesis of ZnO submicrometer to narrosized powders. The process involves rapid freezing of the sprayed precursor solution, drying under vacuum by sublimation of the Solvent and salt decomposition to oxide by thermal treatment. Calcination of dehydrated Zn(NO3)(2) was performed through destruction of the primary crystal structure, i.e. through accumulation of different defect complexes and based on this, the formation of a new state of the ZnO crystal lattice. An analysis of the microstructure evolution of zinc oxide particles in the temperature range from 548 to 898 K is described. The research was performed using differential scanning calorimetry (DSC), scanning electron microscopy (SEM), X-ray powder diffraction (XRPD), electronic paramagnetic resonance (EPR) and infrared spectroscopy (IR). It was shown that the least ("primary") coherent scattering region (580 Angstrom) and the most defective state were ZnO obtained at the lowest calcination temperature (T-c = 548 K). Increase of the calcination temperature (T-c > 548 K) favors uniting of eight closest "primary" domains into "secondary" ones. Unification is accompanied by a pronounced increase in microstrainin "secondary" domains, whose size practically does not depend on the calcination temperature in the region 573-898 K.",
publisher = "Lausanne : Elsevier Science",
journal = "Materials Science and Engineering A-Structural Materials Properties Microstructure and Processing",
title = "Evolution of the microstructure of disperse ZnO powders obtained by the freeze-drying method",
pages = "620-624",
volume = "375",
doi = "10.1016/j.msea.2003.10.113",
url = "https://hdl.handle.net/21.15107/rcub_dais_12881"
}
Marinković, Z., Milošević, O., Nikolić, M. V., Kakazey, M. G., Karpec, M. V., Tomila, T. V.,& Ristić, M. M.. (2004). Evolution of the microstructure of disperse ZnO powders obtained by the freeze-drying method. in Materials Science and Engineering A-Structural Materials Properties Microstructure and Processing
Lausanne : Elsevier Science., 375, 620-624.
https://doi.org/10.1016/j.msea.2003.10.113
https://hdl.handle.net/21.15107/rcub_dais_12881
Marinković Z, Milošević O, Nikolić MV, Kakazey MG, Karpec MV, Tomila TV, Ristić MM. Evolution of the microstructure of disperse ZnO powders obtained by the freeze-drying method. in Materials Science and Engineering A-Structural Materials Properties Microstructure and Processing. 2004;375:620-624.
doi:10.1016/j.msea.2003.10.113
https://hdl.handle.net/21.15107/rcub_dais_12881 .
Marinković, Zorica, Milošević, Olivera, Nikolić, Maria Vesna, Kakazey, M. G., Karpec, M. V., Tomila, T. V., Ristić, Momčilo M., "Evolution of the microstructure of disperse ZnO powders obtained by the freeze-drying method" in Materials Science and Engineering A-Structural Materials Properties Microstructure and Processing, 375 (2004):620-624,
https://doi.org/10.1016/j.msea.2003.10.113 .,
https://hdl.handle.net/21.15107/rcub_dais_12881 .
13
17

The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions

Marinković, Zorica; Mančić, Lidija; Milošević, Olivera

(Oxford : Elsevier Sci, 2004)

