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dc.creatorJugović, Dragana
dc.creatorMitrić, Miodrag
dc.creatorKuzmanović, Maja
dc.creatorCvjetićanin, Nikola
dc.creatorMarković, Smilja
dc.creatorŠkapin, Srečo Davor
dc.creatorUskoković, Dragan
dc.date.accessioned2017-06-10T15:45:07Z
dc.date.issued2012
dc.identifier.issn0032-5910
dc.identifier.urihttp://dais.sanu.ac.rs/123456789/471
dc.description.abstractLithium iron phosphate powders were obtained by solvothermal treatments of quaternary emulsions Triton X-100/cyclohexane/n-hexanol/water at low temperature (180 °C), with or without stirring. Such synthesis conditions allowed for fast crystallization of pure olivine-type LiFePO4 powder, evidenced by the X-ray powder diffraction measurements and energy dispersive spectroscopy. It has been found that stirring drastically changes the morphology of LiFePO4 particles, causing a preferential crystal orientation. Also, a great difference in the morphology was demonstrated by field emission scanning electron microscopy. The powder obtained after only half an hour of the dynamic solvothermal treatment, without additional post annealing, and without carbon coating, was electrochemically active, showing the discharge capacity of 115 mAh g− 1.en
dc.format219 (2012) 128-134
dc.languageen
dc.publisherElsevier
dc.relationinfo:eu-repo/grantAgreement/MESTD/Integrated and Interdisciplinary Research (IIR or III)/45004/RS//
dc.rightsrestrictedAccess
dc.sourcePowder Technologyen
dc.subjectlithium iron phosphate
dc.subjectLiFePO4
dc.subjectelectrode materials
dc.subjectX-ray diffraction
dc.subjectscanning electron microscopy
dc.titleRapid crystallization of LiFePO4 particles by facile emulsion-mediated solvothermal synthesisen
dc.typearticle
dc.rights.licenseARR
dcterms.abstractЈуговић, Драгана; Ускоковић, Драган; Шкапин, Сречо Давор; Марковић, Смиља; Цвјетићанин, Никола; Кузмановић, Маја; Митрић, Миодраг;
dc.citation.spage128
dc.citation.epage134
dc.identifier.doi10.1016/j.powtec.2011.12.028
dc.identifier.scopus2-s2.0-84856431744
dc.type.versionpublishedVersion
dc.identifier.fulltexthttp://dais.sanu.ac.rs/bitstream/handle/123456789/471/paper734-468.pdf


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