Synthesis of ZnO and ZrO2 Powders by Mechanochemical Processing
Само за регистроване кориснике
2007
Чланак у часопису (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
The ZnO and ZrO2 powders were prepared by mechanochemical processing and subsequent heat treatment of the starting powder of precursors mixture of ZnCl2 and Ca(OH)2, and ZrOCl2·8H2O and NaOH, respectively. Inert salt matrix, ether CaCl2 or NaCl, which prevents particle agglomeration was formed during mechanochemical solid state reaction. After mechanochemical treatment, samples were calcined at various temperatures. Selective removal of the matrix phase by washing the resulting powder with appropriate solvent yields almost pure ZnO and ZrO2 powders. Characterization of the powders was performed by X-ray diffraction (XRD), differential thermal and thermo gravimetric analysis (DTA−TG) and scanning electron microscopy (SEM).
Кључне речи:
ZnO / ZrO2 / mechanochemistryИзвор:
Research Trends in Contemporary Materials Science, 2007, 279-284Финансирање / пројекти:
- Синтеза функционалних материјала са контролисаном структуром на молекуларном и нано нивоу (RS-MESTD-MPN2006-2010-142006)
Напомена:
- Materials Science Forum 555
Институција/група
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - JOUR AU - Čeliković, Ana AU - Kandić, Ljiljana AU - Zdujić, Miodrag AU - Uskoković, Dragan PY - 2007 UR - https://www.scientific.net/MSF.555.279 UR - https://dais.sanu.ac.rs/123456789/15645 AB - The ZnO and ZrO2 powders were prepared by mechanochemical processing and subsequent heat treatment of the starting powder of precursors mixture of ZnCl2 and Ca(OH)2, and ZrOCl2·8H2O and NaOH, respectively. Inert salt matrix, ether CaCl2 or NaCl, which prevents particle agglomeration was formed during mechanochemical solid state reaction. After mechanochemical treatment, samples were calcined at various temperatures. Selective removal of the matrix phase by washing the resulting powder with appropriate solvent yields almost pure ZnO and ZrO2 powders. Characterization of the powders was performed by X-ray diffraction (XRD), differential thermal and thermo gravimetric analysis (DTA−TG) and scanning electron microscopy (SEM). T2 - Research Trends in Contemporary Materials Science T1 - Synthesis of ZnO and ZrO2 Powders by Mechanochemical Processing SP - 279 EP - 284 DO - 10.4028/www.scientific.net/MSF.555.279 UR - https://hdl.handle.net/21.15107/rcub_dais_15645 ER -
@article{ author = "Čeliković, Ana and Kandić, Ljiljana and Zdujić, Miodrag and Uskoković, Dragan", year = "2007", abstract = "The ZnO and ZrO2 powders were prepared by mechanochemical processing and subsequent heat treatment of the starting powder of precursors mixture of ZnCl2 and Ca(OH)2, and ZrOCl2·8H2O and NaOH, respectively. Inert salt matrix, ether CaCl2 or NaCl, which prevents particle agglomeration was formed during mechanochemical solid state reaction. After mechanochemical treatment, samples were calcined at various temperatures. Selective removal of the matrix phase by washing the resulting powder with appropriate solvent yields almost pure ZnO and ZrO2 powders. Characterization of the powders was performed by X-ray diffraction (XRD), differential thermal and thermo gravimetric analysis (DTA−TG) and scanning electron microscopy (SEM).", journal = "Research Trends in Contemporary Materials Science", title = "Synthesis of ZnO and ZrO2 Powders by Mechanochemical Processing", pages = "279-284", doi = "10.4028/www.scientific.net/MSF.555.279", url = "https://hdl.handle.net/21.15107/rcub_dais_15645" }
Čeliković, A., Kandić, L., Zdujić, M.,& Uskoković, D.. (2007). Synthesis of ZnO and ZrO2 Powders by Mechanochemical Processing. in Research Trends in Contemporary Materials Science, 279-284. https://doi.org/10.4028/www.scientific.net/MSF.555.279 https://hdl.handle.net/21.15107/rcub_dais_15645
Čeliković A, Kandić L, Zdujić M, Uskoković D. Synthesis of ZnO and ZrO2 Powders by Mechanochemical Processing. in Research Trends in Contemporary Materials Science. 2007;:279-284. doi:10.4028/www.scientific.net/MSF.555.279 https://hdl.handle.net/21.15107/rcub_dais_15645 .
Čeliković, Ana, Kandić, Ljiljana, Zdujić, Miodrag, Uskoković, Dragan, "Synthesis of ZnO and ZrO2 Powders by Mechanochemical Processing" in Research Trends in Contemporary Materials Science (2007):279-284, https://doi.org/10.4028/www.scientific.net/MSF.555.279 ., https://hdl.handle.net/21.15107/rcub_dais_15645 .