TY  - JOUR
AU  - Marinković, Zorica
AU  - Mančić, Lidija
AU  - Milošević, Olivera
PY  - 2004
UR  - https://dais.sanu.ac.rs/123456789/12879
AB  - The nature of exothermal and irreversible structural changes observed during linear heating of nanocrystalline ZnO powders was investigated using differential scanning calorimetry, X ray, SEM and TEM analysis. Nanocrystalline ZnO powders were obtained by ultrasonic spray pyrolysis of 0.8 mol/dm(3) zinc nitrate solution and subsequent decomposition of 2.7 mum sized droplets in the temperature range up to 600 degreesC, F-air = 1.2 dm(3)/min. Produced particles are characterized by uniform and submicronic size, BET = 4.94 m(2)/g, high phase purity and granular or circular "open" surface as the consequence of primary crystallites presence with average size of d = 20 nm. The observed quasi nucleation-growth process during heating of this powder was discussed in the terms of primary crystallites structural changes.
PB  - Oxford : Elsevier Sci
T2  - Journal of the European Ceramic Society
T1  - The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions
SP  - 1929
EP  - 1933
VL  - 24
IS  - 6
DO  - 10.1016/S0955-2219(03)00523-5
UR  - https://hdl.handle.net/21.15107/rcub_dais_12879
ER  - 
@article{
author = "Marinković, Zorica and Mančić, Lidija and Milošević, Olivera",
year = "2004",
abstract = "The nature of exothermal and irreversible structural changes observed during linear heating of nanocrystalline ZnO powders was investigated using differential scanning calorimetry, X ray, SEM and TEM analysis. Nanocrystalline ZnO powders were obtained by ultrasonic spray pyrolysis of 0.8 mol/dm(3) zinc nitrate solution and subsequent decomposition of 2.7 mum sized droplets in the temperature range up to 600 degreesC, F-air = 1.2 dm(3)/min. Produced particles are characterized by uniform and submicronic size, BET = 4.94 m(2)/g, high phase purity and granular or circular "open" surface as the consequence of primary crystallites presence with average size of d = 20 nm. The observed quasi nucleation-growth process during heating of this powder was discussed in the terms of primary crystallites structural changes.",
publisher = "Oxford : Elsevier Sci",
journal = "Journal of the European Ceramic Society",
title = "The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions",
pages = "1929-1933",
volume = "24",
number = "6",
doi = "10.1016/S0955-2219(03)00523-5",
url = "https://hdl.handle.net/21.15107/rcub_dais_12879"
}
Marinković, Z., Mančić, L.,& Milošević, O.. (2004). The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions. in Journal of the European Ceramic Society
Oxford : Elsevier Sci., 24(6), 1929-1933.
https://doi.org/10.1016/S0955-2219(03)00523-5
https://hdl.handle.net/21.15107/rcub_dais_12879
Marinković Z, Mančić L, Milošević O. The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions. in Journal of the European Ceramic Society. 2004;24(6):1929-1933.
doi:10.1016/S0955-2219(03)00523-5
https://hdl.handle.net/21.15107/rcub_dais_12879 .
Marinković, Zorica, Mančić, Lidija, Milošević, Olivera, "The nature of structural changes in nanocrystalline ZnO powders under linear heating conditions" in Journal of the European Ceramic Society, 24, no. 6 (2004):1929-1933,
https://doi.org/10.1016/S0955-2219(03)00523-5 .,
https://hdl.handle.net/21.15107/rcub_dais_12879 .
15
15

Nature of structural changes in LSM-YSZ nanocomposite material during thermal treatments

Marinković, Zorica; Mančić, Lidija; Cribier, J. F.; Ohara, Satoshi; Fukui, T.; Milošević, Olivera

(Elsevier Science Sa, Lausanne, 2004)

