Mechanochemical synthesis of nanocrystalline titanium monoxide
Само за регистроване кориснике
2008
Чланак у часопису (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
Nanocrystalline cubic titanium monoxide, TiOx (0.92 < x < 1.19), with mean crystallite size of ≈ 6 nm, was synthesized by mechanochemical treatment of Ti and TiO2 (rutile) powder mixtures with molar ratios of 1:1, 1.10:1 and 1.25:1. The mechanochemical solid state reaction in a high-energy planetary ball mill was completed for 2 h in either air or argon atmosphere. During heating in vacuum at 900 and 1000 °C for 24 h, nanocrystalline TiOx transforms to a well-crystallized, cubic or monoclinic TiOx. The materials prepared were characterized by XRPD, TGA/DSC and SEM/EDS analysis. © 2008 Elsevier B.V. All rights reserved.
Кључне речи:
ceramics / mechanochemical synthesis / nanomaterials / titanium monoxideИзвор:
Materials Letters, 2008, 62, 17-18, 2769-2771Издавач:
- Elsevier
DOI: 10.1016/j.matlet.2008.01.039
ISSN: 0167-577X
WoS: 000256780700064
Scopus: 2-s2.0-43249090585
Институција/група
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - JOUR AU - Veljković, Ivana AU - Poleti, Dejan AU - Zdujić, Miodrag AU - Karanović, Ljiljana AU - Jovalekić, Čedomir PY - 2008 UR - https://dais.sanu.ac.rs/123456789/3580 AB - Nanocrystalline cubic titanium monoxide, TiOx (0.92 < x < 1.19), with mean crystallite size of ≈ 6 nm, was synthesized by mechanochemical treatment of Ti and TiO2 (rutile) powder mixtures with molar ratios of 1:1, 1.10:1 and 1.25:1. The mechanochemical solid state reaction in a high-energy planetary ball mill was completed for 2 h in either air or argon atmosphere. During heating in vacuum at 900 and 1000 °C for 24 h, nanocrystalline TiOx transforms to a well-crystallized, cubic or monoclinic TiOx. The materials prepared were characterized by XRPD, TGA/DSC and SEM/EDS analysis. © 2008 Elsevier B.V. All rights reserved. PB - Elsevier T2 - Materials Letters T1 - Mechanochemical synthesis of nanocrystalline titanium monoxide SP - 2769 EP - 2771 VL - 62 IS - 17-18 DO - 10.1016/j.matlet.2008.01.039 UR - https://hdl.handle.net/21.15107/rcub_dais_3580 ER -
@article{ author = "Veljković, Ivana and Poleti, Dejan and Zdujić, Miodrag and Karanović, Ljiljana and Jovalekić, Čedomir", year = "2008", abstract = "Nanocrystalline cubic titanium monoxide, TiOx (0.92 < x < 1.19), with mean crystallite size of ≈ 6 nm, was synthesized by mechanochemical treatment of Ti and TiO2 (rutile) powder mixtures with molar ratios of 1:1, 1.10:1 and 1.25:1. The mechanochemical solid state reaction in a high-energy planetary ball mill was completed for 2 h in either air or argon atmosphere. During heating in vacuum at 900 and 1000 °C for 24 h, nanocrystalline TiOx transforms to a well-crystallized, cubic or monoclinic TiOx. The materials prepared were characterized by XRPD, TGA/DSC and SEM/EDS analysis. © 2008 Elsevier B.V. All rights reserved.", publisher = "Elsevier", journal = "Materials Letters", title = "Mechanochemical synthesis of nanocrystalline titanium monoxide", pages = "2769-2771", volume = "62", number = "17-18", doi = "10.1016/j.matlet.2008.01.039", url = "https://hdl.handle.net/21.15107/rcub_dais_3580" }
Veljković, I., Poleti, D., Zdujić, M., Karanović, L.,& Jovalekić, Č.. (2008). Mechanochemical synthesis of nanocrystalline titanium monoxide. in Materials Letters Elsevier., 62(17-18), 2769-2771. https://doi.org/10.1016/j.matlet.2008.01.039 https://hdl.handle.net/21.15107/rcub_dais_3580
Veljković I, Poleti D, Zdujić M, Karanović L, Jovalekić Č. Mechanochemical synthesis of nanocrystalline titanium monoxide. in Materials Letters. 2008;62(17-18):2769-2771. doi:10.1016/j.matlet.2008.01.039 https://hdl.handle.net/21.15107/rcub_dais_3580 .
Veljković, Ivana, Poleti, Dejan, Zdujić, Miodrag, Karanović, Ljiljana, Jovalekić, Čedomir, "Mechanochemical synthesis of nanocrystalline titanium monoxide" in Materials Letters, 62, no. 17-18 (2008):2769-2771, https://doi.org/10.1016/j.matlet.2008.01.039 ., https://hdl.handle.net/21.15107/rcub_dais_3580 .