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dc.creatorSierra-Fernández, Aránzazu
dc.creatorGómez Villalba, Luz Stella
dc.creatorMilošević, Olivera
dc.creatorFort, R.es
dc.creatorRabanal, Maria Eugenia
dc.date.accessioned2019-01-01T12:47:22Z
dc.date.available2016-04-16
dc.date.issued2014
dc.identifier.issn0272-8842
dc.identifier.urihttp://hdl.handle.net/10016/26936
dc.identifier.urihttp://dais.sanu.ac.rs/123456789/4729
dc.description.abstractControlled magnesium hydroxide particles were successfully synthesized via a simple hydrothermal method. The influence of temperature and reaction time on the hydrothermal synthesis of Mg(OH)(2) was studied. The results provide new parameters to control the morphologies, particle sizes, agglomeration level and crystallographic structures of the brucite nanosized. The physic chemical properties of synthesized Mg(OH)(2) nanoparticles have been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) combined with selected area electron diffraction (SAED), high resolution transmission electron microscopy (HR-TEM) and thermogravimetry/differential scanning calorimetry (TG/DSC). It has been shown that the prolongation of reaction time improves the crystalline degree of magnesium hydroxide particles. It was also possible to detect a relevant increase in the degree of crystallinity and a faster crystal growth with defined hexagonal morphologies in the samples obtained at higher temperature. Our results show that this simple hydrothermal route is highly interesting for the large scale production of these nanomaterials. (C) 2014 Elsevier Ltd and Techna Group S.r.l. All rights reserved.en
dc.description.sponsorshipThis study has been supported by the Geomaterials Programme (S2009/MAT-1629) and the ESTRUMAT Programme (S2009/MAT-1585) and it has been carried out in the Department of Materials Science and Engineering and Chemical Engineering of the University Carlos III of Madrid, Spain. The authors are grateful to the National Center for Electron Microscopy (CNME) for its support with TEM.en
dc.format.mimetypeapplication/pdf
dc.language.isoengen
dc.publisherElsevier
dc.relationGeomaterials Programme, S2009/MAT-1629
dc.relationG.D. of Universities and Research, Madrid Regional Government, Spain, Advanced Structural Materials Program - ESTRUMAT (S2009/MAT-1585)
dc.rightsembargoedAccessen
dc.rightsBY-NC-ND*
dc.sourceCeramics International
dc.subject.otherhydrothermal systhesisen
dc.subject.otherbruciteen
dc.subject.othernanocrystalsen
dc.subject.othercrystallizationen
dc.titleSynthesis and morpho-structural characterization of nanostructured magnesium hydroxide obtained by a hydrothermal methoden
dc.typearticle
dc.citation.spage12285
dc.citation.epage12292
dc.citation.volume40
dc.citation.issue8, Part A
dc.identifier.wos000340328600098
dc.identifier.doi10.1016/j.ceramint.2014.04.073
dc.identifier.scopus2-s2.0-84903904272
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