TY  - JOUR
AU  - Marinković, Zorica
AU  - Mančić, Lidija
AU  - Cribier, J. F.
AU  - Ohara, Satoshi
AU  - Fukui, T.
AU  - Milošević, Olivera
PY  - 2004
UR  - https://dais.sanu.ac.rs/123456789/12878
AB  - Nanocomposite powders in the system (La1-xSx)(a)MnO3-YSZ((1-y)) [LSM-YSZ], as an attractive cathode material for high operating solid oxide fuel cell (SOFC), were obtained through ultrasonic spray pyrolysis (1.7 MHz) method. The principle of the synthesis is based on a single-step high temperature aerosol decomposition of atomized precursor solutions composed from yttria stabilized ZrO2 sol (average particle size similar to 60 nm) and corresponding aqueous nitrate and hydrogen peroxide solutions of La, Sr and Mn. Two starting systems were examined: (a) (La0.76Sr0.24)(0.93)MnO3 with 0% YSZ, and (b) (La0.77Sr0.23)(0.92)MnO3-YSZ(0.81) with corresponding molar ratio LSM/YSZ = 48:52. X-ray diffraction analysis of as-prepared powders showed the presence of a lanthanum magnesium oxide and yttrium zirconium oxide. Compositional homogeneity and particle morphology were determined by SEM analysis. LSM-YSZ obtained particles are spherical in shape, submicron in size and composed of primary subgrains. TEM analysis of ultra-cross section revealed dense-packed nanosized grains, several tens of nanometers in diameter. After powders calcination TEM observations confirmed dense particle structure composed of primary grains, with a mean diameter of around 100 nm. The structural changes expressed through the crystallite growth were analyzed by nonisothermal differential scanning calorimetry (DSC).
PB  - Elsevier Science Sa, Lausanne
T2  - Materials Science and Engineering A-Structural Materials Properties Microstructure and Processing
T1  - Nature of structural changes in LSM-YSZ nanocomposite material during thermal treatments
SP  - 615
EP  - 619
VL  - 375
DO  - 10.1016/j.msea.2003.10.270
UR  - https://hdl.handle.net/21.15107/rcub_dais_12878
ER  - 
@article{
author = "Marinković, Zorica and Mančić, Lidija and Cribier, J. F. and Ohara, Satoshi and Fukui, T. and Milošević, Olivera",
year = "2004",
abstract = "Nanocomposite powders in the system (La1-xSx)(a)MnO3-YSZ((1-y)) [LSM-YSZ], as an attractive cathode material for high operating solid oxide fuel cell (SOFC), were obtained through ultrasonic spray pyrolysis (1.7 MHz) method. The principle of the synthesis is based on a single-step high temperature aerosol decomposition of atomized precursor solutions composed from yttria stabilized ZrO2 sol (average particle size similar to 60 nm) and corresponding aqueous nitrate and hydrogen peroxide solutions of La, Sr and Mn. Two starting systems were examined: (a) (La0.76Sr0.24)(0.93)MnO3 with 0% YSZ, and (b) (La0.77Sr0.23)(0.92)MnO3-YSZ(0.81) with corresponding molar ratio LSM/YSZ = 48:52. X-ray diffraction analysis of as-prepared powders showed the presence of a lanthanum magnesium oxide and yttrium zirconium oxide. Compositional homogeneity and particle morphology were determined by SEM analysis. LSM-YSZ obtained particles are spherical in shape, submicron in size and composed of primary subgrains. TEM analysis of ultra-cross section revealed dense-packed nanosized grains, several tens of nanometers in diameter. After powders calcination TEM observations confirmed dense particle structure composed of primary grains, with a mean diameter of around 100 nm. The structural changes expressed through the crystallite growth were analyzed by nonisothermal differential scanning calorimetry (DSC).",
publisher = "Elsevier Science Sa, Lausanne",
journal = "Materials Science and Engineering A-Structural Materials Properties Microstructure and Processing",
title = "Nature of structural changes in LSM-YSZ nanocomposite material during thermal treatments",
pages = "615-619",
volume = "375",
doi = "10.1016/j.msea.2003.10.270",
url = "https://hdl.handle.net/21.15107/rcub_dais_12878"
}
Marinković, Z., Mančić, L., Cribier, J. F., Ohara, S., Fukui, T.,& Milošević, O.. (2004). Nature of structural changes in LSM-YSZ nanocomposite material during thermal treatments. in Materials Science and Engineering A-Structural Materials Properties Microstructure and Processing
Elsevier Science Sa, Lausanne., 375, 615-619.
https://doi.org/10.1016/j.msea.2003.10.270
https://hdl.handle.net/21.15107/rcub_dais_12878
Marinković Z, Mančić L, Cribier JF, Ohara S, Fukui T, Milošević O. Nature of structural changes in LSM-YSZ nanocomposite material during thermal treatments. in Materials Science and Engineering A-Structural Materials Properties Microstructure and Processing. 2004;375:615-619.
doi:10.1016/j.msea.2003.10.270
https://hdl.handle.net/21.15107/rcub_dais_12878 .
Marinković, Zorica, Mančić, Lidija, Cribier, J. F., Ohara, Satoshi, Fukui, T., Milošević, Olivera, "Nature of structural changes in LSM-YSZ nanocomposite material during thermal treatments" in Materials Science and Engineering A-Structural Materials Properties Microstructure and Processing, 375 (2004):615-619,
https://doi.org/10.1016/j.msea.2003.10.270 .,
https://hdl.handle.net/21.15107/rcub_dais_12878 .
10
15

Pyrosol preparation and structural characterization of SnO2 thin films

Tucić, Aleksandar; Marinković, Zorica; Mančić, Lidija; Cilense, Mario; Milošević, Olivera

(Elsevier Science Sa, Lausanne, 2003)

