Complex Metal Oxide Oxidation State Changes Monitoring by TGA and Dilatometric Means
Конференцијски прилог (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
Oxidation processes during metal oxide heat treatment are important events that can be monitored by the means of well-known TGA/DTA and dimensional change diagrams. Powders Mn0.63Zn0.37Fe2O4 oxide was milled in different time duration and thermal analysis techniques afterwards during heating were observed. Cation that serves this purpose well for is Mn ion that passes through Mn2+ to Mn3+ state at 360 °C by oxidation and after that from Mn4+ to Mn3+ reduction process at 580 °C. Minimal data treatment of first derivative on shrinkage for obtaining shrinkage rate diagrams and as well first derivative on thermal gravimetric diagram for obtaining differential thermal gravimetric analysis diagram enable the oxidation and reduction processes monitoring.
Кључне речи:
oxidation / TGA / dilatometryИзвор:
Contemporary batteries and supercapacitors : COIN2022 : program and book of abstracts / International Symposium Belgrade, June 1-2, 2022, 2022, 43-43Издавач:
- Belgrade : University of Belgrade, Faculty of Physical Chemistry
Финансирање / пројекти:
- Министарство науке, технолошког развоја и иновација Републике Србије, институционално финансирање - 200175 (Институт техничких наука САНУ, Београд) (RS-MESTD-inst-2020-200175)
Институција/група
Институт техничких наука САНУ / Institute of Technical Sciences of SASATY - CONF AU - Labus, Nebojša AU - Rosić, Milena AU - Čebela, Maria PY - 2022 UR - https://dais.sanu.ac.rs/123456789/13645 AB - Oxidation processes during metal oxide heat treatment are important events that can be monitored by the means of well-known TGA/DTA and dimensional change diagrams. Powders Mn0.63Zn0.37Fe2O4 oxide was milled in different time duration and thermal analysis techniques afterwards during heating were observed. Cation that serves this purpose well for is Mn ion that passes through Mn2+ to Mn3+ state at 360 °C by oxidation and after that from Mn4+ to Mn3+ reduction process at 580 °C. Minimal data treatment of first derivative on shrinkage for obtaining shrinkage rate diagrams and as well first derivative on thermal gravimetric diagram for obtaining differential thermal gravimetric analysis diagram enable the oxidation and reduction processes monitoring. PB - Belgrade : University of Belgrade, Faculty of Physical Chemistry C3 - Contemporary batteries and supercapacitors : COIN2022 : program and book of abstracts / International Symposium Belgrade, June 1-2, 2022 T1 - Complex Metal Oxide Oxidation State Changes Monitoring by TGA and Dilatometric Means SP - 43 EP - 43 UR - https://hdl.handle.net/21.15107/rcub_dais_13645 ER -
@conference{ author = "Labus, Nebojša and Rosić, Milena and Čebela, Maria", year = "2022", abstract = "Oxidation processes during metal oxide heat treatment are important events that can be monitored by the means of well-known TGA/DTA and dimensional change diagrams. Powders Mn0.63Zn0.37Fe2O4 oxide was milled in different time duration and thermal analysis techniques afterwards during heating were observed. Cation that serves this purpose well for is Mn ion that passes through Mn2+ to Mn3+ state at 360 °C by oxidation and after that from Mn4+ to Mn3+ reduction process at 580 °C. Minimal data treatment of first derivative on shrinkage for obtaining shrinkage rate diagrams and as well first derivative on thermal gravimetric diagram for obtaining differential thermal gravimetric analysis diagram enable the oxidation and reduction processes monitoring.", publisher = "Belgrade : University of Belgrade, Faculty of Physical Chemistry", journal = "Contemporary batteries and supercapacitors : COIN2022 : program and book of abstracts / International Symposium Belgrade, June 1-2, 2022", title = "Complex Metal Oxide Oxidation State Changes Monitoring by TGA and Dilatometric Means", pages = "43-43", url = "https://hdl.handle.net/21.15107/rcub_dais_13645" }
Labus, N., Rosić, M.,& Čebela, M.. (2022). Complex Metal Oxide Oxidation State Changes Monitoring by TGA and Dilatometric Means. in Contemporary batteries and supercapacitors : COIN2022 : program and book of abstracts / International Symposium Belgrade, June 1-2, 2022 Belgrade : University of Belgrade, Faculty of Physical Chemistry., 43-43. https://hdl.handle.net/21.15107/rcub_dais_13645
Labus N, Rosić M, Čebela M. Complex Metal Oxide Oxidation State Changes Monitoring by TGA and Dilatometric Means. in Contemporary batteries and supercapacitors : COIN2022 : program and book of abstracts / International Symposium Belgrade, June 1-2, 2022. 2022;:43-43. https://hdl.handle.net/21.15107/rcub_dais_13645 .
Labus, Nebojša, Rosić, Milena, Čebela, Maria, "Complex Metal Oxide Oxidation State Changes Monitoring by TGA and Dilatometric Means" in Contemporary batteries and supercapacitors : COIN2022 : program and book of abstracts / International Symposium Belgrade, June 1-2, 2022 (2022):43-43, https://hdl.handle.net/21.15107/rcub_dais_13645 .