TY  - JOUR
AU  - Tucić, Aleksandar
AU  - Marinković, Zorica
AU  - Mančić, Lidija
AU  - Cilense, Mario
AU  - Milošević, Olivera
PY  - 2003
UR  - https://dais.sanu.ac.rs/123456789/12877
AB  - Polycrystalline tin oxide thin films were prepared from ethanol solution Of SnCl2.H2O (concentrations: 0.05, 0.1, 0.2 and 0.4 mol/dm(3)) at different substrate temperatures ranging from 300 to 450 degreesC. The kinetic deposition processes were studied in terms of various process parameters. The crystal phases, crystalline structure, grain size and surface morphology are revealed in accordance to X-ray diffractometry and scanning electron microscopy (SEM). Texture coefficients (TCs) for (110), (2 0 0), (2 11) and (3 0 1) reflections of the tetragonal SnO2 were calculated. Structural characteristics of deposited films with respect to varying precursor chemistry and substrate temperature are presented and discussed.
PB  - Elsevier Science Sa, Lausanne
T2  - Journal of Materials Processing Technology
T1  - Pyrosol preparation and structural characterization of SnO2 thin films
SP  - 41
EP  - 45
VL  - 143
DO  - 10.1016/S0924-0136(03)00316-9
UR  - https://hdl.handle.net/21.15107/rcub_dais_12877
ER  - 
@article{
author = "Tucić, Aleksandar and Marinković, Zorica and Mančić, Lidija and Cilense, Mario and Milošević, Olivera",
year = "2003",
abstract = "Polycrystalline tin oxide thin films were prepared from ethanol solution Of SnCl2.H2O (concentrations: 0.05, 0.1, 0.2 and 0.4 mol/dm(3)) at different substrate temperatures ranging from 300 to 450 degreesC. The kinetic deposition processes were studied in terms of various process parameters. The crystal phases, crystalline structure, grain size and surface morphology are revealed in accordance to X-ray diffractometry and scanning electron microscopy (SEM). Texture coefficients (TCs) for (110), (2 0 0), (2 11) and (3 0 1) reflections of the tetragonal SnO2 were calculated. Structural characteristics of deposited films with respect to varying precursor chemistry and substrate temperature are presented and discussed.",
publisher = "Elsevier Science Sa, Lausanne",
journal = "Journal of Materials Processing Technology",
title = "Pyrosol preparation and structural characterization of SnO2 thin films",
pages = "41-45",
volume = "143",
doi = "10.1016/S0924-0136(03)00316-9",
url = "https://hdl.handle.net/21.15107/rcub_dais_12877"
}
Tucić, A., Marinković, Z., Mančić, L., Cilense, M.,& Milošević, O.. (2003). Pyrosol preparation and structural characterization of SnO2 thin films. in Journal of Materials Processing Technology
Elsevier Science Sa, Lausanne., 143, 41-45.
https://doi.org/10.1016/S0924-0136(03)00316-9
https://hdl.handle.net/21.15107/rcub_dais_12877
Tucić A, Marinković Z, Mančić L, Cilense M, Milošević O. Pyrosol preparation and structural characterization of SnO2 thin films. in Journal of Materials Processing Technology. 2003;143:41-45.
doi:10.1016/S0924-0136(03)00316-9
https://hdl.handle.net/21.15107/rcub_dais_12877 .
Tucić, Aleksandar, Marinković, Zorica, Mančić, Lidija, Cilense, Mario, Milošević, Olivera, "Pyrosol preparation and structural characterization of SnO2 thin films" in Journal of Materials Processing Technology, 143 (2003):41-45,
https://doi.org/10.1016/S0924-0136(03)00316-9 .,
https://hdl.handle.net/21.15107/rcub_dais_12877 .
13
13

Preparation of nanostructured Zn-Cr-O spinel powders by ultrasonic spray pyrolysis

Marinković, Zorica; Mančić, Lidija; Marić, R.; Milošević, Olivera

(Elsevier Sci Ltd, Oxford, 2001)

TY  - JOUR
AU  - Marinković, Zorica
AU  - Mančić, Lidija
AU  - Marić, R.
AU  - Milošević, Olivera
PY  - 2001
UR  - https://dais.sanu.ac.rs/123456789/12876
AB  - Ultrasonic spray pyrolysis (1.7 MHz) has been applied for the generation of zinc chromium oxide submicronic (470 nm) particles from the corresponding metal nitrate solution. Heterogeneous gas-liquid/solid chemical reactions occurred in dispersed systems (aerosols) at 1173 K with the residence time ranging from 3 to 6 s. Such a synthesis method enables a high surface reaction and stoichiometric retention at the droplet scale that is of special importance when functional materials with sensing properties are considered. Consequently, homogeneous distributions of the constituting elements and zinc to chromium atomic ratio of about 0.7 are proved by EMAX analysis. The particle morphology, revealed mostly as a composite structure, comprised of primary crystallites smaller than 70 nm. The particle crystalline structure, phase content and decomposition behavior were analyzed in accordance with various methods of analysis (X-ray powder diffraction (XRD). differential scanning calorimetry (DSC). differential thermal analysis (DTA), scanning electron microscopy with X-ray microanalyser (SEM-EMAX)) and discussed in terms of precursor chemistry and process parameters.
PB  - Elsevier Sci Ltd, Oxford
T2  - Journal of the European Ceramic Society
T1  - Preparation of nanostructured Zn-Cr-O spinel powders by ultrasonic spray pyrolysis
SP  - 2051
EP  - 2055
VL  - 21
IS  - 10-11
DO  - 10.1016/S0955-2219(01)00170-4
UR  - https://hdl.handle.net/21.15107/rcub_dais_12876
ER  - 
@article{
author = "Marinković, Zorica and Mančić, Lidija and Marić, R. and Milošević, Olivera",
year = "2001",
abstract = "Ultrasonic spray pyrolysis (1.7 MHz) has been applied for the generation of zinc chromium oxide submicronic (470 nm) particles from the corresponding metal nitrate solution. Heterogeneous gas-liquid/solid chemical reactions occurred in dispersed systems (aerosols) at 1173 K with the residence time ranging from 3 to 6 s. Such a synthesis method enables a high surface reaction and stoichiometric retention at the droplet scale that is of special importance when functional materials with sensing properties are considered. Consequently, homogeneous distributions of the constituting elements and zinc to chromium atomic ratio of about 0.7 are proved by EMAX analysis. The particle morphology, revealed mostly as a composite structure, comprised of primary crystallites smaller than 70 nm. The particle crystalline structure, phase content and decomposition behavior were analyzed in accordance with various methods of analysis (X-ray powder diffraction (XRD). differential scanning calorimetry (DSC). differential thermal analysis (DTA), scanning electron microscopy with X-ray microanalyser (SEM-EMAX)) and discussed in terms of precursor chemistry and process parameters.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Journal of the European Ceramic Society",
title = "Preparation of nanostructured Zn-Cr-O spinel powders by ultrasonic spray pyrolysis",
pages = "2051-2055",
volume = "21",
number = "10-11",
doi = "10.1016/S0955-2219(01)00170-4",
url = "https://hdl.handle.net/21.15107/rcub_dais_12876"
}
Marinković, Z., Mančić, L., Marić, R.,& Milošević, O.. (2001). Preparation of nanostructured Zn-Cr-O spinel powders by ultrasonic spray pyrolysis. in Journal of the European Ceramic Society
Elsevier Sci Ltd, Oxford., 21(10-11), 2051-2055.
https://doi.org/10.1016/S0955-2219(01)00170-4
https://hdl.handle.net/21.15107/rcub_dais_12876
Marinković Z, Mančić L, Marić R, Milošević O. Preparation of nanostructured Zn-Cr-O spinel powders by ultrasonic spray pyrolysis. in Journal of the European Ceramic Society. 2001;21(10-11):2051-2055.
doi:10.1016/S0955-2219(01)00170-4
https://hdl.handle.net/21.15107/rcub_dais_12876 .
Marinković, Zorica, Mančić, Lidija, Marić, R., Milošević, Olivera, "Preparation of nanostructured Zn-Cr-O spinel powders by ultrasonic spray pyrolysis" in Journal of the European Ceramic Society, 21, no. 10-11 (2001):2051-2055,
https://doi.org/10.1016/S0955-2219(01)00170-4 .,
https://hdl.handle.net/21.15107/rcub_dais_12876 .
34
28